Methacrylate-based Composites Research Articles

Microleakage Evaluation of a Silorane-Based and Methacrylate-Based Packable and Nanofill Posterior Composites (in vitro comparative study)

This study compared in vitro the microleakage of a new low shrink silorane-based posterior composite (Filtek™ P90) and two methacrylate-based composites: a packable posterior composite (Filtek™ P60) and a nanofill composite (Filtek™ Supreme XT) through dye penetration test. Thirty sound human upper premolars were used in this study. Standardized class V cavities were prepared at the buccal surface of each tooth. The teeth were then divided into three groups of ten teeth each: (Group 1: restored with Filtek™ P90, Group 2: restored with Filtek™ P60, and Group 3: restored with Filtek™ Supreme XT). Each composite system was used according to the manufacturer's instructions with their corresponding adhesive systems. The teeth were then thermocycled, immersed in 1% methylene blue dye for 24 hours at room temperature, embedded in auto-polymerizing acrylic resin and sectioned longitudinally bucco-lingually. Microleakage was evaluated by assessing the linear dye penetration at the tooth/restoration interface occlusally and gingivally. The highest microleakage score occlusally or gingivally was recorded and the results were analyzed statistically using SPSS version 13. The results of this study showed that the silorane-based posterior composite Filtek™ P90 showed significantly less microleakage than the methacrylate-based packable composite (Filtek™ P60) and the nano-filled composite (Filtek™ Supreme XT) when the tooth-restoration interface is located in enamel.

Effects of Water Sorption and Solubility on Degradation of Silorane and Methacrylate-Based Dental Composites.

Wet oral environment may have deleterious effects on performance of the composites due to influences of water sorption and solubility. The study evaluated the hydrolytic degradation caused because of water sorption and solubility of silorane and methacrylate-based dental composites. Ten disc samples (2 mm × 10 mm) were prepared. Samples were analyzed for water solubility and sorption according to ISO 4049:2000 regulations and tested for mass gain or loss following immersion in water or in artificial saliva at 1 day, 15 days, and 30 days period. Student's 't' test, repeated measures analysis of variance (ANOVA), and Tukey's post-hoc tests determined statistical significance of the experimental results with global significance set at P = 0.05. Considerable sorption and solubility was observed with time in both materials on immersion. Silorane composites showed lower water sorption and solubility than methacrylate-based composite (MBC). Artificial saliva demonstrated higher sorption and solubility compared to distilled water. Silorane composites display enhanced hydrolytic stability even after a month of immersion in contrast to conventional methacrylate-based composites (MBCs), making it a better alternative to MBC resins clinically.

Considerations about Cytotoxicity of Resin-Based Composite Dental Materials: A Systematic Review.

The dental material industry is rapidly developing resin-based composites (RBCs), which find widespread use in a variety of clinical settings. As such, their biocompatibility has gained increasing interest. This literature review presents a summary of research into the cytotoxicity of methacrylate-based composites published from 2017 to 2023. Subject to analysis were 14 in vitro studies on human and murine cell lines. Cytotoxicity in the included studies was measured via MTT assay, LDH assay, and WST-1 assay. The QUIN Risk of Bias Tool was performed to validate the included studies. Included studies (based entirely on the results of in vitro studies) provide evidence of dose- and time-dependent cytotoxicity of dental resin-based composites. Oxidative stress and the depletion of cellular glutathione (GSH) were suggested as reasons for cytotoxicity. Induction of apoptosis by RBCs was indicated. While composites remain the golden standard of dental restorative materials, their potential cytotoxicity cannot be ignored due to direct long-term exposure. Further in vitro investigations and clinical trials are required to understand the molecular mechanism of cytotoxicity and produce novel materials with improved safety profiles.

Microleakage Evaluation of Two Methacrylate-Based Composites (GC Kalore and Luna SDI) in Class II Restorations: A Laboratory Study.

