Plastic Deformation Technique Research Articles

Enhancement of Strength and Hardness in Copper–Chromium–Zirconium Alloy Using Single‐Pass Multi‐Angular Twist Channel Extrusion: A Microstructural and Deformation Study

Herein, the strength and hardness of copper–chromium–zirconium alloy are enhanced in a single pass by a severe plastic deformation (SPD) technique called the multiangular twist channel extrusion (MATE) process. In equal channel angular pressing (ECAP) and twist extrusion (TE), requisite strain and uniformity are achieved through several extrusion passes. MATE is a single‐pass novel SPD technique developed by integrating TE with the ECAP followed by a direct channel zone. The deformation behavior of metal in the MATE process is elucidated through experimental and microstructural studies conducted in each zone. The MATE‐processed Cu–Cr–Zr alloy achieves a hardness of 184.4 Hv and a tensile strength of 645.2 MPa, reflecting an increase of 80.43% and 69.7%, respectively, relative to the annealed condition. The electrical conductivity of the MATE‐processed Cu–Cr–Zr alloy decreases to 74.29% International Annealed Copper Standard. The electron backscatter diffraction investigation reveals an average grain size of 2.8 μm, with 61% comprising low‐angle grain boundaries, while the calculated dislocation density, from X‐ray diffraction analysis, is 3.93 × 1014 m−2. The transmission electron microscopy image verifies the existence of dislocations and precipitates in the Cu–Cr–Zr alloy. The experimental and microstructural findings in each zone have aligned effectively.

Optimizing high-pressure sliding process parameters for grain refinement and enhanced mechanical properties using response surface methodology approach

Lightweight technology has emerged as a crucial focus within transportation machinery manufacturing, driving the pursuit for materials with exceptional strength-to-weight ratios. To address this need, ultra-fine grain (< 500 nm) and nanostructured (< 100 nm) materials are being developed using severe plastic deformation (SPD) techniques, particularly in confined flat sheets. This study focuses on the Multi Pass Incremental Feed High-Pressure Sliding (MPIF-HPS) technique, which offers significant potential for industries such as aerospace and automotive by enhancing the mechanical properties of materials like AA 7075 alloy. This work investigates the development and characterization of ultrafine-grained materials through SPD, focusing on the correlation between ultrafine grain structures and their distinct properties. Utilizing MPIF-HPS processes and design of experiment (DoE) methodologies, the study evaluates the evolution of fine-grained microstructures and the enhancement of boundary characteristics with increasing strain in AA 7075 alloy. The grain size was refined from 600 µm to 6 µm, indicating significant microstructural improvement. Concurrently, mechanical properties were notably enhanced, with hardness increasing from 102 to 165 HV, yield strength from 250 to 605 MPa, and ultimate tensile strength (UTS) from 400 to 650 MPa. The study systematically optimized processing parameters, including pressure, sliding distance, and number of passes, to determine the ideal conditions for grain refinement and mechanical performance. These findings underscore the critical role of strain-induced boundary characteristics in determining the material's final properties, paving the way for tailored solutions to meet specific industrial requirements.

Uncovering the influence of deformation amount on microstructure evolution and mechanical behavior of the multi-DoF formed WE43 magnesium alloy

The urgent need of improving energy efficiency accelerates the development of lightweight magnesium alloy, especially for high-performance wrought magnesium alloy. In this research, multi-degrees of freedom (multi-DoF) forming process as a novel severe plastic deformation technique was applied to the forged-annealed WE43 magnesium alloy plates. The effect of deformation amounts ranging from 10% to 40% on microstructure and mechanical property of the experimental material was investigated in detail. Initially forged-annealed WE43 magnesium alloy is composed of rodlike-shaped Mg12Nd and cuboid-shaped Mg24Y5 at the grain boundaries as well as globular-shaped Mg41Nd5 inside the grains. Multi-DoF forming process results in remarkable microstructure change, which is characterized by increasing dissolution of these second phases, grain refinement, formation of twins and disappearance of basal texture in WE43 magnesium alloy with deformation amounts increasing. Compared with the initial forged-annealed one, the multi-DoF formed WE43 magnesium alloy displays an increasing tensile strength but a decreasing plasticity with deformation amounts increasing. The increasingly improved strength is mainly attributed to the joint contribution of increasing solution strengthening, fine-grained strengthening and work hardening, while the increasingly decreased plasticity is mainly attributed to the increasing dislocation despite the basal texture disappearing. This research will provide a novel method of fabricating high-performance wrought magnesium alloy.

