Optical Angle Research Articles

Degradation of Organic Dye Congo Red by Heterogeneous Solar Photocatalysis with Bi2S3, Bi2S3/TiO2, and Bi2S3/ZnO Thin Films

In this work, bismuth sulfide (Bi2S3) thin films were deposited by a chemical bath deposition (CBD) technique (called soft chemistry), while titanium dioxide (TiO2) nanoparticles were synthesized by sol–gel and zinc oxide (ZnO) nanoparticles were extracted from alkaline batteries. The resulting nanoparticles were then deposited on the Bi2S3 thin films by spin coating at 1000 rpm for 60 s each layer to create heterojunctions of Bi2S3/ZnO and Bi2S3/TiO2. These materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and energy dispersive X-ray spectroscopy (EDX). The optical and contact angle analyses were undertaken by UV–Vis spectroscopy and a contact microscopy angle meter, respectively. The calculated band gap values were found to be between 1.9 eV and 2.45 eV. The Bi2S3 presented an orthorhombic structure, the TiO2 nanoparticles presented an anatase structure, and the ZnO nanoparticles presented a wurtzite hexagonal crystal structure. Furthermore, heterogeneous solar photocatalysis was performed using the Bi2S3, Bi2S3/ZnO, and Bi2S3/TiO2 thin film combinations, which resulted in the degradation of Congo red increasing from 8.89% to 30.80% after a 30 min exposure to sunlight.

A Large-Scan-Range Electrothermal Micromirror Integrated with Thermal Convection-Based Position Sensors.

This paper presents the design, simulation, fabrication, and characterization of a novel large-scan-range electrothermal micromirror integrated with a pair of position sensors. Note that the micromirror and the sensors can be manufactured within a single MEMS process flow. Thanks to the precise control of the fabrication of the grid-based large-size Al/SiO2 bimorph actuators, the maximum piston displacement and optical scan angle of the micromirror reach 370 μm and 36° at only 6 Vdc, respectively. Furthermore, the working principle of the sensors is deeply investigated, where the motion of the micromirror is reflected by monitoring the temperature variation-induced resistance change of the thermistors on the substrate during the synchronous movement of the mirror plate and the heaters. The results show that the full-range motion of the micromirror can be recognized by the sensors with sensitivities of 0.3 mV/μm in the piston displacement sensing and 2.1 mV/° in the tip-tilt sensing, respectively. The demonstrated large-scan-range micromirror that can be monitored by position sensors has a promising prospect for the MEMS Fourier transform spectrometers (FTS) systems.

Determination of the polarization of Xe nuclear spin using transverse and longitudinal Rb in-situ magnetometers in NMR co-magnetometers

NMR co-magnetometers, as novel atomic sensors, can measure the angular velocity information in inertial measurements by detecting the spin precession of Xe nuclei. The Xe polarization plays a crucial role in the sensing unit of co-magnetometers, as it enhances the signal-to-noise ratio (SNR) and sensitivity of NMR sensors. Here we elucidated the Rabi dynamics of Xe nuclear spin and demonstrated two methods to determine the Xe polarization based on the classical Bloch equations. By detecting the optical rotation angle signal, we acquired the amplitude and the phase variations information in two methods, respectively. The transverse magnetometer relies on the amplitude of the free induction decay (FID) signal and applies a short pulse to flip the Xe fields into the transverse plane, enabling precise measurements. On the other hand, the longitudinal magnetometer offers an intuitive approach to measuring the demodulated phase variations by capturing the repetitive flips of longitudinal Xe fields. This paper discusses the advantages and disadvantages of both proposed methods, with the aim of enhancing the accuracy and authenticity of nuclear spin polarization measurements for noble gas atoms in atomic sensors.

Passively Broadband Tunable Dual Circular Dichroism via Bound States in the Continuum in Topological Chiral Metasurface.

