Abstract Through a deoxygenation reaction, fatty acid-containing biomass resources including palm fruit, palm kernels, and soybeans can be converted into green diesel (bio-hydrocarbon). In this study, low-cost Indonesia natural zeolite was utilized as catalyst support for nickel, cobalt and a nickel/cobalt mixture. All prepared catalysts were used as catalyst for bio-hydrocarbon production via deoxygenation of fatty acid. The catalytic activity of each catalyst in the production of bio-hydrocarbon from fatty acid was investigated. Selectivity of each catalyst to hydrocarbon products, heptadecane, heptadecene, octadecene, and octadecane was studied as well. The results showed all prepared mono- and bi-metallic catalyst exhibited high conversion of fatty acid, more than 90% with a different yield of biohydrocarbon.