Impacts of T6 heat treatment on the microstructural, mechanical, and corrosion properties of thixoformed AA7075 alloy produced by cooling slope casting

Abstract Research into semi-solid metal forming techniques has been ongoing for an extended period with the aim of producing near-net shape products from aluminum alloys. The primary focus has traditionally been on casting alloys seeking to offer an alternative to the other processes such as high pressure die casting. Over the past twenty years, wrought aluminum alloys have also been explored for thixoforming operations as an alternative to traditional plastic deformation techniques. This research investigated the impacts of T6 heat treatment on the microstructural, mechanical, and corrosion properties of AA7075 alloy samples produced through cooling slope casting and subsequent thixoforming with different reheating durations. The selected alloy was chosen due to its widespread use in various industries, attributed to its excellent strength-to-density ratio achieved after T6 heat treatment. Building on optimized cooling slope casting parameters from a prior study, the standard solution treatment procedure following thixoforming with extended reheating times was found to be inadequate. Hardness and tensile tests revealed that specimens reheated for 120 min exhibited significantly reduced response to T6 treatment. Despite achieving the targeted hardness value of 154 HB with samples reheated for 20 min prior to thixoforming and T6 heat treatment, especially the elongation at break values were unsatisfactory. Potentiodynamic polarization tests indicated that corrosion primarily involved grain dissolution, with longer reheating times decreasing corrosion resistance due to increased amount of secondary phases and grain isolation. These findings highlight that while AA7075 alloy can be processed into semi-solid formable materials via cooling slope casting, issues such as hot tearing, micro-shrinkage, and physical defects post-thixoforming hinder the achievement of desired tensile properties.

A new severe plastic deformation technique of combined extrusion and torsion to prepare bulk ultrafine grained copper

Reducing grain size is a well-established method for strengthening metals. In this study, a novel severe plastic deformation technique—combined extrusion and torsion (CET) with composite strain—was developed to fabricate bulk ultrafine grained metals. A single pass of CET treatment (with a rotation velocity of 1 r/s and extrusion speed of 3 mm/s) refined coarse-grained copper from 54 μm to 450 nm at room temperature, resulting a significant increase in hardness from 0.55 GPa to 1.3 GPa. The CET technique addresses the limitations of conventional extrusion-processed copper (without torsion), which suffers from gradient microstructure and hardness distribution. It provides enhanced strain accumulation under the same extrusion ratio conditions. The more homogeneous microstructures and properties of CET-processed copper rods are attributed to the reduced strain gradient due to torsion. Additionally, targeted finite element analysis indicated that the CET technology requires 37 % less extrusion load and offers at least 30 % more strain compared to conventional extrusion methods. Compared with other severe plastic deformation methods, such as equal channel angular pressing and high-pressure torsion, which involve simpler deformation processes, the CET technique shows considerable promise for large-scale manufacturing of ultrafine-grained metals.

Investigation into the shear effect of torsion extrusion process

Torsion extrusion (TE) is a severe plastic deformation (SPD) technique with the potential to be used for the preparation of large bulk materials with enhanced mechanical properties. Shear deformation is the key factor for SPD to enhance the materials properties. However, it is not clear by far that what shear strains are dominant in torsion extrusion process and how they distribute in the extruded materials. These issues are crucial to the working parameters design of the torsion extrusion process for maximizing the shear effect. To this end, a plasticine billet with two colors was applied as experimental material, and the material flow pattern was revealed by measuring the twisted bicolor interfaces. The torsion extrusion was implemented using a die with a wavy cross-sectional bearing segment (W-TE), which is able to prevent the circumferential sliding of the materials against the die. Flow velocities were re-built according to the bicolor interfaces at each section in a cylindrical system. Strain rates and shear strains induced by torsion deformation along the radius of the material were formulated based on the velocity field and Eulerian variable derivatives, from which the dominant shear strain can be recognized. A shear effect index (SEI) was proposed to evaluate the contribution of the shear strains induced by torsion, and the distribution of SEI was analyzed. Furthermore, the W-TE experiments on the as-cast TiB2/2026 Al composite were carried out to demonstrate the positive correlation between the shear effect and the microstructural improvement, and finite element simulation for such experiments showed the consistency of the simulated deformation patterns with the plasticine measured ones. The evaluation method and the experimental results deepened the understanding to the shear effect of torsion extrusion process.