Dynamic control for a strong circular dichroism (CD) response is essential in engineering applications such as polarization manipulation, sensing, and imaging. Here, we propose and experimentally demonstrate a broadband tunable dual CD response via bound states in the continuum (BICs) in two-dimensional topologically protected metasurfaces composed of all-dielectric Si chiral grating structures that generate a pair of mixed and degenerated BIC mode and circular dichroic mode (CDM) as an additional degree of freedom in CD manipulation. It is found that a singular CD peak of nearly 100% at 1.6 μm can be achieved by CDM when BIC is hidden under normal incidence, while the CD peak can be split into two in which peak wavelengths can be precisely and linearly tuned over a bandwidth of 180 nm by the incident angle when the BIC mode is excited under oblique incidence. Additionally, dynamic modulation of output polarization states from linear to circular can be arbitrarily achieved at the split CD peaks by controlling the incident angle when asymmetry perturbations on chiral gratings are introduced due to the decoupling of various polarization states at Γ point by BIC to different positions in K space. The proposed chiral grating metasurface exhibits unique angle-sensitive tunable CD spectral characteristics, making it ideal for hyperspectral and spin-selective wavefront shaping, and holds significant promise in various applications such as optical security, angle sensors, chiral lasers, nonlinear filters, and other active chiral optical devices.

Thermal and Mechanical Properties of Bio‐Based Polyamide 56/6 Filled with Talc

AbstractPolyamide composites with varying filler concentrations are prepared using the hot melt extrusion method, employing polyamide 56/6 (PA56/6) and modified talc as fillers. Initially, the thermal characteristics of PA56/6 composites (PA56/6‐talc) are examined through thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC), encompassing parameters such as melting temperature, crystallinity, and decomposition temperature. The hydrophilicity and barrier properties of PA56/6‐talc are assessed using an optical contact angle meter, a water vapor transmission rate tester, and an oxygen transmission rate tester. Furthermore, the mechanical properties of PA56/6‐talc are also scrutinized. The results indicate that PA56/6 exhibits superior hydrophobic, barrier, and mechanical properties, thereby demonstrating its immense potential in garment fabrics and packaging materials.

IXPE observation of PKS 2155-304 reveals the most highly polarized blazar

We report the X-ray polarization properties of the high-synchrotron-peaked (HSP) blazar PKS 2155$-$304 based on observations with the Imaging X-ray Polarimetry Explorer (IXPE). We observed the source between Oct 27 and Nov 7, 2023. We also conducted an extensive contemporaneous multiwavelength (MW) campaign. We find that during the first half ($T_1$) of the IXPE pointing, the source exhibited the highest X-ray polarization degree detected for an HSP blazar thus far, (30.7pm 2.0)<!PCT!>; this dropped to (15.3pm 2.1)<!PCT!> during the second half ($T_2$). The X-ray polarization angle remained stable during the IXPE pointing at 129.4 and 125.4 during $T_1$ and $T_2$, respectively. Meanwhile, the optical polarization degree remained stable during the IXPE pointing, with average host-galaxy-corrected values of (4.3pm 0.7)<!PCT!> and (3.8pm 0.9)<!PCT!> during the $T_1$ and $T_2$, respectively. During the IXPE pointing, the optical polarization angle changed achromatically from sim 140 to sim 90 and back to sim 130 Despite several attempts, we only detected (99.7<!PCT!> conf.) the radio polarization once (during $T_2$, at 225.5 GHz): with degree (1.7pm 0.4)<!PCT!> and angle 112.5 The direction of the broad pc-scale jet is rather ambiguous and has been found to point to the east and south at different epochs; however, on larger scales (> 1.5 pc) the jet points toward the southeast (sim 135 similarly to all of the MW polarization angles. Moreover, the X-ray-to-optical polarization degree ratios of sim 7 and sim 4 during $T_1$ and $T_2$, respectively, are similar to previous IXPE results for several HSP blazars. These findings, combined with the lack of correlation of temporal variability between the MW polarization properties, agree with an energy-stratified shock-acceleration scenario in HSP blazars.

Design of an Electromagnetic Micro Mirror Driving System for LiDAR.

