Mechanical Durability Research Articles

A Fluorinated Imide‐Functionalized Arene Enabling a Wide Bandgap Polymer Donor for Record‐Efficiency All‐Polymer Solar Cells

AbstractAll‐polymer solar cells (all‐PSCs) present compelling advantages for commercial applications, including mechanical durability and optical and thermal stability. However, progress in developing high‐performance polymer donors has trailed behind the emergence of excellent polymer acceptors. In this study, we report a new electron‐deficient arene, fluorinated bithiophene imide (F‐BTI) and its polymer donor SA1, in which two fluorine atoms are introduced at the outer β‐positions in the thiophene rings of BTI to fine‐tune the energy levels and aggregation of the resulting polymers. SA1 exhibits a deep HOMO level of −5.51 eV, a wide bandgap of 1.81 eV and suitable miscibility with the polymer acceptor. Polymer chains incorporating F‐BTI result in a highly ordered π–π stacking and favorable phase‐separated morphology within the all‐polymer active layer. Thus, SA1 : PY‐IT‐based all‐PSCs exhibit an efficiency of 16.31 % with excellent stability, which is further enhanced to a record value of 19.33 % (certified: 19.17 %) by constructing ternary device. This work demonstrates that F‐BTI offers an effective route for developing new polymer materials with improved optoelectronic properties, and the emergence of F‐BTI will change the scenario in terms of developing polymer donor for high‐performance and stable all‐PSCs.

Development and Characterization of Lime-Based Mortars Modified with Graphene Nanoplatelets

Materials for the conservation of cultural heritage must meet specific demands, such as high durability, service life, and compatibility with other materials used in the original building structures. Due to their low permeability to water and water vapor and their high rigidity, the use of Portland cement (PC) mortars, despite their high mechanical resistance and durability, does not represent an appropriate solution for the repair of historic masonry and structures. Their incompatibility with the original materials used in the past, often on a lime basis, is therefore a serious deficiency for their application. On the other hand, lime-based mortars, compared to PC-based materials, are more susceptible to mechanical stress, but they possess high porosity, a high water vapor transmission rate, and moderate liquid water transport. This study aims at the development of two types of lime-based mortars, calcium lime (CL) and hydraulic lime (HL). The modification of mortars was conducted with a carbon-based nanoadditive and graphene nanoplatelets (GNs) in three dosages: 0.1%, 0.3%, and 0.5% of the binder weight. The enhancement of CL mortars by GNs greatly increased mechanical strength and affected heat transport characteristics, while other characteristics such as porosity, water absorption, and drying rate remained almost similar. The application of GNs to HL not only enhanced the strength of mortars but also decreased their porosity, influenced pore size distribution, and other dependent characteristics. It can be concluded that the use of graphene nanoplatelets as an additive of lime-based composites can be considered a promising method to reinforce and functionalize these composite materials. The improved mechanical resistance while maintaining other properties may be favorable in view of the increasing requirements of building materials and may prolong the life span of building constructions.

Flexible Micro‐supercapacitors with Enhanced Energy Density Utilizing Flash Lamp Annealed Graphene‐Carbon Nanotube Composite Electrodes

As demand for micro‐power sources grows, micro‐supercapacitors (MSCs) have become critical for miniaturized devices, offering robust electrochemical energy storage. However, the challenge remains to develop a simple, scalable fabrication method that achieves both high energy and power densities. In this study, we present a refined approach to fabricating MSCs with 3D interconnected graphene/carbon nanotube (CNT) composite electrodes. Our method combines flash lamp annealing (FLA) and laser ablation, where FLA converts graphene oxide (GO) and CNT composite films into 3D‐structured graphene/CNT electrodes, and laser ablation precisely patterns them into interdigitated designs. This dual‐process technique produces MSCs with exceptional electrochemical performance, including an impressive areal capacitance of 26.11 mF/cm2 and a volumetric capacitance of 31.88 F/cm3. These devices also achieve energy densities of 3.72 μWh/cm2 and 4.43 mWh/cm3, maintaining 97% of their initial capacitance under extreme bending, demonstrating outstanding mechanical flexibility and durability. Furthermore, the scalability of this method was validated by configuring MSCs in series and parallel, achieving enhanced voltage and current outputs without additional interconnections. Overall, the integration of FLA and laser ablation holds significant promise for advancing the performance and scalability of micro‐sized energy storage devices, addressing the growing need for efficient, flexible, and high‐capacity micro‐power sources.