Low-Carbon Steel Formed by DRECE Method with Hot-Dip Zinc Galvanizing and Potentiodynamic Polarization Tests to Study Its Corrosion Behavior

The use of low-carbon unalloyed steel with minimal silicon content is widespread in structural steel and automotive applications due to its ease of manipulation. The mechanical properties of this steel can be significantly enhanced through severe plastic deformation (SPD) techniques. Our study focuses on the practical benefits of the dual rolling equal channel extrusion (DRECE) method, which strengthens the steel and has implications for material hardness and the thickness of subsequently applied hot-dip zinc galvanizing. Furthermore, the steel’s corrosion potential and current are investigated as a function of material hardness and thickness. The findings show a 20% increase in hardness HV 30 after the first run through the forming machine, with an additional 10% increase after the second run. Subsequent galvanizing leads to a further 1–12% increase in HV 30 value. Notably, the DRECE hardening demonstrates no statistically significant effect on the corrosion potential and current; however, the impact of galvanizing is as anticipated.

Research Progress on the Microstructure Evolution Mechanisms of Al-Mg Alloys by Severe Plastic Deformation.

Al-Mg alloys are widely used as important engineering structural materials in aerospace engineering, transportation systems, and structural constructions due to their low density, high specific strength, corrosion resistance, welding capability, fatigue strength, and cost-effectiveness. However, the conventional Al-Mg alloys can no longer fully satisfy the demands of practical production due to difficulties caused by many defects. The high strength of Al-Mg alloys as non-heat treatment precipitation-strengthened alloys is achieved primarily by solid solution strengthening along with work hardening rather than precipitation strengthening. Therefore, severe plastic deformation (SPD) techniques can be often used to produce ultrafine-grained structures to fabricate ultra-high strength aluminum alloys. However, this approach often achieves the strengthening of material at the cost of reduced ductility. This paper comprehensively summarizes the various approaches of ultrafine/nanocrystalline materials for enhancing their plasticity, elaborates on the creation of a bimodal microstructure within the alloy, and discusses the formation of a nanotwin microstructure within the alloy and the incorporation of dispersed nanoparticles. The mechanisms underlying both the strengthening and toughening during large plastic deformation in aluminum alloys are summarized, and the future research direction of high-performance ultrafine crystalline and nanocrystalline Al-Mg aluminum alloys is prospected.

Effect of Dislocation Density on the Dynamic Strength of Aluminium

The effects of cold work on dynamic flow strength is studied through measurements of dislocation density and elastic precursor attenuation in shocked aluminium. High-purity aluminium and Al 6082 alloy samples are subjected to up to three passes of rotary swaging, a severe plastic deformation (SPD) technique, in order to produce large variations in starting material conditions. Detailed material characterisation is performed using electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM) to determine the initial dislocation density, texture, grain boundary density and misorientation distribution. Variations in dynamic strength are studied through the evolution of the elastic precursor amplitude with propagation distance in specimens with thicknesses between 0.2 and 1 mm, shock loaded to impact stresses of about 4.6 GPa. It is shown that dynamic strength decreases with increasing initial dislocation density in both materials, demonstrating rare, quantified measurements of a reversal in the effect of dislocation density on yield strength at strain rates around 104 s-1 and above.

