Optical Backscatter Reflectometry Research Articles

Estimating crack tip position in adhesively bonded joints subjected to mode II quasi‐static loading

AbstractThis study aimed at estimating crack tip position in adhesive bonded joints under mode II quasi‐static loading using experimental and numerical approaches. Experimental techniques were utilized and compared, including optical backscatter reflectometry, visual testing, and a novel strategy based on digital image correlation. Additionally, a finite element analysis was employed to identify the numerical crack tip position and the extent of damage within the bondline. This analysis revealed that a significant portion of the crack propagation region in the adhesive is occupied by the fracture process zone. Moreover, optical backscatter reflectometry shows the potential to detect this process zone within the adhesive that the other methods may not detect. This capability is particularly beneficial for detecting damage at early stages.

Towards REPO4 nanocrystal-doped optical fibers for distributed sensing applications

Rayleigh scattering enhanced nanoparticle-doped optical fibers, for distributed sensing applications, is a new technology that offers unique advantages to optical fiber community. However, the existing fabrication technology, based on in situ grown alkaline earth nanoparticles, is restricted to few compositions and exhibit a great dependence on many experimental conditions. Moreover, there is still several uncertainties about the effect of drawing process on the nanoparticle characteristics and its influence on the scattering enhancement and the induced optical loss. In this work, we shed light on all these issues that prevent the progress in the field and demonstrate the suitability of doping optical fibers with YPO4 nanocrystals for developing tunable Rayleigh scattering enhanced nanoparticle-doped optical fibers. An exhaustive 3D microstructural study reveals that their features are closely linked to the fiber drawing process, which allow the size and shape engineering at the nanoscale. In particular, the YPO4 nanocrystals preserve their features to a large extent when the optical fibers are drawn below 1950 °C, which allows obtaining homogeneous nanocrystal features and optical performance. Fabricated fibers exhibit a tunable enhanced backscattering in the range of 15.3–54.3 dB, with respect to a SMF-28 fiber, and two-way optical losses in the range 0.3–160.7 dB/m, revealed by Optical Backscatter Reflectometry (OBR) measurements. This allows sensing lengths from 0.3 m up to more than 58 m. The present work suggests a bright future of YPO4 nanocrystals for distributed sensing field and open a new gate towards the incorporation of other rare-earth orthophosphate (REPO4) nanocrystals with pre-defined characteristics that will overcome the limitations of the current in situ grown alkaline earth-based technology.

Reflector-less refractive index sensors based on etched-tapered high-scattering single-mode optical fibers

Reflector-less refractive index (RI) sensors employ simple optical fiber strictures for the accurate detection of RI changes. They operate in absence of any reflective element such as gratings, filters, interferometers while maintaining the form factor of a reflective probe; the RI dependence is encoded in the Rayleigh backscattering signatures, and is interrogated using optical backscatter reflectometry. In this work, we present a new reflector-less fiber-optic sensor based on two-steps: (1) tapering an optical fiber, followed by (2) rapid etching of the fiber. The combination of the two steps allows obtaining significant advantages in terms of manufacturing, making the process simpler and increasing the distribution of the refractive index detection. The sensitivity obtained is up to 110.9 GHz/RIU (refractive index units), with the possibility of detection over a length of 2.1 mm, with 0.035 mm average spatial resolution over distributed RI sensing.

Enhanced backscatter and unsaturated blue wavelength shifts in F-doped fused silica optical fibers exposed to extreme neutron radiation damage

Amorphous fused silica (a-SiO2) optical fibers, with and without inscribed Bragg gratings, were interrogated using infrared (∼1550 nm) optical backscatter reflectometry during ∼25 days of intense neutron irradiation to a fast (energy > 0.1 MeV) neutron fluence of ∼1021 n/cm2, or ∼1.5 atomic displacements per atom. The reflected light amplitudes in Ge-doped core telecommunications fiber dropped below detection limits (>15 dB attenuation) within 3 days of irradiation (∼1020 fast n/cm2). Amplitudes from a pure silica core, F-doped silica cladding fiber reached equilibrium levels ∼1.5–2 dB higher than pre-irradiation values, whereas Bragg gratings inscribed in the same fiber using a femtosecond laser (point-by-point method) suffered > 45 dB attenuation. Blue wavelength shifts were initially consistent with previous radiation-induced compaction models but increased linearly with increasing neutron fluence (no evidence of saturation) beyond 1020 n/cm2 and exceeded 0.6%, which corresponds to >1,000 °C drift if used to measure temperature changes.