SUGAR CANE BAGASSE ASH IN CONCRETE: A REVIEW

Sugarcane bagasse ash (SCBA), a by product of sugarcane processing, has shown great potential as a supplementary material in concrete production. A review of its application in concrete highlights its benefits, including improved mechanical properties, durability, and sustainability. SCBA contains high levels of silica, which can act as a pozzolanic material, enhancing the compressive strength and reducing the permeability of concrete. Incorporating SCBA also lowers the carbon footprint of concrete, contributing to greener construction practices by partially replacing cement. However, challenges remain, such as the variability in ash quality, proper ash treatment, and optimal blending ratios. Ongoing research focuses on refining these aspects to maximize the benefits of the SCBA in concrete, making it a promising alternative in the construction industry for sustainable development. Keyword - Sugarcane bagasse ash, Compression strength, Percentage strength, Sugarcane Workability, Slump test.

An Adhesive Hydrogel Technology for Enhanced Cartilage Repair: A Preliminary Proof of Concept.

Knee cartilage has limited natural healing capacity, complicating the development of effective treatment plans. Current non-cell-based therapies (e.g., microfracture) result in poor repair cartilage mechanical properties, low durability, and suboptimal tissue integration. Advanced treatments, such as autologous chondrocyte implantation, face challenges including cell leakage and inhomogeneous distribution. Successful cell therapy relies on prolonged retention of therapeutic biologicals at the implantation site, yet the optimal integration of implanted material into the surrounding healthy tissue remains an unmet need. This study evaluated the effectiveness of a newly developed photo-curable adhesive hydrogel for cartilage repair, focusing on adhesion properties, integration performance, and ability to support tissue regeneration. The proposed hydrogel design exhibited significant adhesion strength, outperforming commercial adhesives such as fibrin-based glues. An in vivo goat model was used to evaluate the hydrogels' adhesion properties and long-term integration into full-thickness cartilage defects over six months. Results showed that cell-free hydrogel-treated defects achieved superior integration with surrounding tissue and enhanced cartilage repair, with notable lateral integration. In vitro results further demonstrated high cell viability, robust matrix production, and successful cell encapsulation within the hydrogel matrix. These findings highlight the potential of adhesive hydrogel formulations to improve the efficacy of cell-based therapies, offering a potentially superior treatment for knee cartilage defects.

Laboratory investigation of the impact of water-cement ratio on the mechanical properties and durability of roller-compacted concrete mixtures containing polypropylene fibers

Laboratory investigation of the impact of water-cement ratio on the mechanical properties and durability of roller-compacted concrete mixtures containing polypropylene fibers

Scratch load and indenter type dependent scratch evaluation of milled carbon fiber filled basalt fiber/epoxy composites with factorial design

AbstractThis work investigates the addition of milled carbon fiber reinforcement and its effect on scratch resistance and mechanical durability for basalt fiber/epoxy composites, assessed under varied loading conditions with the aid of different indenter types according to a factorial design. Composites with MCF content from 0 to 10 wt% were prepared. Scratch behaviors under Vickers and Rockwell indenters were studied for loads of 5, 10, and 15 N. The addition of 10 wt% MCF has resulted in scratch hardness increase from 13.255 N/mm2 up to 47.952 N/mm2, depending on the type of indenter used. Precisely, in conditions of a 5 N load and when a Rockwell‐type indenter was used, a scratch hardness maximum of 47.952 N/mm2 was achieved, while for a Vickers‐type indenter under the same conditions, the maximum value of its equivalent was 23.327 N/mm2. Profilometric and SEM analyses evidence that matrix cracks and surface deformation have been reduced with higher MCF content, at least for the application of lower scratch test loads. The mechanical and surface performances of the basalt fiber composites were found to be considerably improved by the reinforcement with MCF.Highlights Scratch resistance for milled carbon fibers increases and peaks at 10 wt% reinforcement. The Rockwell indenter indicates a steady increase in hardness up to 47,952 N/mm2. Peak hardness of 10 wt% is observed under the Vickers indenter for the 5 N load. Higher milled carbon fiber content reduces matrix cracking and surface deformation. There is a clear correlation between scratch performance, milled carbon fiber content, and indenter type.