Electromagnetic micro mirrors are in great demand for light detection and ranging (LiDAR) applications due to their light weight and low power consumption. The driven frequency of electromagnetic micro mirrors is very important to their performance and consumption. An electromagnetic micro mirror system is proposed in this paper. The model of the system was composed of a micro mirror, an integrated piezoresistive (PR) sensor, and a driving circuit was developed. The twisting angle of the mirror edge was monitored by an integrated PR sensor, which provides frequency feedback signals, and the PR sensor has good sensitivity and linearity in testing, with a maximum of 24.45 mV/deg. Stable sinusoidal voltage excitation and frequency tracking was realized via a phase-locked loop (PLL) in the driving circuit, with a frequency error within 10 Hz. Compared with other high-cost solutions using PLL circuits, it has greater advantages in power consumption, cost, and occupied area. The mechanical and piezoresistive properties of micro mirrors were performed in ANSYS 19.2 software. The behavior-level models of devices, circuits, and systems were validated by MATLAB R2023a Simulink, which contributes to the research on the large-angle deflection and low-power-consumption drive of the electromagnetic micro mirror. The maximum optical scan angle reached 37.6° at 4 kHz in the behavior-level model of the micro mirror.

Research on the Measurement System and Remote Calibration Technology of a Dual Linear Array Camera

Abstract In order to accurately measure the flight trajectory of the projectile in a long-distance target range, it is important to establish a vertical target measurement system with a two-line array camera at several positions along the range. In the present work, a calibration system using dual theodolites is proposed to calibrate the vertical target measurement system of a dual linear array camera at different positions along a long target range. The present study investigates the principle of intersection measurement in the vertical target measurement system with a double linear array camera and presents the projectile’s target coordinate measurement formula. The calibration method of the measurement system is developed based on an analysis of the parameters in the projectile coordinate measurement formula. The calibration method only requires calibration of the camera’s distortion coefficient, the optical axis angle, and the principal point, ensuring a simplified and expedited calibration process. After calibration, the vertical target measurement system with a 3 m × 3 m measurement area is simulated and analyzed, yielding an error distribution diagram and identifying the factors that influence the measurement accuracy of the projectile’s target coordinates.

Dielectric elastomer-driven liquid prism enabling two-dimensional beam control

In this paper, a dielectric elastomer (DE)-driven liquid prism enabling two-dimensional beam control is proposed. The proposed liquid prism consists of a flexible driver and a liquid cavity. The glass plate is driven by DE to change the tilt angle of the liquid-solid interface for beam steering and field of view (FOV) tuning. The maximum optical deflection angle of 8.13° and response time of 76.77 ms were measured, the variable FOV capability was also verified. The proposed liquid prism can be used in beam modulation, microscope systems.

Negative reflection and total internal reflection at the internal surface of lithium niobate crystal

In this paper we analytically find out the expression for the wave vector and Poynting vector in the reflection domain for negative uniaxial material. We investigate the impact of the optical axis rotation and incident angle on the wave vector and Poynting vector reflected from the internal surface of lithium niobate crystal when the light is propagating from the denser anisotropic medium to the rarer isotropic medium. We derive the Brewster angle condition and discuss the walk-off between TE and TM polarized light. We explore where the wave vector and Poynting vector are parallel after reflection. In further analysis, we look into the phase differences between ordinary and extraordinary reflected light after total internal reflection from the internal surface of lithium niobate crystal. The necessary conditions for linear polarization and circular polarization have been established. The impact of optical axis orientation is also taken into consideration. The refractive index for the isotropic material for the desired polarization response has been found as 2.18, 2.1, and 2.03 at 632 nm, 1550 nm, and 3500 nm, respectively.

A new fabrication method for enhancing the yield of linear micromirror arrays assisted by temporary anchors

As one of the most common spatial light modulators, linear micromirror arrays (MMAs) based on microelectromechanical system (MEMS) processes are currently utilized in many fields. However, two crucial challenges exist in the fabrication of such devices: the adhesion of silicon microstructures caused by anodic bonding and the destruction of the suspended silicon film due to residual stress. To solve these issues, an innovative processing method assisted by temporary anchors is presented. This approach effectively reduces the span of silicon microstructures and improves the Euler buckling limit of the silicon film. Importantly, these temporary anchors are strategically placed within the primary etching areas, enabling easy removal without additional processing steps. As a result, we successfully achieved wafer-level, high-yield manufacturing of linear MMAs with a filling factor as high as 95.1%. Demonstrating superior capabilities to those of original MMAs, our enhanced version boasts a total of 60 linear micromirror elements, each featuring a length-to-width ratio of 52.6, and the entire optical aperture measures 5 mm × 6 mm. The linear MMA exhibits an optical deflection angle of 20.4° at 110 Vdc while maintaining exceptional deflection flatness and uniformity. This study offers a viable approach for the design and fabrication of thin-film MEMS devices with high yields, and the proposed MMA is promising as a replacement for digital micromirror devices (DMDs, by TI Corp.) in fields such as spectral imaging and optical communication.

