Microstructural Characterization Research Articles

Development of Functionally Graded HA-Al2O3-TiO2 Composite Coating on Ti Alloy: Microstructural Characterization, Nano-mechanical Properties, and Wear Behavior

Development of Functionally Graded HA-Al2O3-TiO2 Composite Coating on Ti Alloy: Microstructural Characterization, Nano-mechanical Properties, and Wear Behavior

Effect of hole dimension on microstructure and properties of nano SiC reinforced Al7075 matrix using friction stir processing

This study examines the influence of hole diameter in friction stir processing (FSP) on the microstructure and mechanical properties of Al7075/nSiC nanocomposites. Experiments conducted with hole diameters of 2 mm, 3 mm, and 4 mm show that a 3 mm hole diameter results in the finest grain size (24.6 µm), highest tensile strength (290.34 MPa), and greatest microhardness (139.42HV). Microstructural characterization confirms optimal nanoparticle distribution and grain refinement at this diameter. These findings validate the hypothesis, indicating that a 3 mm hole diameter in FSP is critical for improving the mechanical performance of Al7075/nSiC composites. This study provides valuable insights for optimizing FSP parameters to develop advanced metal matrix composites.

Study on the Influence of Industrial Coke Oven Size on the Quality of Metallurgical Coke

The large-scale coke oven is a developing trend in coking technology, and the influence of the industrial coke oven size on the quality of metallurgical coke needs to be revealed. Under the same raw coals and blending ratios, metallurgical cokes were obtained from top-loading coke ovens with carbonization chamber heights of 6 and 7 m, respectively. The macroscopic quality and microstructure of the refined metallurgical cokes were comprehensively tested. The results showed that the conventional cold and thermal strength indexes of Coke-7m were better than those of Coke-6m. The comprehensive thermal strength at multiple temperatures further showed that the thermal strength advantage of Coke-7m was mainly manifested at low temperatures (1050 and 1100 °C) or a high temperature (1300 °C), where the solution-loss reaction mode of coke tended to be the “uniform reaction model” or “unreacted core model”. At medium temperatures, the solution-loss reaction mode tended to be the “gradient reaction model”, which had a greater destructive effect on the thermal strength of coke. At this time, the thermal strengths of the two cokes were close. Microstructure characterization revealed that industrial coke oven size mainly affected the carbon structure of coke but had little effect on pore structure. The advantage of Coke-7m regarding carbon structure is an important reason for its superior macroscopic quality compared to Coke-6m.

Mechanical properties improvement of titanium alloy and its grain boundary dislocation evolution mechanism by novel electroshock treatment

Titanium alloys are extensively utilized in the aerospace industry due to their exceptional strength and resistance to corrosion. However, litmited performance and high dispersion has always existed for the traditional manufacturing process. A novel Electroshock Treatment (EST) procedure proposed by author's team can synergistically improve the mechanical properties and its consistency of titanium alloys under limited temperature rise, but the relevant mechanism is not yet clear. In present work, the effects of various EST conditions on the mechanical characteristics were investigated by uniaxial tensile testing, and the effect mechanism was revealed using multi-scale microstructure characterization of titanium alloys, such as SEM, EBSD and TEM. The uniaxial tensile test results show that, compared with the sample without EST, the average elongation after fracture improved by 12.5%, the strength-plastic product improved by 16.1%, and the consistency of UTS and elongation after fracture improved by 63.4% and 57.1%, respectively, with a slight increase of tensile strength (30 MPa) after appropriate treatment (current density of 0.93 × 108A/m2, and pulse duration of 300 ms). The multi-scale microscopic characterization reveals a more uniform distribution of stress concentration in TC11 titanium alloy following the appropriate EST process. Besides, the entanglement of dislocations is reduced with some dislocations being annihilated. Especially, the remaining dislocations undergoing orderly rearrangement at grain boundaries after EST. The homogenization of local lattice distortion distribution and orderly rearrangement of dislocations at grain boundaries are the primary factors contributing to the comprehensive improvement in the mechanical properties and consistency of TC11 Titanium alloy.