Towards Automatic Crack Size Estimation with iFEM for Structural Health Monitoring.

The inverse finite element method (iFEM) is a model-based technique to compute the displacement (and then the strain) field of a structure from strain measurements and a geometrical discretization of the same. Different literature works exploit the error between the numerically reconstructed strains and the experimental measurements to perform damage identification in a structural health monitoring framework. However, only damage detection and localization are performed, without attempting a proper damage size estimation. The latter could be based on machine learning techniques; however, an a priori definition of the damage conditions would be required. To overcome these limitations, the present work proposes a new approach in which the damage is systematically introduced in the iFEM model to minimize its discrepancy with respect to the physical structure. This is performed with a maximum likelihood estimation framework, where the most accurate damage scenario is selected among a series of different models. The proposed approach was experimentally verified on an aluminum plate subjected to fatigue crack propagation, which enables the creation of a digital twin of the structure itself. The strain field fed to the iFEM routine was experimentally measured with an optical backscatter reflectometry fiber and the methodology was validated with independent observations of lasers and the digital image correlation.

Investigation of the Optical Properties of Silicon-on-Insulator Microring Resonators Using Optical Backscatter Reflectometry

Introduction. Optical backscatter reflectometry is one of the most promising methods used to examine characteristic parameters relevant to the design of microring resonators. This method paves the way for experimental determination of the coupling coefficient and propagation loss. However, experimental verification of this technique by comparing the transmission characteristics obtained by reflectometry and those directly measured by an optical vector analyzer has not been carried out.Aim. To determine the parameters of microring resonators by optical reflectometry and to calculate on their basis the transmission characteristics of microring resonators. To compare the calculated transmission characteristics with those obtained experimentally using a high-resolution vector analyzer.Materials and methods. The characteristic parameters of silicon-on-insulator microring resonators were investigated using an ultra-high resolution reflectometer. An original algorithm was employed to derive the characteristic parameters of microring resonators from reflectograms. An optical vector analyzer was used to study the transmission characteristics of microring resonators. Numerical modeling of transmission characteristics considering the obtained parameters was carried out according an analytical approach based on partial wave analysis.Results. The obtained values of the power coupling coefficient κ = 0.167 and propagation losses α = 3.25 dB/cm were used for numerical simulation of the transmission characteristics of a microring resonator. These characteristics were found to agree well with those obtained experimentally. The free spectral range of 88.8 GHz and Q-factor of 45 000 were determined.Conclusion. An experimental study of the characteristic parameters of silicon-on-insulator microring resonators was conducted using an optical backscatter reflectometer. The performed comparison of the experimental and theoretical transmission characteristics showed good agreement, which indicates the high accuracy of the determined resonator parameters and, as a result, the relevance of the described method.

Thermo-Visco-Elastometry of RF-Wave-Heated and Ablated Flesh Tissues Containing Au Nanoparticles.

We report non-contact laser-based Brillouin light-scattering (BLS) spectroscopy measurements of the viscoelastic properties of hyperthermally radiofrequency (RF)-heated and ablated bovine liver and chicken flesh tissues with embedded gold nanoparticles (AuNPs). The spatial lateral profile of the local surface temperature in the flesh samples during their hyperthermia was measured through optical backscattering reflectometry (OBR) using Mg-silica-NP-doped sensing fibers distributed with an RF applicator and correlated with viscoelastic variations in heat-affected and ablated tissues. Substantial changes in the tissue stiffness after heating and ablation were directly related to their heat-induced structural modifications. The main proteins responsible for muscle elasticity were denatured and irreversibly aggregated during the RF ablation. At T > 100 °C, the proteins constituting the flesh further shrank and became disorganized, leading to substantial plastic deformation of biotissues. Their uniform destruction with larger thermal lesions and a more viscoelastic network was attained via AuNP-mediated RF hyperthermal ablation. The results demonstrated here pave the way for simultaneous real-time hybrid optical sensing of viscoelasticity and local temperature in biotissues during their denaturation and gelation during hyperthermia for future applications that involve mechanical- and thermal-property-controlled theranostics.

