In this work we present a new experimental technique alternative to Acoustic Emissions, which makes use of sound signal sensing, to complement the assessment of the mechanical behaviour of sand grains. A post-processing protocol is also proposed. By using this technique in combination with microscopy during in-situ compression tests, it was possible to capture complementary features in the complex mechanical behaviour of granular materials. In addition to that, dominant acoustic frequencies in the sound emitted by sand grains during failure were captured. The method has been applied to study the effects of chemical composition, morphology and grain sizes on the failure mechanics of three types of single sand grains. The advantages of this approach over other traditional techniques to capture failure events during cracking of granular materials have also been clearly demonstrated.
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