Mechanical Properties Of Materials Research Articles

Fabrication and Characterization of Biomedical Ti-Mg Composites via Spark Plasma Sintering.

The fabrication of Ti-Mg composite biomaterials was investigated using spark plasma sintering (SPS) with varying Mg contents and sintering pressures. The effects of powder mixing, Mg addition, and sintering pressure on the microstructure and mechanical properties of the composite materials were systematically analyzed. Uniform dispersion of Mg within the Ti matrix was achieved, confirming the efficacy of ethanol-assisted ball milling for consistent mixing. The Young's modulus of the composite materials exhibited a linear decrease with increasing Mg content, with Ti-30vol%Mg and Ti-50vol%Mg demonstrating reduced modulus values compared to pure Ti. Based on density measurements, compression tests, and Young's modulus results, it was determined that the sinterability of Ti-30vol%Mg saturates at a sintering pressure of approximately 50 MPa. Moreover, our immersion tests in physiological saline underscore the profound significance of our findings. Ti-30vol%Mg maintained compressive strength above that of cortical bone for 6-to-10 days, with mechanical integrity improving under higher sintering pressures. These findings mark a significant leap towards the development of Ti-Mg composite biomaterials with tailored mechanical properties, thereby enhancing biocompatibility and osseointegration for a wide range of biomedical applications.

Compressive Performance of the PVC Foam Materials used as Sandwich Panel Core

PVC foam materials are preferred in many engineering applications because of their lightweight nature and strength/weight ratio. They are mainly used as the core material in the middle of sandwich panels with improved flexural rigidity. The mechanical performances of sandwich panels, such as flexural load-deflection, core shear load, core shear failure load, and indentation failure load, directly depend on the mechanical properties of the core material. In this study, compression tests of AIREX C70 PVC foams with three different densities were performed. The elastic modulus and strength results obtained from the compression tests were compared with the mechanical properties provided in the dataset supplied by the material manufacturer. The core yield loads of a concept sandwich panel were then obtained using the compression mechanical properties of the core, which were obtained from datasets and experimental results. When the core yield loads obtained using both data were compared, it was revealed that the load obtained using the dataset data was 23% inaccurate. Thus, the study explained why compression tests are necessary even though the mechanical properties of PVC foam materials are known in the datasheet.

Ultrashort echo time magnetic resonance elastography for quantification of the mechanical properties of short T2 tissues via optimal control-based radiofrequency pulses.

The aim of the current study is to demonstrate the feasibility of radiofrequency (RF) pulses generated via an optimal control (OC) algorithm to perform magnetic resonance elastography (MRE) and quantify the mechanical properties of materials with very short transverse relaxation times (T2 < 5 ms) for the first time. OC theory applied to MRE provides RF pulses that bring isochromats from the equilibrium state to a fixed target state, which corresponds to the phase pattern of a conventional MRE acquisition. Such RF pulses applied with a constant gradient allow to simultaneously perform slice selection and motion encoding in the slice direction. Unlike conventional MRE, no additional motion-encoding gradients (MEGs) are needed, enabling shorter echo times. OC pulses were implemented both in turbo spin echo (OC rapid acquisition with refocused echoes [RARE]) and ultrashort echo time (OC UTE) sequences to compare their motion-encoding efficiency with the conventional MEG encoding (classical MEG MRE). MRE experiments were carried out on agar phantoms with very short T2 values and on an ex vivo bovine tendon. Magnitude images, wave field images, phase-to-noise ratio (PNR), and shear storage modulus maps were compared between OC RARE, OC UTE, and classical MEG MRE in samples with different T2 values. Shear storage modulus values of the agar phantoms were in agreement with values found in the literature, and that of the bovine tendon was corroborated with rheometry measurements. Only the OC sequences could encode motion in very short T2 samples, and only OC UTE sequences yielded magnitude images enabling proper visualization of short T2 samples and tissues. The OC UTE sequence produced the best PNRs, demonstrating its ability to perform anatomical and mechanical characterization. Its success warrants in vivo confirmation in further studies.