Ultra-sensitive measurement of small optical rotation angles using quantum entanglement based on a quasi-Wollaston prism beam splitter

The measurement of optical rotation is fundamental to optical atomic magnetometry. Ultra-high sensitivity has been achieved by employing a quasi-Wollaston prism as the beam splitter within a quantum entanglement state, complemented by synchronous detection. Initially, we designed a quasi-Wollaston prism and intentionally rotated the crystal axis of the exit prism element by a specific bias angle. A linearly polarized light beam, incident upon this prism, is divided into three beams, with the intensity of each beam correlated through quantum entanglement. Subsequently, we formulated the equations for optical rotation angles by synchronously detecting the intensities of these beams, distinguishing between differential and reference signals. Theoretical analysis indicates that the measurement uncertainty for optical rotation angles, when using quantum entanglement, exceeds the conventional photon shot noise limit. Moreover, we have experimentally validated the effectiveness of our method. In DC mode, the experimental results reveal that the measurement uncertainty for optical rotation angles is 4.7 × 10−9 rad, implying a sensitivity of 4.7 × 10−10 rad/Hz1/2 for each 0.01 s measurement duration. In light intensity modulation mode, the uncertainty is 48.9 × 10−9 rad, indicating a sensitivity of 4.89 × 10−9 rad/Hz1/2 per 0.01 s measurement duration. This study presents a novel approach for measuring small optical rotation angles with unprecedentedly low uncertainty and high sensitivity, potentially playing a pivotal role in advancing all-optical atomic magnetometers and magneto-optical effect research.

Magnetic field density concentrated permanent magnet structure for electromagnetic MEMS scanning mirror

The study investigates the inadequacy of driving torque in large-diameter Micro-electro Mechanical Systems Electromagnetic Scanning Mirrors (MEMS-ESM) and introduces fresh insights into the power efficiency of traditional MEMS-ESM devices. A novel permanent magnet structure (PMS) and driving principle are devised, drawing upon the phenomenon of concentrated magnetic field density and a custom-designed PMS inner profile. In comparison to L-shaped and I-shaped PMSs, the proposed PMS delivers up to 3.48 times and 3.76 times greater driving torque within the same form factor. Moreover, the optimized proposed PMS has been experimentally proven to reduce power consumption by 53.3% and 81.4% and reduce total driving current by 31.3% and 55.0%, making it the sole solution that conforms to the safe current range. Additionally, the research analyzes the impact of variations in the optical scanning angle on the optimal PMS design. It is noteworthy that the proposed PMS enables the substitution of L-type and I-type PMSs with smaller package sizes, all while preserving torque, thus promoting the miniaturization of MEMS-SM.

Design and analysis of polarization-insensitive molybdenum-based ultra-wideband solar energy absorber with wide-incident-angle

We introduce an ultra-wideband absorber with a molybdenum and Al2O3 multilayer structure for solar energy harvesting. The proposed structure could maintain its structural integrity at high temperatures thanks to the refractory materials used in its construction. Under normal incidence of optical waves, absorption of more than 90% is achieved throughout a broad range of wavelengths from 300 nm to approximately 3177 nm with a bandwidth of 2877 nm which covers ultraviolet, visible, and near-infrared spectral bands. The average absorption in that band is calculated to be 96.46%. The proposed design’s symmetrical characteristic makes the absorber insensitive to the polarization of the incident optical wave. Furthermore, throughout a broad range of optical wave angles of incidence for both transverse electric and transverse magnetic polarizations, the absorber supports absorptivity greater than 80%.

