This article describes an experimental and straightforward technique towards the simultaneous estimation of temperature-dependent thermal conductivity and specific heat of metals. The thermal model is based on transient nonlinear one-dimensional heat conduction across a metallic sample, which is subject to a constant heat flux on the upper side, and insulated on the bottom side. The thermal analyses are performed in plates of 304 stainless steel and WC10Co cemented carbide. The Levenberg–Marquardt method is employed to provide the solution to an inverse heat conduction problem capable of simultaneously evaluating the temperature-dependent thermophysical properties using transient temperature measurements. Through sensitivity analysis, it is possible to obtain prior information about estimation feasibility and establish all experimental aspects. The imperfect contact at the heater-plate interface causes contact resistance effect, which is considered a reducing agent on heat flux. Beck's nonlinear function minimization technique is used to confirm the reliability of the inverse estimation technique by using the achieved outcomes to recover the heat flux imposed on the test plate. Furthermore, the statistical study into confidence bounds and comparison with literature reveal the robustness of the results. Finally, the accuracy of the developed approach is investigated through the analysis of the errors deriving from experimental and numerical procedures.
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