In recent years, dental composite resins such as tooth-colored restoration are frequently used to restore dental cavities, coronal fractures, and congenital defects. This study aimed to evaluate the microleakage of two methacrylate-based composites (GC Kalore and Luna SDI) in class II restorations. In this experimental study, a total of 18 intact human premolars previously extracted for periodontal and orthodontic reasons were randomly divided into two groups. Similar class II cavities (box only) were prepared on all teeth and restored with two different composites. In group 1, a bonding agent (Single Bond 2-SB2; 3M ESPE) and Luna SDI composite in mesial cavities and GC Kalore composite in distal cavities were used. In group 2, Single Bond 2 and GC Kalore composite in mesial cavities and Luna SDI composite in distal cavities were applied. They were then subjected to 2000 thermal cycles in a water bath between 5-55°C (dwell time: 30 seconds in every bath and transfer time: 10 seconds). Then, they were immersed in a 2% basic fuchsin dye solution for 24 hours. After rinsing with water, they were sectioned mesiodistally and evaluated for microleakage using a stereomicroscope. Independent t-test (Mann-Whitney test) showed no statistically significant difference for microleakage in mesial and distal class II restorations between GC Kalore composite and Luna SDI composite (p = 1.000) (p= 0.852). A total of 83.4% of the Luna SDI composite samples and 66.6% of the GC Kalore composite had a microleakage score of ≤3 in class II cavities. In the present study, marginal microleakage was found mainly at the gingival floor extending to 1/3 of the axial wall for the Luna SDI composite and GC Kalore composite. Furthermore, no statistically significant difference was found between the microleakage of the Class II cavities restored with Luna SDI composite and GC Kalore composite.

Degradation of Dental Methacrylate-Based Composites in Simulated Clinical Immersion Media.

The selection of restorative materials with regard to the longevity and durability of a restoration is of crucial importance for daily dental practice and requires that the degradation of the material in the oral environment can be assessed. The aim of this study was to investigate the extent to which the mechanical properties of four (Esthet X, Ceram X, Filtek Supreme XT, and Filtek Supreme XT flow) resin-based composites (RBCs) alter during storage in saliva substitutes (artificial saliva) for 24 h and 28 days and in the context of simulated, more aggressive clinical conditions, including cycles exposure to de- and remineralization, alcohol, or salivary enzymes. For this purpose, flexural strength and modulus were determined in a three-point bending test (n = 20) followed by Weibull analysis, while quasi-static behavior was evaluated by instrumented indentation techniques. Degradation occurred in all RBCs and all aging protocols and was quantifiable at both macroscopic and microscopic levels. The postulated stabilizing effect on degradation through the incorporation of urethane-based co-monomers into the organic matrix or a higher filler loading is refuted. Even though modern RBCs show high clinical survival rates, biodegradation remains an issue that needs to be addressed.

Triacrylamide-Based Adhesives Stabilize Bonds in Physiologic Conditions

In this study, an acrylamide-based adhesive was combined with a thiourethane-based composite to improve bond stability and reduce polymerization stress, respectively, of simulated composite restorations. The stability testing was conducted under physiologic conditions, combining mechanical and bacterial challenges. Urethane dimethacrylate was combined with a newly synthesized triacrylamide (TMAAEA) or HEMA (2-hydroxyethyl-methacrylate; control) to produce a 2-step total-etch adhesive system. Methacrylate-based composites (70 wt% silanized filler) were formulated, containing thiourethane oligomers at 0 (control) or 20 wt%. Standardized preparations in human third molars were restored; then, epoxy replicas were obtained from the occlusal surfaces before and after 7-d storage in water or with Streptococcus mutans biofilm, which was tested after storage in an incubator (static) or the bioreactor (mechanical challenge). Images were obtained from the replicas (scanning electron microscopy) and cross sections of the samples (confocal laser scanning microscopy) and then analyzed to obtain measurements of gap, bacterial infiltration, and demineralization. Microtensile bond strength of specimens stored in water or biofilm was assessed in 1-mm2 stick specimens. Data were analyzed with analysis of variance and Tukey’s test (α = 0.05). HEMA-based materials had greater initial gap measurements, indicating more efficient bonding for the acrylamide materials. When tested in water, the triacrylamide-based adhesive had smaller gaps in the incubator or bioreactor. In the presence of biofilm, there was less difference among materials, but the acrylamide/thiourethane combination led to statistically lower gap formation in the bioreactor. HEMA and TMAAEA-based adhesives produced statistically similar microtensile bond strengths after being stored in water for 7 d, but after the same period with biofilm-challenged specimens, the TMAAEA-based adhesives were the only ones to retain the initial bond strength values. The use of a stable multiacrylamide-based adhesive led to the preservation of the resin-dentin bonded interface after a physiologically relevant challenge. Future studies will include a multispecies biofilm model.

