One part type, solventless acrylic adhesives containing divalent metal salts of dibasic acid mono(methacryloyloxypropyl) esters as one of the monomer components were prepared to investigate the effect of the metal carboxylate group on adhesive properties. The adhesives contained a succinate, maleate, phthalate, or hexahydrophthalate group. The metal in the metal carboxylate group was Ca, Mg or Zn. Adhesive strength was determined using nuts and bolts as adherends. The strength increased markedly with increase in the content of the metal carboxylate group for the succinate or maleate-containing systems. The influence of the metal species was clearly seen for the former systems. Chemical resistance, corrosivity, and adhesive to oily surfaces were also evaluated.