Cytotoxicity and Microbiological Properties of Ceramic CAD/CAM Materials Subjected to Surface Treatment with Nanometric Copper Layer

The aim of this study is to present the characteristics and a comparison of four different commercial materials dedicated to the CAD/CAM technique in dentistry, all of which can be classified as ceramic materials. Its purpose is also to evaluate the impact of surface treatment on the cytotoxicity and microbiological properties of the materials. The CAD/CAM technique has a perpetually growing role in modern reconstructive dentistry. It requires a material’s possession of peculiar characteristics, such as mechanical resistance, durability, functionality (similar to natural tissues), good aesthetics and biocompatibility. To critically evaluate a biomaterial, both manufacturer claims and in vitro tests should be considered. Further steps of evaluation may include animal tests and clinical trials. There are certain attributes of biomaterials that may be modified by surface treatment that can be crucial to the clinical success of the material. The evaluated materials were Vita Suprinity (VITA-Zahnfabrik, Germany), Vita Mark II (VITA-Zahnfabrik, Germany), Celtra Duo (Dentsply Sirona, USA) and Empress Cad (Ivoclar Vivadent, Liechtenstein). They are available in the form of prefabricated blocks of various diameters and are popular among operators performing clinical procedures using CAD/CAM. Standardized blocks of each material were prepared. Half of them had their surface polished. Further, half of all the samples were covered by a nano-copper layer. The samples were evaluated for cytotoxicity, presented on a 0–4 scale, adhesion susceptibility and potential of forming a biofilm on their surface. Physicochemical properties such as the water contact angle (WCA) were evaluated for the tested materials. The influence of copper coating on cytotoxicity cannot be unequivocally stated or denied. Surface polishing did not affect the materials’ cytotoxicity, but it increased the WCA of all materials and, therefore, their hydrophobicity. Different degrees of adhesion ability and biofilm formation were dependent on the species of microorganisms and properties of the dental materials.

Artificial neural network-enhanced mathematical simulation based on Carrera unified formulation for dynamic analysis and structural integrity assessment of advanced nanocomposites reinforced tunnel structures

This article presents the application of the Carrera Unified Formulation (CUF) for dynamic analysis and structural integrity assessment of advanced nanocomposite-reinforced tunnel structures. CUF offers a generalized framework that simplifies the modeling of complex structures, providing an efficient approach to address the dynamic behavior of nanocomposites. Advanced nanocomposites, which enhance mechanical performance and durability, are increasingly used in critical infrastructure such as tunnel systems. Traditional methods often fall short in capturing the intricate interactions within these materials, particularly under dynamic loads. CUF overcomes these challenges by incorporating higher-order theories and multi-scale analysis, allowing for accurate prediction of displacements, stresses, and potential failure modes. To further validate the results, an Artificial Neural Network (ANN) model is trained using simulated data, ensuring robust predictions for various loading conditions. The ANN assists in approximating the dynamic response and integrity of the structure, enabling real-time assessments with minimal computational expense. The combined CUF-ANN approach demonstrates high accuracy and efficiency, making it a reliable tool for the structural integrity assessment of nanocomposite-reinforced tunnels. This study highlights the significant potential of integrating CUF and ANN for the analysis and design of advanced engineering structures subjected to dynamic environmental conditions.