Evaluation of the Effect of Water on the Flexural and Shear Strength of Silorane and Methacrylate-based Composites; A Review of Long-term Studies

Evaluation of the Effect of Water on the Flexural and Shear Strength of Silorane and Methacrylate-based Composites; A Review of Long-term Studies

The Influence of Pineapple Leaf Fiber Orientation and Volume Fraction on Methyl Methacrylate-Based Polymer Matrix for Prosthetic Socket Application.

This work reports on the use of low-cost pineapple leaf fiber (PALF) as an alternative reinforcing material to the established, commonly used material for prosthetic socket fabrication which is carbon-fiber-reinforced composite (CFRC) due to the high strength and stiffness of carbon fiber. However, the low range of loads exerted on a typical prosthetic socket (PS) in practice suggests that the use of CFRC may not be appropriate because of the high material stiffness which can be detrimental to socket-limb load transfer. Additionally, the high cost of carbon fiber avails opportunities to look for an alternative material as a reinforcement for composite PS development. PALF/Methyl Methacrylate-based (MMA) composites with 0°, 45° and 90° fiber orientations were made with 5–50 v/v fiber volume fractions. The PALF/MMA composites were subjected to a three-point flexural test to determine the effect of fiber volume fraction and fiber orientation on the flexural properties of the composite. The results showed that 40% v/v PALF/MMA composite with 0° fiber orientation recorded the highest flexural strength (50 MPa) and stiffness (1692 MPa). Considering the average load range exerted on PS, the flexural performance of the novel composite characterized in this work could be suitable for socket-limb load transfer for PS fabrication.

Cytotoxicity of Silorane and Methacrylate based Dental Composites on Human Pulp Cells

Introduction: The ingredients from the dental restoratives are known to leach and elicit a host response. The prerequisite to deem a material biocompatible requires its toxicologic evaluation. The study was performed to analyze the probable toxicity resulting from silorane-based composite (SBC) with methacrylate-based composite (MBC). Materials and Methods: The in vitro cytotoxicity test, methyl thiazolyl tetrazolium (MTT) assay, evaluated the cell viability and proliferation rate of dental pulp cells (DPCs). The extirpated pulp was cultured in α-MEM-containing supplements and incubated at 37°C. DPCs were subjected to varying doses of SBC or MBC at different time intervals after attaining confluence and monitored for proliferation and viability via MTT assay. An independent Student t test was performed to compare the effect of composites on the DPC. The cytotoxicity levels were compared using one-way analysis of variance and posthoc Tukey multiple comparison test at 5% level of significance and P-value of 90%) in the first 24 hours. The count significantly reduced by the end of 48 hours (minimum 65% in 25 μg/ml) at all concentrations (P

Minimal intervention in dentistry: which is the best approach for silorane composite restoration repairs?