Cost-effective 3D-printed rotatable reflectors for two-dimensional beam steering

In this paper, we have developed a 2D optical scanning module comprising cascaded 3D-printed one-axis rotating mirrors with large areas (30×30mm2 for the X-direction scan and 60×25mm2 for the Y-direction scan). Each mirror device contains a square or rectangular silicon substrate coated with aluminum, serving as the mirror. A 3D-printed structure, including the mirror frame (with four embedded mini permanent magnets on the backside), torsion springs, and base, is combined with the mirror; two electromagnets are situated under the mirror as the actuation mechanism. We apply DC voltage to the electromagnets to create magnetic force. The electromagnets can interact with the permanent magnets to make the mirror rotate. The X scan of the 2D scanning module can achieve a static optical scan angle of ∼11.8deg at the -X corners, and the corresponding Y-scan angle is ∼4.5deg, both with 12 VDC. Moreover, we have observed a fan-shaped distortion, a phenomenon not thoroughly studied previously for combining two single-axis scan mirrors. Therefore, we also perform a simulation to establish and demonstrate a correlation between the simulation prediction and experimental results. The 2D scanning module can be a low-cost alternative to the expensive conventional galvanometer scanners, and it can be used to upgrade a rangefinder to a simplified LiDAR.

Insights into the broadband emission of the TeV blazar Mrk 501 during the first X-ray polarization measurements

Aims. We present the first multiwavelength study of Mrk 501 that contains simultaneous very-high-energy (VHE) γ-ray observations and X-ray polarization measurements from the Imaging X-ray Polarimetry Explorer (IXPE). Methods. We used radio-to-VHE data from a multiwavelength campaign carried out between March 1, 2022, and July 19, 2022 (MJD 59639 to MJD 59779). The observations were performed by MAGIC, Fermi-LAT, NuSTAR, Swift (XRT and UVOT), and several other instruments that cover the optical and radio bands to complement the IXPE pointings. We characterized the dynamics of the broadband emission around the X-ray polarization measurements through its multiband fractional variability and correlations, and compared changes observed in the polarization degree to changes seen in the broadband emission using a multi-zone leptonic scenario. Results. During the IXPE pointings, the VHE state is close to the average behavior, with a 0.2–1 TeV flux of 20%–50% of the emission of the Crab Nebula. Additionally, it shows low variability and a hint of correlation between VHE γ-rays and X-rays. Despite the average VHE activity, an extreme X-ray behavior is measured for the first two IXPE pointings, taken in March 2022 (MJD 59646 to 59648 and MJD 59665 to 59667), with a synchrotron peak frequency > 1 keV. For the third IXPE pointing, in July 2022 (MJD 59769 to 59772), the synchrotron peak shifts toward lower energies and the optical/X-ray polarization degrees drop. All three IXPE epochs show an atypically low Compton dominance in the γ-rays. The X-ray polarization is systematically higher than at lower energies, suggesting an energy stratification of the jet. While during the IXPE epochs the polarization angles in the X-ray, optical, and radio bands align well, we find a clear discrepancy in the optical and radio polarization angles in the middle of the campaign. Such results further support the hypothesis of an energy-stratified jet. We modeled broadband spectra taken simultaneous to the IXPE pointings, assuming a compact zone that dominates in the X-rays and the VHE band, and an extended zone stretching farther downstream in the jet that dominates the emission at lower energies. NuSTAR data allow us to precisely constrain the synchrotron peak and therefore the underlying electron distribution. The change between the different states observed in the three IXPE pointings can be explained by a change in the magnetization and/or the emission region size, which directly connects the shift in the synchrotron peak to lower energies with the drop in the polarization degree.

Stabilization of oil‐in‐water emulsion gels by pH‐induced electrostatic interactions between soybean protein isolate microgel particles and xanthan gum

AbstractIn this paper, a colloidal dispersion at different pH containing soybean protein isolate (SPI) microgel particles and xanthan gum (XG) was used as the aqueous phase to prepare O/W emulsion gels with soybean oil. Properties of SPI microgel particles were analyzed by particle size, Zeta‐potential, secondary structure, optical contact angle, dynamic interface tension, and SEM testing, respectively. Results showed that pH impact microgels particle size and Zeta‐potential and their emulsification properties. It turned out that only at pH 3, 6, 7, and 8 can construct emulsions successfully. Based on a comparison of microstructure and macroscopic properties, it was found that at pH 3, proteins and polysaccharides were oppositely charged, electrostatic attraction between them reduced proteins located at the interface, and was more likely to form larger droplets, resulting in a bimodal droplet distribution and larger sizes. Conversely, at the pH of 6, 7, and 8, respectively, emulsions exhibited a uniform droplet distribution and more solid‐like rheological properties due to the powerful electrostatic repulsion between SPI and XG. Also, emulsion gels co‐stabilized with proteins and polysaccharides under electrostatic repulsion conditions showed an ideal recovery ability. Overall, this work would be beneficial to the use of emulsion gels in fat substitute systems.