Mechanical and microstructure characterisation of 2.5D C/C-SiC composites applied for the brake disc of high-speed train

Carbon fibre reinforced silicon carbide (C/C-SiC) composite materials have attracted increasing attention in brake system of high-speed trains, due to their low density, high specific strength, thermal stability, and frictional wear performance. This study aims to explore the mechanical properties of the 2.5D C/C-SiC composites, in order to characterise its potential application to the friction braking system of high-speed trains. To comprehensively evaluate the mechanical performance of the 2.5D C/C-SiC composites, the chemical vapor infiltration (CVI) method was adopted to prepare novel samples with high densification and low content of residual Si. The mechanical properties and failure mechanisms of the composites were investigated under various loading conditions, including tension, compression, bending, and shear tests. The experimental results indicated that the 2.5D C/C-SiC composites exhibited superior mechanical properties, with average in-plane tensile strength, compressive strength, bending strength, and interlaminar shear strength reaching 127.67 MPa, 326.92 MPa, 355.74 MPa, and 9.77 MPa, respectively, which are 2–8 times higher than the mechanical properties of C/C-SiC composites in existing publications. Under different loading conditions, the composites demonstrated characteristics of ductile fracture, pseudo-plastic compression fracture, pseudo-plastic bending fracture, and brittle shear fracture. Both high fibre content and the formation of SiC structure were advantageous for enhancing the load-bearing performance of C/C-SiC composites. The outstanding mechanical properties of the 2.5D C/C-SiC composite render the brake disc highly resistant to deformation and cracking under high stress, thereby enhancing its durability and establishing it as the ideal material for the next generation of high-speed train brake discs.

Microstructural characterization and creep deformation response of an Inconel-600/Inconel-625 welded joint obtained by oscillating GMAW process.

This investigation presents the microstructural characterization and creep failure mechanism of a dissimilar weld (DW) of Inconel 600 (IN600) and Inconel 625 (IN625) at a temperature of 675 °C and different stress levels. Optical microscopy (OM), scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), and Vickers microhardness test were used to characterize the welded joint, the creep rupture features, and microstructural characteristics of the DW respectively. The experimental results show that the crept samples consistently broke on the base material of the IN600 side and that the failure was mainly controlled by the plastic deformation of coarser austenitic grains, dynamic recrystallization, and the coalescence and growth of microcracks that resulted from the evolution of the Cr-rich carbides along the grain boundaries that conducted to a transgranular fracture mode.

Dynamic transition of internal oxides during high dew point heat treatment in Fe-2.4Mn-0.4Si-0.13 C alloy

The origin of the dynamic transition of internal oxides was clarified in Fe-2.4Mn-0.4Si-0.13C-based steel during decarburization annealing at 1073K. High dew point with H2 gas leads to the formation of deep decarburized ferrite layers containing grain boundary internal oxides. Microstructural characterization reveals the oxide transition from Mn2SiO4 to α-SiO2 at the tip of the internal oxidation layer and from α-SiO2 to Mn2SiO4 at the middle range of the internal oxidation layer. The dynamic transition between Mn2SiO4 and α-SiO2 is understood by the depletion in Mn contents and change of oxygen content, which change the normalized driving force of both oxides. The study gives a detailed mechanism of internal oxide formation and growth in multi-phase steel during high dew point annealing. Impact statementDuring high dew-point decarburization annealing, the fluctuation of Mn contents affects the driving force to form an internal oxide, resulting in the dynamic transition between Mn2SiO4 and α-SiO2.

Annealing characteristics and mechanism interpretation of high-performance swaged W-Y2O3 alloy

The evolution of the internal microstructure of tungsten (W) alloys during thermal mechanical processing and annealing is complex. This study employs systematic annealing experiments, tensile tests, and microstructural characterization to scientifically analyze a high-performance W-Y2O3 (WYO) alloy post-swaging. The aim is to gain a thorough understanding of the microstructural basis of the material's properties and to explore the relationship between these property changes and the annealing process. We quantify the trends of low-angle grain boundaries under various annealing temperatures, revealing their strong correlation with the ductility of W alloys. Annealing swaged WYO below the recrystallization temperature effectively enhances its mechanical properties. Findings not only provide scientific support for the further application and development of W alloys but also offer valuable insights into how mechanical and thermal treatment processes can optimize material properties.