BackgroundThis study aimed to evaluate surface treatments, adhesives and composites for repairing silorane based restorations. Material and MethodsOne hundred and twenty truncated cones (2 mm smaller diameter and 4 mm larger diameter) made of silorane composite were divided in 12 groups according with the surface treatment (diamond bur and oxide aluminum abrasion), the adhesive (Adper Scothbond Multipurpose (3M ESPE), Ecusit (Voco) and Filtek P90 Adhesive (3M ESPE)). Each group was subdivided in two according with the composite used for repair (methacrylate and silorane). The repair was made with a second truncated cone build over the first one and bond strength assssed by tensile strength. Data were submitted to ANOVA 3-way and Tukey’s test (p<0.05). ResultsThere was difference only for the adhesives and the composites, with conventional adhesives (Adper Scothbond Mutipurpose) and methacrylate-based composites (Filtek Z350) presenting superior tensile strength compared to the silorane ones (P90 Adhesive system and composite). ConclusionsTherefore, it must be concluded that silorane composite can be repaired with methacrylate base composites and adhesives. Key words:Silorane composites, composites, bond strength, minimal intervention.

The effect of different curing units on the degree of polymerization of different composite resins

Objective: The aim of this study was to investigate the degree of polymerization of composite resins cured with different light-curing units (LCUs). Materials and Methods: Three bulk-fill composite (Beautifil Bulk-Fill Giomer, Filtek Bulk-Fill, and X-Tra Fill) and a methacrylate-based composite (Filtek Z250) were used in this study. Thirty disc-shaped specimens, 4 mm thick, were prepared from each composite resin. Specimens were divided into three groups and polymerized with light-emitting diode (LED), Plasma arch curing unit (PAC), and quartz-tungsten halogen LCU. The bottom and top surface microhardness of the specimens stored in distilled water for 24 h at 37°C after polymerization was measured with a universal test device. The hardness ratio (HR) of specimens was calculated by the bottom surface microhardness/top surface microhardness formula. Data were analyzed by two-way ANOVA and Tukey's least significant difference post hoc tests (α = 0.05). Results: Statistically significant differences were detected between the mean HR values of the specimens polymerized with different LCUs (P Conclusion: The degree of polymerization of the composite resin restoration may be affected by the structural properties of the resin and the type of LCU. The clinician may use alternative techniques, especially in deep cavities.

Dynamic covalent chemistry (DCC) in dental restorative materials: Implementation of a DCC-based adaptive interface (AI) at the resin–filler interface for improved performance

ObjectiveDental restorative composites have been extensively studied with a goal to improve material performance. However, stress induced microcracks from polymerization shrinkage, thermal and other stresses along with the low fracture toughness of methacrylate-based composites remain significant problems. Herein, the study focuses on applying a dynamic covalent chemistry (DCC)-based adaptive interface to conventional BisGMA/TEGDMA (70:30) dental resins by coupling moieties capable of thiol–thioester (TTE) DCC to the resin–filler interface as a means to induce interfacial stress relaxation and promote interfacial healing. MethodsSilica nanoparticles (SNP) are functionalized with TTE-functionalized silanes to covalently bond the interface to the network while simultaneously facilitating relaxation of the filler–matrix interface via DCC. The functionalized particles were incorporated into the otherwise static conventional BisGMA/TEGDMA (70:30) dental resins. The role of interfacial bond exchange to enhance dental composite performance in response to shrinkage and other stresses, flexural modulus and toughness was investigated. Shrinkage stress was monitored with a tensometer coupled with FTIR spectroscopy. Flexural modulus/strength and flexural toughness were characterized in three-point bending on a universal testing machine. ResultsA reduction of 30% in shrinkage stress was achieved when interfacial TTE bond exchange was activated while not only maintaining but also enhancing mechanical properties of the composite. These enhancements include a 60% increase in Young’s modulus, 33% increase in flexural strength and 35% increase in the toughness, relative to composites unable to undergo DCC but otherwise identical in composition. Furthermore, by combining interfacial DCC with resin-based DCC, an 80% reduction of shrinkage-induced stress is observed in a thiol–ene system “equipped” with both types of DCC mechanisms relative to the composite without DCC in either the resin or at the resin–filler interface. SignificanceThis behavior highlights the advantages of utilizing the DCC at the resin–filler interface as a stress-relieving mechanism that is compatible with current and future developments in the field of dental restorative materials, nearly independent of the type of resin improvements and types that will be used, as it can dramatically enhance their mechanical performance by reducing both polymerization and mechanically applied stresses throughout the composite lifetime.