Distributed fibre optic monitoring of mode I fatigue crack propagation in adhesive bonded joints and comparison with digital image correlation

The feasibility of applying Optical Backscatter Reflectometry as a backface strain monitoring method for bonded joints subjected to mode I fatigue crack propagation was studied. Visual evaluation and Digital Image Correlation methods were applied to track the crack-tip position and the onset of plasticisation in the adhesive, respectively. The methods were compared to understand the relationship between the changes in the optical fibre measurements and the crack propagation. The absolute maximum strain values gave important information about the crack propagation stage (stable or high velocity) within the adhesive and fast-rate crack propagation, which resulted in a sudden increase in strain values. Finally, the strain peak position was found to be a valuable indicator of crack tip position.

Tunable distributed sensing performance in Ca-based nanoparticle-doped optical fibers

Rayleigh scattering enhanced nanoparticle-doped optical fibers is a technology very promising for distributed sensing applications, however, it remains largely unexplored. This work demonstrates for the first time the possibility of tuning Rayleigh scattering and optical losses in Ca-based nanoparticle-doped silica optical fibers by controlling the kinetics of the re-nucleation process that nanoparticles undergo during fiber drawing by controlling preform feed, drawing speed and temperature. A 3D study by SEM, FIB-SEM and optical backscatter reflectometry (OBR) reveals an early-time kinetics at 1870 °C, with tunable Rayleigh scattering enhancement 43.2–47.4 dB, regarding a long-haul single mode fiber, SMF-28, and associated sensing lengths of 3–5.5 m. At 2065 °C, kinetics is slower and nanoparticle dissolution is favored. Consequently, enhanced scattering values of 24.9–26.9 dB/m and sensing lengths of 135–250 m are attained. Finally, thermal stability above 500 °C and tunable distributed temperature sensitivity are proved, from 18.6 pm/°C to 23.9 pm/°C, ∼1.9–2.4 times larger than in a SMF-28. These results show the promising future of Rayleigh scattering enhanced nanoparticle-doped optical fibers for distributed sensing.

Distributed sensing based real‐time process monitoring of shape memory polymer components

AbstractShape memory polymer (SMP) materials have the capacity to undergo large deformations imposed by mechanical loading, hold a temporary shape, and then recover their original shape upon exposure to a particular external stimulus. The fiber reinforced shape memory polymer composites (SMPCs) with enhanced structural performances give a boost to breakthrough technologies for large‐scale engineering applications. This article presents a novel technique for distributed optical fiber sensor (DOFS) embedded SMPCs intended for real‐time process monitoring of large‐scale engineering applications such as deployable space structures. Herein a carbon fiber reinforced SMPC was tested under a three‐point flexural shape memory process and the DOFS data were acquired through optical backscatter reflectometry. Experiments were conducted in a temperature controlled thermal chamber coupled with a 10 kN electromechanical testing system. DOFSs offered unique advantages for spatially distributed dynamic temperature and strain measurements during the shape memory process. Compared to the standard test method dynamic mechanical analysis, larger samples can be tested effectively by using a single DOFS with large strain levels and shape complexity. The proposed technique demonstrated the ability of embedded DOFSs for in‐situ shape memory characterization such as shape fixity ratio, shape recovery ratio and recovery rate. This technique will eliminate the challenges hindering the process monitoring and performance evaluation of large SMPC components operating in their real working environments.

Green-Synthesized Silver Nanoparticle-Assisted Radiofrequency Ablation for Improved Thermal Treatment Distribution.

Thermal ablation therapy is known as an advantageous alternative to surgery allowing the treatment of multiple tumors located in hard-to-reach locations or treating patients with medical conditions that are not compatible with surgery. Appropriate heat propagation and precise control over the heat propagation is considered a weak point of thermal ablation therapy. In this work, silver nanoparticles (AgNPs) are used to improve the heat propagation properties during the thermal ablation procedure. Green-synthesized silver nanoparticles offer several attractive features, such as excellent thermal conductivity, biocompatibility, and antimicrobial activity. A distributed multiplexed fiber optic sensing system is used to monitor precisely the temperature change during nanoparticle-assisted radiofrequency ablation. An array of six MgO-based nanoparticles doped optical fibers spliced to single-mode fibers allowed us to obtain the two-dimensional thermal maps in a real time employing optical backscattering reflectometry at 2 mm resolution and 120 sensing points. The silver nanoparticles at 5, 10, and 20 mg/mL were employed to investigate their heating effects at several positions on the tissue regarding the active electrode. In addition, the pristine tissue and tissue treated with agarose solution were also tested for reference purposes. The results demonstrated that silver nanoparticles could increase the temperature during thermal therapies by propagating the heat. The highest temperature increase was obtained for 5 mg/mL silver nanoparticles introduced to the area close to the electrode with a 102% increase of the ablated area compared to the pristine tissue.