Optimized mechanical properties of the hot forged Ti–6Al–4V alloy by regulating multiscale microstructure via laser shock peening

The hot forged Ti–6Al–4V alloy demonstrates well constructed microstructure and balanced mechanical properties, which promotes its wide application in aviation field. However, its relative poor resistance to wear and foreign object impact usually leads to the cumulative damage, causing sudden failure and serious accident. Laser shock peening (LSP) is a novel surface plastic deformation technique, which could strengthen the surface layer of components through gradient grain structure. Nevertheless, the specific mechanism of microstructure evolution and mechanical properties enhancement of LSP processed hot forged Ti–6Al–4V alloy is still obscure, and its corresponding explanation would help the wide application. In the present research, the hot forged Ti–6Al–4V alloy was processed by LSP to regulate its superficial microstructure and improve mechanical properties, helping to understand the inner mechanism. The results reveal that LSP could simultaneously result in the merging of ultrafine α-Ti grains and refinement of coarse α-Ti grains, which reconstruct the dual-size grain structure. The crystal tilting and transformation promoted by the generation and movement of dislocations benefit the merging of ultrafine grains. Due to the different slip systems in dual phases, β-Ti phases exhibit much greater response to slip under surface plastic deformation, which are enforced to deform and construct the shell structure by sliding and phase transformation, while the α-Ti phases act as the core to synergistically construct ‘core-shell’ like structure. The increase of LSP impact time promotes the well wrapping of the ‘core-shell’ like structure and strengthens it by abundant dislocations, which also forms the gradient grain structure from surface to inner. Since the microstructure regulation and crystal defects engineering, the LSP improves the surface damage resistance and mechanical properties of the hot forged Ti–6Al–4V alloy obviously. Such results indicate a new technology to increase the properties of the hot forged Ti–6Al–4V alloy component further.

Low-Temperature Superplasticity of Ultrafine-Grained Aluminum Alloys: Recent Discoveries and Innovative Potential.

The last two decades have witnessed significant progress in the development of severe plastic deformation techniques to produce ultrafine-grained materials with new and superior properties. This review examines works and achievements related to the low-temperature superplasticity of ultrafine-grained aluminum alloys. The examples are provided of the possibility to observe low-temperature superplasticity in aluminum alloys at temperatures less than 0.5 Tmelt and even at room temperature, and herein, we demonstrate the cases of achieving high ductility and high strength in aluminum alloys from processing utilizing severe plastic deformation. Special emphasis is placed on recent studies of the formation of segregations of alloying elements at grain boundaries in UFG Al alloys and their influence on the development of grain boundary sliding and manifestation of low-temperature superplasticity. In addition, the current status and innovative potential of low-temperature superplasticity in aluminum alloys are observed.

EFFECTS OF PROCESSING AL-MG ALLOY BY SEVERE PLASTIC DEFORMATION: TENSILE PROPERTIES AT HIGH TEMPERATURES

Aluminum and wrought non age-hardenable such as Al-Mg alloys became interesting alternatives for various structural applications in spite of generally moderate strength, but relatively good formability and good corrosion resistance. Increasing overall strength while preserving or even improving ductility in special conditions without any any change in chemical composition that oppositely could alter other features of the material - such as weldability, becomes an objective worthy of research. A suitable way to increase the potential of Al-Mg alloys is the raising up the mechanical properties by structural refinement. Ultrafine grain size provides enhanced mechanical and/or physical properties such as strength and very good ductility – close to superplasticity at slightly higher strain rate and relatively lower temperatures – and better corrosion resistance. Well-known as one of the most encouraging and efficacious structure refining method amid other severe plastic deformation (SPD) techniques, equal channel angular pressing (ECAP) has been deeply investigated thanks to dramatic improvements in structure and therefore properties of bulk ultrafine grained/nanostructured materials. The aim of this study is to evaluate by tensile testing at higher temperatures the mechanical properties of an Al-3.4%Mg alloy previously processed by ECAP up to 8 passes, as a candidate for replacing AA5154 which contains different amounts of chromium. The tensile tests conducted at different temperatures using a computer-controlled testing machine with different strain rates showed in terms of engineering stress vs. engineering strain evolution that the ECAPed Al-3.4%Mg alloy have the potential to be used in technological processes at high temperatures, opening opportunities for industrial applications requiring high ductility.