Protective silicide coating fabricated on ductile VNbTa refractory complex concentrated alloy: Microstructure, high-temperature oxidation and wear behaviors

VNbTa refractory complex concentrated alloy (RCCA) possesses broad application prospects in a wide temperature window owing to its remarkable strength-ductility synergy and super rolling formability, whereas poor oxidation resistance will give rise to excessive wear above 800 ℃. In this contribution, we aim to fabricate a protective silicide coating on VNbTa RCCA for the purposes of enhancing high-temperature oxidation as well as wear resistance. Microstructural characterizations revealed that a uniform and intact coating was obtained under the optimized processing condition of pack cementation. The coating is mainly composed of single-phase (VNbTa)Si2, along with a thin M5Si3-type interdiffusion zone. Compared with bare alloy, the coated specimens exhibit remarkable oxidation resistance at 1000 ℃ due to the preferential formation of protective SiO2 scale. Meanwhile, the coated specimens maintain desirable wear resistance from 800 ℃ to 1000 ℃. The results of this study would offer a valuable reference to expedite the future engineering applications of RCCAs.

Corrosion Resistance of FeCrMnxAlCu High-Entropy Alloys in 0.5 M H2SO4 Solution

In this study, FeCrMnxAlCu high-entropy alloys with varying Mn contents (x = 2.0, 1.5, 1.0, 0.5, and 0) were prepared using a vacuum arc melting furnace. The phase structure and microstructure of the alloys before and after corrosion were characterized via X-ray diffraction, scanning electron microscopy, and energy-dispersive X-ray spectroscopy. The corrosion resistance of the alloys in a 0.5M H2SO4 solution was comprehensively evaluated through potentiodynamic polarization, electrochemical impedance spectroscopy, immersion tests, white light interferometry, and X-ray photoelectron spectroscopy. Microstructural characterization results revealed that the FeCrMnxAlCu high-entropy alloys exhibited mixed FCC and BCC phase structures and featured typical dendritic and interdendritic regions. Corrosion tests indicated that as the Mn content decreased, the corrosion resistance of the high-entropy alloys improved, and the corrosion type transitioned from dendritic to interdendritic. Among these alloys, the FeCrAlCu high-entropy alloy exhibited the highest corrosion resistance, with the highest positive corrosion potential (Ecorr = −0.11V), the lowest corrosion current density (Icorr = 1.02 × 10−5 A∙cm2), minimal corrosion depth, and the lowest corrosion rate (0.1592mm/y). After corrosion, a composite oxide protective film was formed on the alloy surface, effectively hindering further penetration of the H2SO4 solution and exhibiting excellent corrosion resistance.

Study on the effect of Sc and Zr addition on microstructure, mechanical property and fracture behavior of electron beam welded Be-Al alloys

Because of various excellent properties of low density, high specific strength and stiffness, high modulus, good thermal stability and corrosion-resistant, beryllium-aluminum (Be-Al) alloys have shown great potential to be used in nuclear industries. However, Be-Al alloys suffer from the bottlenecks of low solubility between Be and Al and the lack of effective technology for fabricating large-sized products. Herein, based on Sc and Zr addition, Be-Al-Sc-Zr alloys are successfully fabricated by conducting the electron beam welding (EBW) technology, and the effect of Sc and Zr addition on microstructure, mechanical property and fracture behavior of Be-Al-Sc-Zr alloys is studied. Microstructural characterizations show that both the EBWed Be-Al and Be-Al-Sc-Zr alloys exhibit two distinct zones of substrate zone (SZ) and fusion zone (FZ). Compared to grain size of the SZ and FZ in Be-Al alloys, grain sizes of these two zones in Be-Al-Sc-Zr alloys are significantly refined, thus leading to ultimate tensile strength (UTS) of the Be-Al-Sc-Zr alloys (~176MPa) approximately 150% higher than that of the Be-Al alloys (~118MPa). Besides, a newly generated third phase (TP), which is confirmed as Be13(Scx, Zr1-x), forms within Al phase in both SZ and FZ of the Be-Al-Sc-Zr alloys. Different from fracture behavior of Be-Al alloys that preferentially fractures within Al phase or near the Be/Al interface, fracture of the Be-Al-Sc-Zr alloys is prone to occur within Be phase. As revealed by the calculation results of finite element method (FEM), the underlying mechanism for different fracture behaviors mainly ascribes to that the reinforcement of the Al phase and the existence of the newly formed TP can greatly increases the internal stress and even causes stress concentration within Be phase of the Be-Al-Sc-Zr alloys. The present findings may provide more insights to the micro-alloying and deformation mechanism of Be-Al alloys that with enhanced mechanical properties.