Polymerization Shrinkage of Five Bulk-Fill Composite Resins in Comparison with a Conventional Composite Resin

The polymerization shrinkage of methacrylate-based composites is among the most important causes of failure of composite restorations. The manufacturers claim that bulk-fill composites have a lower polymerization shrinkage than conventional composites. This study aimed to assess the polymerization shrinkage of five bulk-fill composites in comparison with a conventional composite. In this in-vitro experimental study, composite discs (n=30) were fabricated using everX Posterior (EXP), Filtek Bulk-Fill Posterior (FBP), SonicFill 2 (SF2), Tetric N-Ceram Bulk-Fill (TNB), X-tra fil (XF), and Filtek Z250 conventional composite at the center of a metal ring bonded to a microscope slide and were covered with a coverslip. This assembly was transferred to a linear variable differential transformer (LVDT). Light-curing (1200 mW/cm2) was performed from underneath the slide for 30 seconds. The deflecting disc method and LVDT were used to assess the dimensional changes of the samples (indicative of polymerization shrinkage) at 1, 30, 60, and 1800 seconds following the onset of light irradiation. Data were analyzed using one-way analysis of variance (ANOVA) and Tukey's test. The groups were significantly different regarding polymerization shrinkage (P<0.002). The polymerization shrinkage of the tested composites following the onset of light irradiation ranged from 0.19 to 3.03. EXP showed a significantly higher polymerization shrinkage than other composites at 30, 60, and 1800 seconds after light irradiation, while XF showed the lowest polymerization shrinkage at the aforementioned time points. The tested bulk-fill composites had a polymerization shrinkage similar to that of the conventional composite.

Active diazonium-modified zeolite fillers for methacrylate-based composites

ABSTRACTThe surface properties of the fillers have a significant effect on the mechanical properties of the composites. Despite many uses of diazonium interface chemistry, it has rarely been used in the modification of fillers, although it has much to offer. In this work zeolite surface was modified by 4-(dimethylamino)benzenediazonium cation to obtain an active filler having dimethylamino groups for potential further applications. Modification effectiveness was determined by means of scanning-electron microscopy, energy-dispersive X-ray spectroscopy and X-ray photoelectron spectroscopy. All applied methods confirmed the presence of an organic layer on the surface of modified zeolite, thereby the success of modification. A modified material was applied as an active filler in a methacrylic-resin-based photocurable composites which are mainly used in many dental applications. To verify the active properties of a zeolite filler some mechanical properties, as well as crosslinking ability were examined. All conducted tests proved that the addition of some amount of modified filler is beneficial for the final composite.

Silorane versus methacrylate composites: A comparative study of the micro-leakage

This in vitro study aimed to evaluate the micro-leakage at the occlusal and cervical margins in class II cavities in permanent molars restored with a low shrink silorane resin composite (Filtek P90) applied with or without etching and two methacrylate-based composite resins (valux plus and Amelogen® plus). Two standardised class II box cavities were prepared in proximal surfaces of 60 sound non-fluorotic permanent molars which were divided into three groups of 20 each according to the type of composite. Group I: silorane-based composite (Filtek P90) in the mesial cavity and methacrylate-based microhybrid composite (Adper single bond 2/valux plus) in the distal cavity, Group II: silorane-based composite in the mesial cavity and silorane-based composite with previous etching in the distal cavity, and Group III: silorane-based composite in the mesial cavity and methacrylate-based micro-hybrid composite (PQ1 /Amelogen plus) in the distal cavity. The samples underwent an artificial aging with thermocycling. Root apices were sealed with transparent orthodontic resin and coated with transparent varnish except 1 mm around the restoration. The specimens were immersed in 1% methylene blue solution at room temperature for 48 hour. The samples were sectioned longitudinally in the mesiodistal direction and evaluated under a stereomicroscope at 20X. Scoring was done according to the depth of methylene blue penetration into the cavities. Statistical analysis of the data was performed using SPSS 17.0 software. Silorane-based composite resin showed less micro-leakage than the methacrylate-based composites. Etching improved the sealing ability of silorane restorations. Silorane-based composite preceded by etching had less micro-leakage among the other materials used in this in vitro study. Keywords: Silorane, methacrylate based composite, sealing, micro-leakage, class II cavity

Effect of rinsing time and surface contamination on the bond strength of silorane-based and dimethacrylate-based composites to enamel.