Comparison of DOFS Attachment Methods for Time-Dependent Strain Sensing.

Structural health monitoring (SHM) is a challenge for many industries. Over the last decade, novel strain monitoring methods using optical fibers have been implemented for SHM in aerospace, energy storage, marine, and civil engineering structures. However, the practical attachment of optical fibers (OFs) to the component is still problematic. While monitoring, the amount of substrate strain lost by the OF attachment is often unclear, and difficult to predict under long-term loads. This investigation clarifies how different attachment methods perform under time-dependent loading. Optical fibers are attached on metal, thermoset composite, and thermoplastic substrates for distributed strain sensing. Strains along distributed optical fiber sensors (DOFS) are measured by optical backscatter reflectometry (OBR) and compared to contact extensometer strains under tensile creep loading. The quality of the bondline and its influence on the strain transfer is analyzed. Residual strains and strain fluctuations along the sensor fiber are correlated to the fiber attachment method. Results show that a machine-controlled attachment process (such as in situ 3-D printing) holds great promise for the future as it achieves a highly uniform bondline and provides accurate strain measurements.

Experimental analysis of mode I crack propagation in adhesively bonded joints by optical backscatter reflectometry and comparison with digital image correlation

The relationship between the response of backface strain distributed sensing by Optical Backscatter Reflectometry and the damage in the adhesive was studied using double cantilever beam specimens. Digital Image Correlation and visual inspection provided information about the crack-tip position and the extension of the cohesive process zone. The comparison between the features of the backface strain pattern and the position and size of the cohesive zone led to the conclusion that, for the studied adhesive, backface distributed sensing allows for the onset of plastic deformations ahead of the crack-tip to be identified, opening new perspectives for fatigue crack monitoring and in-service measurements.

Graphical Optimization of Spectral Shift Reconstructions for Optical Backscatter Reflectometry.

Optical backscatter reflectometry (OBR) is an interferometric technique that can be used to measure local changes in temperature and mechanical strain based on spectral analyses of backscattered light from a singlemode optical fiber. The technique uses Fourier analyses to resolve spectra resulting from reflections occurring over a discrete region along the fiber. These spectra are cross-correlated with reference spectra to calculate the relative spectral shifts between measurements. The maximum of the cross-correlated spectra—termed quality—is a metric that quantifies the degree of correlation between the two measurements. Recently, this quality metric was incorporated into an adaptive algorithm to (1) selectively vary the reference measurement until the quality exceeds a predefined threshold and (2) calculate incremental spectral shifts that can be summed to determine the spectral shift relative to the initial reference. Using a graphical (network) framework, this effort demonstrated the optimal reconstruction of distributed OBR measurements for all sensing locations using a maximum spanning tree (MST). By allowing the reference to vary as a function of both time and sensing location, the MST and other adaptive algorithms could resolve spectral shifts at some locations, even if others can no longer be resolved.

Fatigue crack growth analysis in composite bonded joints by back face distributed strain sensing and comparison with X-ray microtomography

Fatigue crack growth in composite, single lap bonded joints is analysed by back face distributed strain sensing, using optical backscatter reflectometry. Crack growth is inferred from the back-face strain profile measured with high spatial resolution along optical fibres bonded on the joints. The indications about the position of the crack front are compared with micro computed tomography scans conducted on specimens at suitable interruptions of the fatigue tests. By the proposed technique, crack initiation can be clearly detected, and measurements of crack growth are in good agreement with observations, with decreasing error with increasing crack length.

Load estimation and vibration monitoring of scale model wind turbine blades through optical fiber sensors

Experimental activities on wind turbine models allow to speed up their design as well as the development of robust and effective control algorithms. Intending to have large information on load distribution on the blades, this work presents an experimental setup of a model wind turbine blade instrumented with two different types of optical fiber sensors (FOS). The first one is a traditional chain of Fiber Bragg Grating sensors, able to measure a large number of strain values; the second is based on Optical Backscatter Reflectometry (OBR), able to provide a continuous strain measurement. The experimental setup is calibrated to estimate load distribution along the blade and the two technologies are compared. The results of the experimental campaign suggest that optical fiber sensors could represent an interesting solution for real-time continuous load monitoring purposes.