Effect of cobalt on Microstructure and toughness properties of 9Cr-1.8W-0.4Ni-xCo weld metal

In this research, microstructural characterization and mechanical properties of 9%Cr, 0.4%Ni (including W and Mo) steel weld metal with alloyed cobalt were investigated. Due to their strong creep resistance, oxidation resistance, and low thermal expansion, 9%Cr steels are used in nuclear power plants, petrochemical industries, and fossil fuel-powered power plants that operate in high temperature conditions. In this context, weld metals comprising 0.5 %, 1 % and 1.5 % cobalt and cobalt-free weld metal were produced by SMAW (shielded metal arc welding) technique. Microstructure of the weld metals were characterized with optical microscope (OM), scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD). Also, XRD analysis was performed on the bulk samples and precipitated carbide/nitride phases extracted from the weld metals. In addition, differential scanning calorimetry (DSC) was used to determine the phase transformations. Thermo-Calc modeling study was also performed. Hardness, tensile and Charpy-V impact tests were carried out to determine the mechanical properties. The hardness did not change significantly when cobalt up to 1.5 % in the weld metal. However, with the increase of cobalt, the yield and tensile strength increased without affecting the elongation value too much. In the Charpy impact tests performed at different temperatures (−40 °C, −20 °C, +20 °C, +40 °C, +60 °C), the amount of cobalt increased toughness, especially at +40 and + 60oC temperatures. Ductile brittle transformation temperature (DBTT) of the weld metal with 1.5 % Co decreased from 29 °C to 15 °C compared to cobalt free weld metal. It is thought that this may be caused by the further separation of C, Cr and W from the matrix through forming precipitate by the cobalt effect. Besides the mechanical properties, microstructure was also affected by adding Co with inhibition of delta ferrite formation which decrease the toughness. Curie temperature increased with increasing cobalt content detected by DSC.

Microstructural and fatigue characterization of 316L stainless steel subjected to flow drilling and tapping: comparison with machined threads

Despite extensive research on the plastic deformation of materials to enhance their fatigue resistance, the influence of the flow tapping process on the fatigue resistance of drilled and tapped bars remains poorly understood. Herein, the fatigue performance of flow-drilled (friction-drilled) and flow-tapped 316L stainless steel bars was experimentally analyzed and compared with that of conventional material-shearing-based drilling and tapping operations. The effect of flow processes on the material properties was evaluated via microhardness tests and microstructural analyses. The results indicated that the hardness near the holes produced via flow forming was 62 % higher than that of the base metal. Moreover, grain refinement and plastic deformation were observed beneath the thread surfaces. Metallographic observations revealed the occurrence of craters and folds at the crest of the flow-formed threads. Following the ASTM F382-17 standard, four-point bending fatigue tests were performed at three stress amplitudes with a stress ratio of 0.1. No noteworthy differences were observed when the maximum bending moments applied were at 75 % and 60 % of the bending moment at yield. However, when the maximum bending moment applied was limited to 50 % of the bending moment at yield, the average fatigue life of the specimens with machined threads was longer than that of their flow-formed counterparts. Fractographic observations were used to identify the crack initiation regions and elucidate the underlying fracture mechanisms. For both types of specimens, failure originated at the crest of the first thread, beneath the surface of the maximum tensile stress. The flow-processed specimens exhibited secondary cracks at the root of the threads, where grain refinement also occurred. This study provides robust empirical evidence that using flow-forming processes to thread 316L stainless steel does not systematically improve the fatigue resistance of the material surrounding the holes. Furthermore, by optimizing the flow process and eliminating discontinuities, the threading process proposed herein could help improve the fatigue resistance of orthopedic implants.

Comparison and validation of stochastic microstructure characterization and reconstruction: Machine learning vs. deep learning methodologies

In the world of computational materials science, the knowledge of microstructure is vital in understanding the process-microstructure–property linkage across various length-scales. To circumvent costly experimental characterizations, typically, analyses on ensembles of 3D microstructures within a numerical framework are preferred. Utilizing a moment invariants-based physical descriptor, the current work quantifies the variations in the microstructural topology of 3D synthetic data of polycrystalline materials. For the first time, the validation of synthetic microstructures based on two unique AI-based reconstruction approaches was compared, providing valuable insights into the diverse characteristics of each methodology. Virtual 3D microstructure volumes of forged Ti-7Al and additively manufactured 316L stainless steel alloys were generated from 2D experimental data using two methods — Markov Random Field (MRF) and deep learning-based volumetric texture synthesis. Quantitative evaluation and validation of the reconstructed volumes were carried out with the aid of moment invariants by comparing local features associated with grain-level properties, such as grain size and shape. The normalized central moments previously employed to compare 2D grain topology were expanded to 3D. With the advent of various reconstruction algorithms, especially AI-based, the validation methodology outlined in this work can be adopted to evaluate the robustness of various 3D reconstruction frameworks as well as ensure spatial equivalency of the target microstructures.