Pt Schwarz crystals stabilized by minimal-surface grain boundaries and twins at the grain size limit

Schwarz crystals with uniformly distributed twins enclosed by general grain boundaries (GBs) resembling triply minimal-surfaces were observed in high stacking fault energy metal Pt which is believed not readily to twin. By refining the grains of pure Pt from 140 μm to several nanometers via plastic deformation technique, deformation twins were found to emerge numerously and the structural morphologies of Schwarz crystals can be identified at grain sizes below 4 nm. Both experiments and atomistic simulations suggest that Pt Schwarz crystals are thermally stable at temperatures approaching the thermal equilibrium melting point. The measured room temperature microhardness as a function of grain size, on the other hand, may increase monotonically up to 12.9 GPa, revealing a sustained Hall-Petch relationship. The observed outstanding mechanical stabilities can be attributed to that, regardless of the critical twin size and the stacking fault energy of the material, the plastic deformation at the grain size limit is solely limited by twinning and both the nucleation and bowing-out of twinning partial dislocations from GB sources are notoriously difficult according to simulations and theory.

Excellent strength-ductility synergy of Cu-Al alloy with a gradient nanograined-nanotwinned surface layer

Gradient nanostructured (GNS) metallic materials have shown significant potential in achieving excellent mechanical properties. However, the underlying strengthening mechanisms resulting from plastically inhomogeneous deformation in GNS materials, particularly those involving nanotwinned structures, remain inadequately understood. In this study, a gradient nanograined-nanotwinned (GNNT) surface layer was generated on a Cu-Al alloy using the severe plastic deformation technique known as single-point diamond turning. Uniaxial tensile and localized micropillar compression tests were conducted to compare the mechanical properties of GNNT samples with conventional gradient nanograined (GNG) and uniform coarse-grained (CG) Cu/Cu-Al counterparts. The results revealed that the GNNT samples exhibit excellent strength-ductility synergy, with a yield strength of approximately 329 MPa, tensile strength of around 477 MPa, and uniform ductility of about 48 %, thereby demonstrating remarkable strain hardening capacity and mechanical stability. These characteristics are further supported by the observed strong back stress effect, well-preserved mobile dislocation density, and effective suppression of grain coarsening in the GNNT surface layer. In contrast to the evident mechanically induced grain coarsening through grain boundary (GB) migration in the GNG surface layer, grain coarsening through twin boundary (TB) migration in GNNT surface layers is effectively inhibited by Lomer-Cottrell (L-C) locks formed by TB-stacking fault and TB-TB intersections, resulting in significantly enhanced structural stability. Furthermore, the L-C locks also extensively contribute to the high density of mobile dislocations observed in the GNNT samples. These findings provide valuable insights into the optimization of GNS structures for achieving excellent strength-ductility synergy in metallic materials.

Parts repairing and microstructural refinement of high-pressure die cast aluminum alloys through friction stir processing for bulk production

A key challenge in the production of high-grade automotive aluminum components through the High-Pressure Die Casting (HPDC) process is the imperative to minimize imperfection. In addressing this concern, this study utilizes friction stir processing (FSP), a widely recognized intense plastic deformation technique. FSP is applied to systematically alter the microstructure of HPDC Al-4Mg-2Fe, a prominent alloy extensively used in the die-casting sector. By using the pass strategy to incorporate both one-pass and two-pass approaches, the microstructure is selectively altered to establish a defect-free processed zone. The utilization of FSP demonstrates its efficacy in breaking aluminum dendrites and acicular silicon particles, leading to a uniformly dispersed arrangement of equiaxed silicon particles within the aluminum-based matrix. In addition, FSP eradicates porosity and disintegrates needle-like Fe particles, resulting in a more refined and homogeneously distributed structure. Subsequently, the material's mechanical properties processed by FSP were assessed in the longitudinal direction concerning the processing axis and then compared with those of the original base material.The microstructural refinement and reduction in porosity induced by FSP result in a notable enhancement in hardness, with an increase of 23 % after one pass and 37 % after two passes. The substantial improvement in mechanical properties during the FSP process is predominantly attributed to modifications in the morphology, refinement, and dispersion of intermetallic particles within the matrix. This improvement is further complemented by the ultrafine dispersion of casting defects.This study underscores the efficacy of FSP as a valuable tool for modifying microstructures and improving mechanical properties in HPDC Al-4Mg-2Fe alloys. Such advancements align with the lightweighting objectives pursued by the automotive industry.