Structural integrity assessment and optimization of control surfaces in coaxial unmanned aerial vehicles: A case study of a micro coaxial UAV

Unmanned aerial vehicles (UAVs) play a pivotal role in modern society which requires lightweight yet robust structures to fulfill increasingly complex tasks. This study presents a cost-effective prototyping approach to assess the structural integrity of control surfaces within the innovative Coaxial Unmanned Aerial Vehicle version 3.0 (MCR UAV v3.0). Integrating a hybrid design with coaxial propulsion for vertical stabilization and yaw control, the MCR UAV v3.0 incorporates control surfaces (ailerons) to manage roll and pitch movements during flight. The design process relies on a comprehensive understanding of material mechanical properties, particularly polylactic acid (PLA) specimens fabricated via fused deposition modeling (FDM) with varying infill percentages and building angles. A novel fluid-structure interaction method is developed in order to analyze four control surface topologies: concave (A), optimized concave (B), convex (C), and optimized convex (D). Findings reveal that the optimized design significantly improves stress distribution in the fuselage-control surface interface while reducing aileron weight by approximately 70%. Subsequently, a functional UAV prototype incorporating optimized ailerons is manufactured. Flight tests affirm the efficacy of the ailerons in controlling roll and pitch motions. This work significantly contributes by introducing the novel MCR UAV v3.0 and conducting a comprehensive assessment of fuselage-control surface structural stability, offering insights into enhanced UAV design and performance for diverse applications.

Progress on mechanical and tribological characterization of 2D materials by AFM force spectroscopy

AbstractTwo-dimensional (2D) materials are potential candidates for electronic devices due to their unique structures and exceptional physical properties, making them a focal point in nanotechnology research. Accurate assessment of the mechanical and tribological properties of 2D materials is imperative to fully exploit their potential across diverse applications. However, their nanoscale thickness and planar nature pose significant challenges in testing and characterizing their mechanical properties. Among the in situ characterization techniques, atomic force microscopy (AFM) has gained widespread applications in exploring the mechanical behaviour of nanomaterials, because of the easy measurement capability of nano force and displacement from the AFM tips. Specifically, AFM-based force spectroscopy is a common approach for studying the mechanical and tribological properties of 2D materials. This review comprehensively details the methods based on normal force spectroscopy, which are utilized to test and characterize the elastic and fracture properties, adhesion, and fatigue of 2D materials. Additionally, the methods using lateral force spectroscopy can characterize the interfacial properties of 2D materials, including surface friction of 2D materials, shear behaviour of interlayers as well as nanoflake-substrate interfaces. The influence of various factors, such as testing methods, external environments, and the properties of test samples, on the measured mechanical properties is also addressed. In the end, the current challenges and issues in AFM-based measurements of mechanical and tribological properties of 2D materials are discussed, which identifies the trend in the combination of multiple methods concerning the future development of the in situ testing techniques.

REVIEW: AN EXPERIMENTAL STUDY ON EFFECT OF NANO MATERIALS ON STRENGTH OF CONCRETE AND PLANE STRESS ANALYSIS USING ANSYS SOFTWARE

These days, making efficient and cost-effective use of resources has taken precedence. The main ingredient in concrete, cement has been under criticism in recent years for the quantity of CO2 released during production. Although cement has better mechanical properties, it hasn't been able to live up to the expectations in terms of durability. Owing to cement's shortcomings, scientists started looking into additives that would enhance concrete's qualities while also making it stronger and lighter. Fly ash, silica fume, and other micro particles were added to cementitious materials to improve their compactness, strength, and durability. These additives were also selected because they are eco-friendly by products of industrial waste that may be handled ethically. Fly ash has significant disadvantages because it is not good for initial strength increase and setting time. Because silica fume affects cementitious material performance, researchers have recently become interested in combining it with ceramic waste and rice husk ash. A more effective way to utilize rice husk ash, a by-product of rice cultivation, would be to replace 10% to 15% of cement. Studies have shown improvements in the durability performance of recycled ceramic waste concrete and rice husk ash concrete. There are issues since the RHA production process is quite time-consuming. With the discovery of nano-particles (NP) smaller than 100 nm, researchers have advanced the field of nanotechnology to new levels. The mechanical properties of many materials, including polymers and cementitious materials, can be enhanced by NP. NP is also helpful in the fields of food, engineering, and medicine. This led researchers to investigate the effects of nano-silica (NS) on concrete in further detail. Nano materials can improve the compressive strength and ductility of concrete. In this project an effort will be made to increase the compressive strength of concrete using Nano materials and waste product like GGBS. Also plane stress analysis of concrete cubes and cylinders is to be done using Ansys Software to find deformation, principal stresses and shear stresses. Keywords: Nano –Silica, Nano Titanium dioxide, Ansys, GGBS, Compressive strength

Alternative concrete aggregates - Review of physical and mechanical properties and successful applications

Concrete is one of the most widely used construction materials, yet its production is associated with significant environmental impacts. One approach to mitigate such impacts is to use alternative aggregates. However, the limited knowledge about the availability and benefits of these unconventional materials, as well as concerns about their quality and performance, have hindered their adoption. This paper aims to analyse the potential benefits and limitations of using alternative aggregates in concrete by reviewing examples from three primary sources: construction and demolition waste (CDW), end-of-life materials (i.e., tyre rubber, glass, and plastic), and forest and agricultural waste (i.e., rice husk, wood, and hemp). First, the main sources and treatment needs are analysed. Then, a comprehensive macro analysis is provided on the physical and mechanical properties of concrete materials, discussing the results in terms of the aggregate nature and substitution ranges. The collected experimental data are also compared with estimations based on different models from two published codes, suggesting that more specific design-oriented models need to be developed to relate concrete's physical and mechanical properties using different waste-type aggregate replacements. Selected data analyses are presented to help the readers obtain the optimum content for specific structural or non-structural applications. Examples of successful application of alternative aggregates in construction projects and products are also provided and discussed.