The influence of volcanic ash (VA) on the mechanical properties and freeze-thaw durability of lime kiln dust (LKD)-stabilized kaolin clayey soil

Improving soft clay soil's mechanical properties and durability has been the subject of intense research. In this context, traditional stabilizers such as cement and lime have been introduced as the most widely used materials. However, the utilization of these conventional additives poses several challenges due to recent global concerns regarding the reduction of greenhouse gas emissions. Therefore, international research is shifting toward using environmentally friendly soil-stabilizing waste materials. This study, for the first time, evaluates the stabilization of kaolin clay soil using lime kiln dust (LKD) as a high CaO content waste pozzolan and volcanic ash (VA) as a natural pozzolan with considerable SiO2 and Al2O3 contents. In general, the research aims to demonstrate the effective performance of these two inexpensive and environmentally friendly additives in improving the mechanical characteristics and durability of kaolin clay soil, thereby providing the essential groundwork for the practical application of this method in stabilizing soft clay soil. This study included preparing samples with LKD at 3%, 5%, 7%, and 10% of the dry weight of clay and replacing LKD with VA at 0%, 25%, 75%, and 100%. The specimens were cured for 3, 7, and 28 days. Following the curing process, the optimal sample was subjected to varying numbers of freeze-thaw (F-T) cycles. The samples were examined by conducting a series of standard compaction, unconfined compressive strength (UCS), ultrasonic pulse velocity (UPV), scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FTIR), and X-ray diffraction (XRD) tests at different stages of adding stabilizers, as well as before and after exposure of F-T cycles. The findings revealed that adding LKD and VA increased the UCS by accelerating and improving the pozzolanic and hydration reactions. Also, the combination of LKD and VA in kaolin soil enhanced F-T durability, resulting in less strength deterioration even after 10 cycles, when compared to the untreated control sample. In particular, the optimal mixture containing 5% LKD and 25% VA replacement improved 11 times in UCS compared to untreated kaolin clay and showed a slight reduction of only 7% after 10 F-T cycles. Overall, the incorporation of LKD and VA enhanced the mechanical properties and F-T durability of kaolin clay soil, making it a low-cost, sustainable, and eco-friendly option for soil improvement.

Optimizing drying time of lacquer-based MTCS-modified SiO2-TiO2 coatings for enhanced mechanical durability, superhydrophobicity and photocatalytic activity

This research successfully improved the mechanical durability of a superhydrophobic coating on wet lacquer. Methyltrichlorosilane (MTCS) modified SiO2-TiO2 nanoparticles (NPs) were applied to a wet lacquer layer with various drying times using a simple spraying technique. The optimal coating exhibited superhydrophobicity with a water contact angle of 157° and a sliding angle of 2°. Additionally, the superhydrophobic surface could withstand over 100,000 water drops, 200 g of sand, and 40 tape-peeling repetitions, indicating high mechanical stability. Moreover, the superhydrophobic surface demonstrated photocatalytic activity by degrading methylene blue (MB) solution. The coating showed excellent adaptability to different substrates, including automotive body panels, with self-cleaning properties. This simple and effective strategy has potential for large-scale fabrication for practical applications in various industrial fields.

Performance evaluation of high-performance concrete mixes incorporating recycled steel scale waste as fine aggregates

In this study, steel-scale waste (SSW), a byproduct generated during the manufacturing of steel, was investigated as a potential alternative to natural fine aggregates (sand) for preparing high-performance concrete (HPC). Three grades of sand and SSW with different particle sizes were mixed in varying combinations. Three different compaction techniques (loose, tamped, vibration) were employed. The optimum packing density for both SSW and natural aggregates was achieved using the vibration compaction method. Since the combination of 50 % sand and 50 % SSW exhibited the best packing density for both materials, this bi-grade aggregate mixture was selected for the mix preparation. The mechanical tests (compressive strength, flexural strength) and durability assessment (bulk water sorptivity, rate of water absorption, chloride ion penetration) were performed to achieve the desired objectives. The specimens were exposed to two different curing regimes i.e., normal curing and heat curing at elevated temperature. A significant increase in compressive and flexural strength was observed with the increased content of SSW. A compressive strength as high as 140 MPa was obtained for the HPC mix containing SSW aggregates and steel fibers. The replacement ratio of SSW was optimized to achieve better strength and durability. Experimental results showed that heat curing was more effective than conventional curing methods in improving the performance of the concrete.