Constrained groove uniform pressing process for achieving homogeneously improved properties in copper

Constrained groove pressing (CGP) is a popular method to produce an ultrafine-grained microstructure and thus enhanced mechanical properties in the metal sheet. CGP is a severe plastic deformation technique that simultaneously presses the metal sheet with flat and grooved dies to subject it to large shear strain without changing the dimensions. The inherent inhomogeneity of the processed sheet may be a drawback of the CGP process. According to published research, this is caused by the sharp edges of the grooved dies responsible for additional bending strain along with shear strain. Moreover, even if the grooves are made circular, it can impart constant bending strain, but the shear strain varies. In this research, a new die has been designed to impart constant combined bending and shear strain in the metal sheet using constrained groove uniform pressing. Hence, the process is changed as the number of presses required for 1 pass are changed and named constrained groove unform pressing. C101 was used as the material for the new process. Properties of the copper sheet observed to be improved homogeneously as it was processed through the new die and process. The uniformity of the imposed strain was verified by theoretical, experimental, and simulation results.

Experimental research on mechanical, material, and metallurgical properties of Inconel 600: Application in elevated temperature environment

Experimental research on mechanical, material, and metallurgical properties of Inconel 600: Application in elevated temperature environment

Interaction of electric current with burnishing parameters in surface integrity assessment of additively manufactured Inconel 718

One of main problem associated with surface sever plastic deformation (SSPD) techniques like low plasticity burnishing (LPB) of metallic materials is limitation of surface integrity improvement at further loads (i.e. static force or pass number). It is due to interlocking of dislocation motion that limits further plastic deformation. As a plausible solution, in the present work, electric current assisted burnishing (ECAB) is introduced to use the concept of electroplasticity in surface integrity (roughness, hardness and residual stress) enhancement of Inconel 718 by additive manufacturing. Nevertheless, there are some researches which use this method to enhance performance of SSPD, the interaction effect of electrical parameter like current density with other parameters haven’t been studied well. Thus, to make the process optimized in terms of surface integrity aspects, parametric study of ECAB process with focus on interaction of current density with other LPB parameters merits further investigations. Thus, in the present work, an experimental study was carried out to identify the interaction effect of current density (as main parameter of ECAB) with other burnishing parameters (spindle speed, feed rate, current density, pass number and static force) on surface integrity aspects. Analysis of variances was further carried out to identify the contribution of each parameter on performance measures. Then, the interaction plots based on polynomial regression were developed, analyzed and discussed based on the physic of plastic deformation and some microscopic analysis like surface topography, scanning electron microscopy and X-ray diffraction analysis. It was found from the results that electric current density has the greatest effect on surface integrity aspect with contribution of 60 % on surface roughness, 68.5 % on hardness and 30 % on surface compressive residual stress. On the other hand it was found that this parameter has high interaction with process factors while applying different current density changes the optimum burnishing setting for each performance measures. Application of LPB at optimum parameter setting causes improvement of surface roughness of as-built material about 54 %; further improvement of 70 % and 85 % in roughness values were also achieved when the electric current with densities of 5A/mm2 and 10A/mm2, respectively were applied to burnishing process at optimum setting. It was also found that application of optimum LPB as well as optimum ECAB with densities of 5A/mm2 and 10A/mm2, results in improving the surface hardness about 17.5 %, 42 % and 68 %, respectively. In addition, under foresaid post-processing sequence, the surface compressive residual stress enhanced from 121 MPa (tensile type) for as-built material to −208 MPa, −345 MPa and −488 MPa (compressive type). Finally, the most optimum solution results in minimum surface roughness as well as maximum hardness and residual stress were identified by desirability approach function as 300RPM spindle speed, 0.08 mm/rev feed rate, 10A/mm2 current density, 3 pass number and 300 N force. To show the application of this optimization in a real life problem, fatigue resistance of optimum samples for high cycle and low cycle testing were obtained and compared with as-built material. It was found that following this post-treatment, the life cycle of samples improves from 160 % to 270 %, respectively that affirms practical application and manufacturing efficiency of proposed approach.