Integrating a Physical Model with Multi-Objective Optimization for the Design of Optical Angle Nano-Positioning Mechanism

In light of recent advancements in synchrotron radiation technology and nano-technology, there has been a marked increase in the need for ultra-precision nano-positioning mechanisms. This paper presents a method that integrates physical models with multi-objective optimization for developing an optical angle nano-positioning mechanism. We begin by examining the actual motion law of the mechanism, based on kinematic principles. The outcomes from this kinematic analysis facilitate a static analysis of the flexible hinge, identified as a critical component of the mechanism. Subsequently, we establish a dynamic model for the entire mechanism. By employing the physical model as a base and combining it with the optimization algorithm, we identify the optimal design parameters for the mechanism. The design achieves a resolution of 50 nrad and meets the specified requirements. The first-order inherent frequency of the mechanism is approximately 43.75 Hz. There is a discrepancy of 2.63% from the finite element modal analysis results and a 3.33% difference from the theoretical analysis results, validating the reliability of the design method proposed in this study.

Preparation and Corrosion Resistance of OMMT/EP Composite Coatings in Sulfur-Containing Sodium Aluminate Solution

Organic montmorillonite (OMMT) was prepared from Na-montmorillonite (MMT) by Hexadecylamine (HDA) modification. The composite material has good smoothness, acidity, and salt resistance. OMMT was characterized using small-angle X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy, and a video optical contact angle measuring instrument. The results showed that the layer spacing was enlarged from 1.44 nm to 2.87 nm after the modification, and the hydrophobicity performance was greatly improved. The organic modification of MMT was successful. The surface morphology, roughness, and anticorrosion properties of the organic montmorillonite/epoxy (OMMT/EP) composite coating were investigated and compared with those of the epoxy (EP) coating. The OMMT/EP composite coating had a flatter surface than the EP coating. The roughness was reduced from 65.5 nm to 10.3 nm. The electrochemical impedance spectroscopy showed that the composite coating’s thickness positively affected its anticorrosion performance, the corrosion current density (Icorr) decreased with the increase in thickness, and its maximum impedance was much larger than that of EP coating. The protection efficiency of the OMMT/EP composite coating was 77.90%, which is a significant improvement over the EP’s 31.27%. In addition, the corrosion resistance of the composite coating gradually decreased with increasing immersion time, but the change was insignificant.

Ultra‐Low‐Power Tunable Topological Photonic Filter on Hybrid Integrated Lithium Tantalite and Silicon Platform

AbstractIntegrated tunable optical filters are essential components in photonic signal processors, telecom systems, sensors, and quantum optical devices. Two of the most important features of a tunable filter are its dimensions and power consumption. Herein, the design and experimental validation of an on‐chip optical filter composed of a 1D topological photonic crystal cavity based on a hybrid integrated lithium tantalite‐silicon platform is presented. The strong optical confinement of the boundary state allows the fabrication of a tunable filter with an ultra‐compact size of 1.14 × 75 µm2 is demonstrated. Moreover, lithium tantalite has excellent electro‐optic properties and enables ultra‐low‐power wavelength tuning of the topological boundary state. The measured power consumption and tuning efficiency of the device are 0.0218 nW pm−1 and 6.64 pm V−1, respectively. The anisotropy of thin‐film lithium tantalite is verified by evaluating its tuning efficiency at different optical angles. The device can compensate for thermally induced refractive index changes ≈20 °C, exhibiting operational robustness. High‐speed transmission experiments confirm the stability of the developed tunable filter. This optical filter implements a topological structure with a compact size and can potentially be applied in on‐chip quantum optics, nonlinear optics, and optical sensing.