This study concerns the analysis of atmospheric nitrogen dioxide and formaldehyde vertical column data in Kinshasa. The methodology uses the principle of synchronous detection. To do this, an algorithm was implemented and applied to search for the different harmonics in the spectra and to determine their respective characteristics. A multitude of harmonics was found in all frequency domains for each time series of the abundances of the considered atmospheric pollutants. The results of this study reveal an analysis technique capable of extracting weak signals embedded in a very high amplitude noise. In addition, apart from the information on the frequency, the analysis by synchronous detection makes it possible to obtain the phase and the amplitude of these signals extracted from the noise. Additionally, synchronous detection is able to find a particular oscillation buried in the noise and to determine its characteristics. It is therefore possible to study the phenomena associated with this oscillation (the rhythm of human activities, the alternation of seasons, the various tides, the Madden Julian or EL NINO oscillations) as well as the forces that maintain it (the various gravitational forces). The knowledge of the characteristics of a particular oscillation could also allow the exploration of the atmospheric environment of Kinshasa (emission site, altitude and relative abundance of atmospheric pollutants)