The Influence and Mechanism of Polyvinyl Alcohol Fiber on the Mechanical Properties and Durability of High-Performance Shotcrete

This study investigates the impact of polyvinyl alcohol (PVA) fibers on the mechanical properties and durability of high-performance shotcrete (HPS). Results demonstrate that PVA fibers have a dual impact on the performance of HPS. Positively, PVA fibers enhance the tensile strength and toughness of shotcrete due to their intrinsic high tensile strength and fiber-bridging effect, which significantly improves the material’s splitting tensile strength, deformation resistance, and toughness, and the splitting tensile strength and peak strain have been found to be increased by up to 30.77% and 31.51%, respectively. On the other hand, the random distribution and potential agglomeration of PVA fibers within the HPS matrix can lead to increased air-void formations. This phenomenon raises the volume content of large bubbles and increases the average bubble area and diameter, thereby elevating the pore volume fraction within the 500–1200 μm and >1200 μm ranges. Therefore, these microstructural changes reduce the compactness of the HPS matrix, resulting in a decrease in compressive strength and elastic modulus. The compressive strength exhibited a reduction ranging from 10.44% to 15.11%, while the elastic modulus showed a decrease of between 8.09% and 12.67%. Overall, the PVA-HPS mixtures with different mix proportions demonstrated excellent frost resistance, chloride ion penetration resistance, and carbonation resistance. The electrical charge passed ranged from 133 to 370 C, and the carbonation depth varied between 2.04 and 6.12 mm. Although the incorporation of PVA fibers reduced the permeability and carbonation resistance of shotcrete, it significantly mitigated the loss of tensile strength during freeze–thaw cycles. The findings offer insights into optimizing the use of PVA fibers in HPS applications, balancing enhancements in tensile properties with potential impacts on compressive performance.

Innovative Hemp Shive-Based Bio-Composites: Part I: Modification of Potato Starch Binder by Sodium Meta-Silicate and Glycerol

The growing demand for sustainable building materials has boosted research on plant-based composite materials, including hemp shives bound with biodegradable binders. This study investigates the enhancement of potato-starch-based binders with sodium metasilicate and glycerol to produce eco-friendly bio-composites incorporating hemp shives. Potato starch, while renewable, often results in suboptimal mechanical properties and durability in its unmodified form. The addition of sodium metasilicate is known to improve the mechanical strength and thermal stability of starch-based materials, while glycerol acts as a plasticizer, potentially enhancing flexibility and workability. Bio-composites were produced with varying concentrations of sodium metasilicate (0–107% by mass of starch) and glycerol (0–133% by mass of starch), and their properties were evaluated through thermal analysis, density measurements, water absorption tests, compressive strength assessments, and thermal conductivity evaluations. The results demonstrate that sodium metasilicate significantly increases the bulk density, water resistance, and compressive strength of the bio-composites, with enhancements up to 19.3% in density and up to 2.3 times in compressive strength. Glycerol further improves flexibility and workability, though excessive amounts can reduce compressive strength. The combination of sodium metasilicate and glycerol provides optimal performance, achieving the best results with an 80% sodium metasilicate and 33% glycerol mixture by weight of starch. These modified bio-composites offer promising alternatives t2 o conventional building materials with improved mechanical properties and environmental benefits, making them suitable for sustainable construction applications.