BackgroundThe aim of this study was to assess whether saliva contamination and rinsing time for 15, 30, and 60 seconds, affects the shear bond strength of silorane and methacrylate-based composites to enamel.Material and MethodsTwo light cure resin, P60 (3M ESPE) and Filtek LS Silorane were tested. 120 sound premolars were randomly divided into four groups of 30 teeth based on composite type with or without saliva contamination after etching and rinsing. Each group was further divided into three subgroups according to their rinsing time. Then a cylinder of the composite was bonded to the enamel and Shear bond strength was assessed. To determine the failure mode, the bonded surfaces were then observed under SEM. In addition, the DC of each group was measured at pH levels of 4 and 7 using FTIR spectroscopy. The data were analyzed with one-way ANOVA and post hoc analysis followed by Fisher’s least significant difference.ResultsThe bond strength of the non-contaminated methacrylate group was significantly higher than the other groups (p< 0.0001). In addition, there was no significant deference between the methacrylate subgroups. In the silorane groups, the shear bond strength was higher in the rinsing time of 15 seconds. Failure pattern was mainly adhesive. The DC of the Methacrylates had no significant difference at pH 4 and pH 7, but was significantly higher than that of siloranes (p< 0.0001). While the DC of the siloranes at pH 4 was significantly higher than at pH 7 (p< 0.0001).ConclusionsSaliva contamination in both composites reduces bond strength. Increasing rinsing time in Methacrylates proves ineffective. In non-contaminated siloranes, excessive rinsing time reduced bond strength. The best-recommended rinsing time for both composite is 15 seconds. Key words:Composite resins, silorane composite resin, methacrylates, shear strength.

Comparison of Shear Bond Strength of Silorane and Methacrylate-Based Composites to IPS Empress 2 Ceramic with Various Surface Treatments

Objectives Treatment of chipped or fractured porcelain with composite resin is considered as an economic treatment for minor fractures in ceramics. The aim of this study was to evaluate the effect of different ceramic surface treatments on bond strength of methacrylate-based and silorane-based composite resin to IPS Empress 2.Methods Sixty IPS Empress 2 ceramic discs were fabricated and after etching with 9.6% hydrofluoric acid, they were divided into six groups:(1) P90 primer and bonding agent + Filtek P90 composite resin; (2) Single Bond + Filtek Z250 composite resin; (3) similar to the first group+ silane pretreatment; (4) similar to the second group + silane pretreatment; (5) silane pretreatment + Filtek P90 composite resin; (6) silane pretreatment + Filtek Z250 composite resin. Each specimen was subjected to shear load until fracture occurred. Statistical analysis was performed using one-way ANOVA, Tukey’s test and t-test.Results Regardless of the type of surface treatment, Z250 composite demonstrated significantly higher shear bond strength than P90 composite (P < 0.05). Group 4 showed the highest shear bond strength values with statistically significant difference with other groups while the fifth group showed the least values (P < 0.05).Conclusion Silane coating along with the application of adhesive system and etching in methacrylate-based composite was the most efficient surface treatment in terms of bond strength.

Discoloration Effects of Traditional Turkish Beverages on different Composite Restoratives.