Temperature compensation of the fiber-optic based system for the shape reconstruction of a minimally invasive surgical needle

This paper presents the methodology for temperature compensation of a system for shape reconstruction of a minimally invasive surgical needle. The system is based on four optical fibers glued along the needle at 90∘ from each other and connected to the optical backscattering reflectometry interrogator. The interrogator measures backscattered light from four fibers, which shifts as a response to temperature or strain variations. During minimally invasive surgery the fibers sense both the strain change (due to the needle bending) and the temperature change (due to the difference between the temperature of the environment and the human body). Shape reconstruction is based on the strain measurements, so the temperature readings need to be compensated. The methodology of compensation is based on the two pairs of opposite fibers, which measure the same temperature change and opposite strain. The spectral shifts of the opposite fibers are added to find only the temperature component and the result is subtracted from the whole spectral shift to find the strain change detected by each fiber. This method has been validated by repeated constant insertion into a temperature-varying phantom. The algorithm has succeeded in the extraction of the strain component, which found to be the same in all trials despite the changing temperature.

Picomolar detection of thrombin with fiber-optic ball resonator sensor using optical backscatter reflectometry

A ball resonator, positioned on the tip of an optical fiber, has been developed as a biosensor for the prototypic detection of thrombin. The device was fabricated with a fast and repeatable CO2 laser splicing method, followed by gold-sputtering and functionalization for the measurement of various protein concentrations. The ball resonator acts as a weak interferometer with a return loss below − 50 dB, and it is interrogated with an optical backscatter reflectometer measuring the reflection spectrum. We report here a sample presenting high sensitivity (1273.74 nm/RIU, RIU = refractive index units), which allows protein detection in the range 0.4–100 pM, with a limit of detection of 1.56 pM in logarithmic response.

Modelling of light scattering by gold nanoparticles at optical fibre interfaces

Optical fibre backscatter reflectometry is an important technique for Structural Health Monitoring (SHM). In recent years, increasing the intensity of backscattered light in backscatter reflectometry has shown the advantage of improving the signal detection in shape sensing and temperature detection due to the increase of signal to noise ratio and this approach could potentially be used to improve the performance of an SHM system. Doping nanoparticles (NPs) is a method to increase the intensity of backscattered light in distributed fibre optic sensing. The increased intensity of light backscattered by the NPs needs to be investigated to design suitable optical sensing fibres with NPs for backscatter reflectometry. In this work NPs were added to refractive index matching liquid and tested with commercial NP suspensions experimentally between the tips of two optical fibres. An estimate of the intensity of backscattered light from the NPs in this structure was performed by simulation to give a better understanding of the expected levels of intensities of scattered light from NPs in this distributed fibre optic sensing configuration. We present analytical models based on Mie theory and the Monte Carlo Method. Simulated results are presented, for a broad bandwidth Gaussian spectra shape incident light with a central wavelength around 1550 nm, to match the experimental conditions in this work. The novelty is in developing this model for scattered light by NPs at optical fibre interfaces and the evaluation of the possibility of detection by the calculated scattered intensity levels.

Distributed X-Ray Dosimetry With Optical Fibers by Optical Frequency Domain Interferometry

This article reports on the first demonstration of in situ , real-time dosimetry realized with an enhanced backscattering optical fiber, and a high-resolution optical backscattering reflectometry measurement. This work is devised to overcome the current problems in monitoring radiotherapy treatments, in particular, the difficult evaluation of not only the actual X-ray dose that is accumulated on the target volume but also the distribution profile of the ionizing radiation beam. Overall, the research aims at developing a dose sensor with the most demanding features of small form factor, spatial profiling, and remote interrogation. The experiments have been conducted by evaluating the spatial profile of radiation-induced spectral shift of the Rayleigh backscattering along an optical fiber exposed to X-rays. The sensing element is a section of specialty optical fiber whose Rayleigh backscattering signature changes under ionizing radiation. The specialty fiber is designed to exhibit an enhanced backscattering, in order to overcome the poor sensitivity to radiation of standard optical fibers that are normally, used in telecommunications. The enhanced sensitivity is achieved by doping the core with either aluminum or magnesium nanoparticles, and two different fibers have been fabricated and tested. The experimental results show the capability of real time detection of the radiation profile from high-dose rates (700 Gy/min) to low-dose rates (2 Gy/min). Moreover, different sensing mechanisms and responses to high- and low-dose rates are evidenced. A comparison with a quasi-distributed sensing system based on an array of fiber Bragg gratings (FBGs) is discussed, highlighting the superior performance of the backscattering approach in terms of sensitivity and spatial resolution, whereas the array of FBGs exhibits an advantage in terms of sampling speed.