Creep rupture properties of dissimilar welded joint of ferritic/martensitic P92 steel and Inconel 617 alloy

The dissimilar welded joint (DWJ) comprising P92 steel and Inconel 617 (IN617) is frequently utilized in advanced ultra-supercritical (AUSC) boilers. In present work the creep rupture behaviour, rupture mechanism and microstructure evolution of DWJ of P92 steel and IN617 with Ni-based ERNiCrCoMo-1 filler, were examined at 650 °C under the stress range of 120–200 MPa. The results of the creep test indicated that the location of creep rupture varied across different testing conditions, encompassing areas such as P92 base metal and the fine-grained heat-affected zone (FGHAZ). The creep tested specimens within the stress range of 180–200 MPa exhibited failure originating from P92 base metal, predominantly influenced by plastic deformation. The failure manifested in a transgranular mode, driven by the formation, growth, and eventually coalescence of microvoids. The creep tested specimens within the stress range of 120–150 MPa displayed the characteristic ofType IV failure, primarily attributed to matrix softening and the absence of adequate precipitates to pin the PAGBs. Microstructural characterization unveiled the presence of microvoids along the PAGBs, facilitating microvoid nucleation primarily owing to the existence of the coarse brittle carbide phase. The growth of these microvoids over a period of time during tertiary stage of creep which lead to their coalescence and the formation of microcracks, ultimately resulting in premature intergranular failure. The specimen creep exposed at 650 °C under the lower stress of 120 MPa exhibited higher creep rupture life for 432 h. The SEM/EDS study of the crept sample of 120 MPa is also confirmed the presence of intermetallic laves phases in regions near the fracture tip and in the heat-affected zones (HAZs). Although the creep tested specimens at 150 MPa and 120 MPa exhibited failure in the FGHAZ and their elemental SEM/EDS analysis confirmed the presence of an oxide layer and notch formation near the interface of P92 base metal and ErNiCrCoMo-1 filler weld. The FESEM study revealed the growth of the oxide layer in the notch region, and it also showed the presence of multiple cracks and microvoids in the oxide layer. The formation and propagation of the oxide notch mainly led to the interfacial failure. The crept specimens subjected to 180 MPa and 200 MPa did not exhibit any cracks or microvoids in HAZs. However, specimens that failed under applied stresses of 120 MPa and 150 MPa revealed the presence of a high density of microvoids in the FGHAZ, inter-critical heat-affected zone (ICHAZ), and in the region of the coarse-grained heat-affected zone (CGHAZ) adjacent to the interface attached with an oxide layer.

Microstructural and functional characterization of sintered fly ash

The utilization of industry by-products, such as fly ash, was investigated. However, the research results have yet to report the functional characteristics of fly ash. This paper deals with the processing, microstructure, and functional characterization of fly ash using a novel powder metallurgy method. The elemental composition, mineralogical phases, morphology phases, electrical and dielectric properties were determined by XRF, XRD, SEM, and impendence analyzer, respectively. The effect of additives on fly ash’s microstructure and functional properties was studied. As a result, sintered fly ash possesses better microstructure and dielectric properties as a function of frequency and temperature. It is suggested that sintered fly ash can be utilized for electronic packaging and EMI shielding applications.