Use of biomass from Amazonian agro-industrial waste for the production of energy

This research aims to analyze the physical and mechanical properties of briquettes made by açaí, cupuaçu, and murumuru waste from agro-industrial activity in a region of the Brazilian Amazon. For the production of briquettes, biomass with different granulometry (48, 60, 65, and 80 mesh) was sent to hydraulic pressure at constant pressure (15t) with various pressing times (15, 20 and 30 minutes). This process occurred without the addition of binders. The obtained outcomes were evaluated for storage time, bulk density, energy density, calorific value, impact strength, water absorption, and mechanical durability. The briquettes produced with açaí and cupuaçu presented good mechanical characteristics compared to murumuru. Concerning the calorific value, the latter showed better results. There was no alteration in the physical and mechanical properties determinant for the material to present favorable energy generation and durability. The açaí briquettes demonstrated better physical and mechanical properties, while murumuru briquettes indicated the best energy properties. Thus, the use of biomass from different agro-industrial wastes from the Amazon proved to be relevant for the elaboration of briquettes, being an alternative in the production of sustainable energy and adding to the reduction of the accumulation of improper waste disposed of in the environment.

Investigation on effects of nano-reinforcement on the mechanical properties, fatigue, and microstructural analysis of dissimilar AA6061- Mg AZ31B weld joints

Weld joints have been subject to substantial improvement in mechanical durability and wear resistance in recent years. This research work challenge can be answered by incorporating nano-materials into the weld zone. Mechanical and metallurgical aspects of friction stir welded (FSW) butt joints made of AA6061 aluminum and Mg AZ31B alloys have been examined in this work, both with and without the use of naturally derived biochar nanoparticles. The biochar particle was extracted from rice husk. Throughout the whole weld joint manufacturing process, a tool with a rotational speed of 1400 rpm, a welding speed of 40 mm min−1, and a tapered pin profiled tool were employed. During the joint fabrication process, the constant axial load of 7 kN, plunge depth of 0.2 mm, and constant dwell time of 0.3 s were also maintained. In order to improve the mechanical attributes of the weld joints, different wt% of biochar such as 1%, 2%, and 3%, were applied at the interface region of the weld joints. The experimental results revealed that the percentage of reinforced nano-materials plays a significant effect in improving the weld joint qualities. The testing results of reinforced friction stir-welded joint qualities were compared to those of simple friction stir welded joints made without and with adding the nanoparticles. The best results were obtained when 2 wt% of biochar particles was added to the weld interface region. The presence of biochar nano-particles, in addition to their contribution to increased grain refinement in the weld nugget region, was also seen in the region. It was discovered that the event distribution of particles at the nugget zone significantly enhanced the mechanical and wear resistance qualities of the weld joints that were manufactured. The optical microscope was used to analyze the microstructures in the weld nugget region, and a scanning electron microscope (SEM) was utilized to examine the fracture analysis of the tensile samples. The presence of 2 wt% biochar particles in the weld nugget region resulted in a considerable increase in the mechanical characteristics of the weld connections. The ultimate tensile strength, hardness, and yield strength of the weld nugget results 197 MPa, 173 HV, 163 MPa. Overall, when compared to the qualities of the base material and plain weld joints. The mechanical properties and wear resistance of the weld joints have improved significantly. When biochar particles were used as reinforcement particles during the fabrication phase of the joint, a mechanism for pinning was observed in the weld microstructure.

Preparation of Pressure-Resistant and Mechanically Durable Superhydrophobic Coatings via Non-Solvent Induced Phase Separation for Anti-Icing.

Inspired by the lotus leaf effect, superhydrophobic coatings have significant potential in various fields, However, their poor pressure resistance, weak mechanical durability, and complex preparation processes severely limit practical applications. Here, a method for preparing pressure-resistant and durable superhydrophobic coatings by simply spray-coating a phase separation suspension containing fluorinated silica nanoparticles and polyolefin adhesive onto substrates is introduced, which forms superhydrophobic coatings with a porous and hierarchical micro-/nanostructure. The resulting superhydrophobic coatings exhibit outstanding pressure resistance, maintaining a Cassie-Baxte state after 18 days of submersion in 1 m of water. Furthermore, the coatings demonstrate remarkable mechanical durability, withstanding 200 cycles of Taber abrasion, 100 cycles of tape-peeling, and 750g of sand abrasion. The coatings also show excellent chemical stability, enduring long-term immersion in corrosive liquids and 120 d of outdoor exposure. Additionally, the coatings display excellent anti-icing properties and can be applied to various substrate surfaces. This approach improves on the limitations of conventional superhydrophobic coatings and accelerates the application of superhydrophobic coatings in real-world environments.