The aim of this study was to evaluate the discoloring effects of five beverages including, especially, traditional Turkish ones on five commonly used dental composites by using a spectrophotometer device. Five methacrylate-based composites (shade A2) were selected to evaluate their color stability (175 disk samples). Four of them (Filtek Ultimate Universal, Clearfil Majesty ES-2, Tetric EvoCeram, and Cavex Quadrant Universal LC) were nanofilled universal composites for both anterior and posterior restorations, and one (Clearfil Majesty Posterior) was nano-superfilled for posterior restorations. The tested beverages were tamarind syrup, ottoman syrup, turnip juice, pomegranate juice, and distilled water (control). All samples were kept in an incubator at 37°C for 12 days (measured at 3rd, 6th, 12th day intervals) in immersion solutions which was equivalent to 1 year in vivo. Color measurements were made with VITA Easyshade Advance (Vident, Brea, CA) spectrophotometer device according to CIE L*a*b* system. Statistical analysis was performed with analysis of variance and least significant difference test to analyze differences in L*a*b* and ΔE values. All materials showed significant discoloration (p < 0.05) when compared with the control group. The highest ΔE was observed in turnip juice, whereas ottoman syrup had the lowest ΔE. Tetric EvoCeram showed the lowest ΔE, while Clearfil Majesty ES-2 showed the highest ΔE. In all the groups tested, clinically unacceptable ΔE values were obtained. Although color stability of methacrylate-based composites has been widely investigated, this has not been done before with these kinds of immersion solutions. Potential discoloration might be limited by dietary adjustments based on in vitro evaluations.

Effect of water storage on flexural strength of silorane and methacrylate-based composite resins.

ObjectivesThis study assessed the effect of water storage on the flexural strength (FS) of low shrinkage composites.Materials and MethodsA total of 165 bar-shaped specimens (2 × 2 × 25 mm) were fabricated of 2 low shrinkage composites (Filtek P90 [3M ESPE], GC Kalore [GC International]) and a conventional methacrylate-based composite (Filtek Z250 [3M ESPE]). The specimens were subjected to 3-point bending test at 6 time intervals, namely: immediately after curing, at 24 hours, 1 week, 1 month, 6 months, and 1 year following storage in wet and dry conditions. The FS of the specimens were measured by applying compressive load at a crosshead speed of 1.0 mm/min. Data was analyzed using 3-way analysis of variance (ANOVA) and Tukey's test.ResultsThree-way ANOVA revealed significant interactions between time, type of composite, and storage condition (p = 0.001). Tukey's multiple comparison test revealed significant reductions in FS of all composites after 6 months and 1 year of storage in distilled water compared to dry condition.ConclusionsFiltek P90 showed the highest and GC Kalore showed the lowest FS after 1 year storage in distilled water. The immediate high strength of Filtek Z250 significantly decreased at 1 year and its final value was lower than that of Filtek P90.

Fracture resistance of premolars teeth restored by silorane, nanohybrid and two types of fiber-reinforced composite: an in-vitro study

Objective The objective was to evaluate and compare the fracture resistance of human maxillary premolars teeth restored with low shrinkage microhybrid composite Silorane-based; Filtek P90 LS, conventional methacrylate-based nanohybrid composite; Ceram X Mono, and two types of fiber-reinforced composites (FRCs); Alert and XENIUS base, micro glass fibers and short glass fibers, respectively in mesio-occluso-distal cavities. Materials and methods A total of 45 human maxillary premolars were selected. Standardized mesio-occluso-distal cavities were prepared in all teeth. Five prepared teeth received no treatment and served as controls (group 1). A total of 40 teeth were randomly divided into four experimental groups (n = 10); group 2: low shrinkage Silorane-based composite, group 3: nanohybrid resin composite, group 4: microfibers reinforced resin composite, and group 5: short fibers reinforced resin composite. Restorations were done for all groups. After being stored 24 h at 37°C, fracture resistance was measured in a universal Instron testing machine by using a 4 mm diameter steel sphere which was applied on tooth buccal and lingual cusps at a cross-head speed of 2 mm/min until fracture occurred. Statistical analysis One-way analysis of variance and Tukey's post-hoc test. Results Highest mean fracture resistance was observed with FRC, nanohybrid, Silorane and lastly with control respectively. Statistically Significant difference was revealed by analysis of variance (P ≤ 0.0001) and Tukey's post-hoc test (P ≤ 0.0001). Conclusion Among the experimental groups, FRC showed the highest fracture resistance.