Mechanical and Microstructural Characterization of a Nano-stabilized Sandy Soil

AbstractThis research investigates the potential of using nanoparticles, Poly Aluminum Silicate and Poly Calcium Silicate, and industrial by-products, Recycled Glass Powder (RGP) and Ground Granulated Ballast Furnace Slag (GGBS) to enhance the durability and strength of a sandy soil, particularly in wet or saturated conditions where water table is close to building foundations. The study aims to determine the optimal content and concentration of additives and assess their influence on the compressive strength and the failure strain. The optimal content and concentration of dry additives and alkaline solutions were determined. Uniaxial compressive strength tests were conducted on various stabilized geopolymers, considering factors such as alkaline activator type, nanoparticle type and percentage, and degree of saturation. Scanning electron microscopy images were taken and analyzed to verify geomechanical testing outcomes. Mixtures with nanomaterials exhibited greater strength than untreated soil, with some exhibiting up to a tenfold increase. GGBS-based samples displayed a twofold increase in strength with nanomaterial addition, while RGP-based samples experienced reduced strength. However, both nanomaterials addressed the durability concerns in wet conditions. The addition of 2% nanomaterials to GGBS-based mixtures led to significant strength gains, with some showing a 20% increase after saturation. This research indicated the potential of nanoparticles and industrial by-products in resolving a major concern regarding geopolymers which is the lack of durability in wet or saturated conditions. These findings have implications for eco-friendly geoconstruction materials and practices.

Effect of precipitation hardening on the microstructure, mechanical, and corrosion properties of additively manufactured A20X aluminum alloy

The effect of age hardening treatment on microstructure, tensile properties, and corrosion behavior of additively manufactured A20X alloy was investigated. Three single-step aging temperatures (150 °C, 175 °C, and 200 °C) and one double-step aging temperature (pre-aging at 165 °C followed by aging at 185 °C) along with varying heat treatment durations ranging from 30 min to 144 h, were studied systematically. Microstructural characterizations revealed that the co-existence of coherent/semi-coherent (Ω, θ′) and incoherent precipitates (θ) resulted in the maximum hardening effect (up to 30 % higher microhardness). This improved the yield strength at room and 150 °C by 33.4 % and 22.6 %, respectively. Double aging delivered the best combination of microstructure with fine grains and optimal precipitate assembly in a short duration (12–16 h). The heat-treated LPBF A20X showed higher ductility and similar mechanical properties compared to the cast A20X. However, optimal precipitate characteristics reduced the corrosion potential by 13–16 % due to a higher galvanic reaction. The highest corrosion potential (−0.622 V) was achieved in the solutionized state.

Investigation on the compressive strength of desulfurization gypsum binary cementitious materials with low energy consumption: the utilization enhancement of industrial wastes

Geopolymer, a new low carbon green cementing binder, has widely been used as an alternative to Ordinary Portland cement (OPC), which effectively reduces carbon emissions and industrial solid waste stockpiles on land, also improving solid waste utilization. To raise the utilization of sulphate solid waste and decrease energy consumption, desulphurization gypsum (DG)-based binary cementitious materials were synthesized, and the effects of DG dosage and alkali exciter components on the compressive strength of binary cementitious materials were investigated. In addition, the improvement mechanism of the mechanical properties of binary cementitious materials was revealed by microstructure characterization tools. The results prove that the optimum compressive strength of 52.5 ± 0.5MPa is achieved with a DG dosage of 20%, SiO2/Na2O of 1, water glass dosage of 10% and water-cement ratio of 0.5. Due to the continuous reaction of sulphate in DG with Ca2+ and reactive silicates/aluminosilicates during the curing process, the crystals of ettringite (AFt) are generated and filled the pores of binary cementitious materials and thus furtherly enhancing its compressive strength. And the gel products wrap the AFt that has been filled in the inter-vacancy space on the surface of aluminosilicates already formed at an earlier stage. In summary, ground granulated blast-furnace slag (GGBS) and DG work synergistically to reduce the negative effects of delayed AFt and increase the compressive strength of the geopolymer.

Enhancing the tribological characteristics of the biocompatible Ti-6Al-4 V alloy via heat treatment: An experimental analysis

The tribological behaviour of the Ti-6Al-4 V biocompatible alloy fabricated using laser powder bed fusion (LPBF) was experimentally investigated for prosthesis implants. Annealing heat treatment was executed to improve its tribological performance. The microstructure and microhardness characterization were performed using scanning electron microscope (SEM) and Vickers microhardness. The wear test was processed using a SS304 spherical ball in simulated body fluid (SBF) at body temperature. The ball on a flat tribometer was used to determine wear rate, depth, width, and friction coefficient at 15 N. The results revealed that a needle-like martensite α' structure was noticed on the as-deposited sample. Microstructural characterization significantly affects wear morphologies. The heat-treated specimen showed a more desirable wear performance than the as fabricated.