Photothermal superhydrophobic coating for concrete: Highly effective anti/deicing performance and corrosion resistance

Superhydrophobic concrete is an effective method to prevent corrosion of internal steel bar. However, existing superhydrophobic concrete is difficult to remove the ice on the superhydrophobic concrete surface. Here, we overcame this problem by developing a photothermal superhydrophobic coating for concrete, which obtained from polydimethylsiloxane (PDMS), multi-walled carbon nanotubes (MWCNT) and further superhydrophobicity. This photothermal superhydrophobic coating showed the excellent superhydrophobicity, self-cleaning property, anti-fouling property, and the long anti-icing time. In addition, the ice on the coating would rapidly melt into the water which easily rolled off the surface under the irradiation of infrared light. This coating not only had the good chemical durability and mechanical durability, but also had the corrosion resistance performance. This work will enrich superhydrophobic concrete technology and promote the application of superhydrophobic concrete in practical building.

Mechanical properties and durability of lightweight cenosphere cementitious composites under coupling effect of dry-wet cycles and salt erosion

Cenospheres are suitable as supplementary cementitious materials to partially replace cement in the production of environmentally friendly lightweight cenosphere cementitious composites (LCCC). In this study, the correlation between the content and particle size of the cenosphere, the early curing system and the performance of LCCC was analyzed. The macroscopic properties and microstructural changes of LCCC under the conditions of dry-wet cycles and salt erosion were studied with different early curing conditions. The durability changes of LCCC mortar under the coupling effect of salt erosion and dry-wet cycles were studied by examining the mass loss rate, relative dynamic modulus of elasticity and salt corrosion resistance coefficient of LCCC mortar. Finally, a comparative analysis of the impact of existing cracks on the performance of LCCC under the coupling effect of dry-wet and salt erosion was conducted. The main innovation of the study includes the mechanical properties and durability of LCCC under dry-wet-salt erosion conditions, as well as the clarification of the impact of prefabricated cracks on the mechanical properties and durability of LCCC. It is found that the flexural strength and the compressive strength of specimens cured at high temperature is generally lower than that of the specimens cured under normal temperature conditions. The wet-dry salt corrosion can exacerbate the erosion the outer shell and inner wall of cenospheres and disrupt the stability of the internal interface transition zone (ITZ) in LCCC. LCCC with CsS exhibits better macroscopic performance and microstructural properties. Pre-existing cracks accelerates the erosion in the cenosphere shell and inner wall under salt solution.

Eight years of thin noise reducing asphalt layer monitoring in an urban environment

The City of Antwerp initiated a pilot project on thin noise reducing asphalt layers in an urban environment with the aim to investigate the behavior of the asphalt layers from a noise perspective with respect to urban traffic without neglecting the mechanical durability. Five thin asphalt layers were selected and compared with a reference section. The pavements were constructed in October 2016 on two different test sites. The construction was followed up extensively. The acoustical quality of the thin asphalt layers is followed up in time. Close-ProXimity (CPX) measurements are performed according to ISO 11819-2 within certain time intervals after construction to follow up the evolution. Texture measurements according to ISO 13473 are linked to the noise measurement results. Visual inspections are performed at regular intervals. The results of eight years of monitoring are discussed. While some test sections are already partially replaced, others are still in acceptable condition. The major concern in the STOLA project is to learn about a good balance between the noise reducing capacity of the chosen thin asphalt layers, a limited degradation of the noise performance during its lifetime and a good mechanical performance delaying ravelling and texture changes as long as possible.