Deformation mechanism and hardening behavior of gradient heterostructured magnesium alloys prepared by severe shear deformation

Lightweight equipment in aerospace and other fields urgently requires magnesium (Mg) alloys components with high-strength plasticity. For this reason, in this study, a gradient heterogeneous structure containing nanocrystallines was constructed successfully using a severe shear deformation process that combines severe plastic deformation techniques and torsional deformation characteristics. The evolution of the microstructure and hardness of Mg-12.12Gd-4.2Y-2.28Zn-0.36Zr (wt%) alloys prepared by severe shear deformation with changes in deformation temperature were investigated. The gradient heterogeneous structure of the alloys formed naturally under high hydrostatic pressure and severe shear stress, and its thickness increased with the deformation temperature. With the application of shear stress, a large amount of rotational dynamic recrystallization (RDRX) behavior occurs in the alloys, refining the coarse initial grains (∼126.3 µm) into fine grains (∼2.03 µm) or even ultrafine grains (∼1 µm). During the RDRX process, low angle grain boundaries (LAGBs) began to form at high distorted grain boundaries and unique lamellar structures, followed by a rapid expansion into the interior of the grains, which ultimately results in the grains being completely covered by subgrains. Meanwhile, the continuously broken long-period stacking-ordered (LPSO) phase and the precipitated bright rare earth rich (RE-rich) phase provide a large number of nucleation sites, further promoting the refinement process of the grains. Subsequently, the grains were further refined to nanocrystallines through the formation and rotation of subgrains under continuous loading of stress. The massive formation of nano-precipitated phases (β phases) along grain boundaries were accompanied by the complete disappearance of other types of second phases. The sources of β phases formation include the layer-by-layer decomposition of the cellular phases and the dissolution/re-precipitation of the LPSO phases. In addition, the introduction of shear stress promotes the random orientation of the DRXed grains through the extensive activation of pyramidal <a> and pyramidal <c+a> slip. The hardness of the alloys gradually decreased as the cumulative strain decreased at different deformation temperature conditions. When the deformation temperature was 440°C, the alloys reached a maximum hardness of 127.67 HV, which was nearly 43.5% higher than homogenized alloys. The ultra-high hardness of the alloys prepared by severe shear deformation is mainly attributed to grain boundary hardening, diffusion hardening and hetero-deformation induced (HDI) hardening.

Nanostructuring of Ferritic Steel: A Review on Enhanced Surface Properties Using Ultrasonic Shot Peening

Nanostructuring of ferritic stainless steel refers to the process of intentionally reducing the grain size of the material at the nanoscale level. By manipulating the microstructure of the steel, it is possible to enhance its mechanical, physical, and chemical properties. Nanostructuring can significantly improve the strength, hardness, and wear resistance of ferritic stainless steel, while still maintaining its corrosion resistance. The increased density of grain boundaries and the complex dislocation network within the nanostructured material contribute to these improved properties. Moreover, the nanostructured ferritic stainless steel exhibits enhanced thermal stability, leading to better high-temperature performance and resistance to creep deformation. The small grain size also allows for increased precipitation of secondary phases, such as carbides, nitrides, or intermetallic compounds, which can further improve the material's properties. There are several methods to achieve nanostructuring in ferritic stainless steel, such as severe plastic deformation (SPD) techniques like high-pressure torsion, equal channel angular pressing, and accumulative roll bonding. These techniques impose extreme plastic deformation on the material. Leading to grain refinement below the micrometre range. Also, a novel method of surface nanostructuring ultrasonic shot peening (USP) is discussed in detail. Shot peening is a process in which small, spherical media, typically made of steel or ceramic, called "shots," are propelled onto the surface of a material at high velocities. Ultrasonic shot peening enhances the traditional shot peening process by introducing high-frequency vibrations to the shots. These vibrations are generated by an ultrasonic transducer, which is immersed in a bath of shots and liquid. The vibrations are transmitted through the liquid to the shots, causing them to collide with the surface of the ferritic steel at even higher velocities and energy levels than in traditional shot peening. In summary, nanostructuring of ferritic stainless steel offers great potential for tailoring the material's properties to meet specific application requirements, including improved strength, hardness, wear resistance, corrosion resistance, and high-temperature performance. USP is an effective surface treatment method for ferritic steel, offering advantages in terms of fatigue life, stress corrosion cracking resistance, surface hardness, and wear resistance.