Poisson's Ratio Prediction of Injection Molded Thermoplastics Using Differential Scanning Calorimetry.

In the development of thermoplastic products, it is necessary to conduct the necessary mechanical tests and evaluate the reliability of thermoplastics in each case, because the mechanical properties of the same material vary depending on the molding process conditions and product shape. In order to build a sustainable society, it is expected that the evaluation of the mechanical properties of thermoplastics, which are resource and energy saving, will be required. In this paper, the glass transition temperature and melting point of injection-molded thermoplastics were evaluated by differential scanning calorimetry, and the correlation between Poisson's ratio and free volume was obtained by applying the theory proposed by Flory et al. A certain correlation was found between the Poisson's ratio of polymers and the change in free volume determined by the glass transition temperature. It is also clear that this relationship can be approximated by orders of magnitude. The Poisson's ratio of the core layer tended to be smaller than that of the skin layer. It has also been found that there is a negative correlation between the Young's modulus and the free volume of the polymer material.

Mechanical properties of composite materials with low-covered polyrotaxane and plasma-surface-modified hexagonal boron nitride

An effective method for fabricating flexible materials containing thermally conductive fillers, such as hexagonal boron nitride (hBN), utilizes plasma surface modification and polyrotaxane (PR) with movable cross-linking points. This study demonstrated that lowering the coverage rates of PR composites increased the mobility of the cross-linking points. Plasma surface modification improved the dispersion of hBN and enabled homogeneous deformation of the PR composites owing to movable cross-linking points. Studying the deformation with a model including a finite extension effect indicated that the sliding range in the low-covered PR composites was extended compared to that in the high-covered PR composites, resulting in a smaller Young’s modulus, longer extension, and higher toughness.

An open-source membrane stretcher for simultaneous mechanical and structural characterizations of soft materials and biological tissues

The ability to simultaneously measure material mechanics and structure is central for understanding their nonlinear relationship that underlies the mechanical properties of materials, such as hysteresis, strain-stiffening and -softening, and plasticity. This experimental capability is also critical in biomechanics and mechanobiology research, as it enables direct characterizations of the intricate interplay between cellular responses and tissue mechanics. Stretching devices developed over the past few decades, however, do not often allow simultaneous measurements of the structural and mechanical responses of the sample. In this work, we introduce an open-source stretching system that can apply uniaxial strain at a submicron resolution, report the tensile force response of the sample, and be mounted on an inverted microscope for real-time imaging. Our system consists of a pair of stepper-based linear motors that stretch the sample symmetrically, a force transducer that records the sample tensile force, and an optically clear sample holder that allows for high-magnification microscopy. Using polymer samples and cellular specimens, we characterized the motion control accuracy, force measurement robustness, and microscopy compatibility of our stretching system. We envision that this uniaxial stretching system will be a valuable tool for characterizing soft and living materials.

The effect of temperature on monocrystalline Si nanoindentation side effects: A molecular dynamics study

Monocrystalline Si materials has been widely used in the fields of micro-electro-mechanical systems and electronic chips. At the micro and nanoscale, there are differences in the mechanical properties at the workpiece side compared to its interior. Meanwhile, temperature also has a significant impact on the mechanical properties of materials. In this paper, to analyze the effect of the temperature on the nanoindentation side effect of monocrystalline Si, a series of molecular dynamics (MD) simulations of nanoindentation are performed under six different temperatures. The simulation results show that the plastic deformation behavior, indentation force, internal stress, and the Internal defects are closely related to the temperature in nanoindentation. This work attributes a better understanding of the temperature effect on the nanoindentation side effect of the monocrystalline Si materials.

Verification of the Laser Powder Bed Fusion Performance of 2024 Aluminum Alloys Modified Using Nano-LaB6.

The application of 2024 aluminum alloy (comprising aluminum, copper, and magnesium) in the aerospace industry is extensive, particularly in the manufacture of seats. However, this alloy faces challenges during laser powder bed fusion (PBF-LB/M) processing, which often leads to solidification and cracking issues. To address these challenges, LaB6 nanoparticles have been investigated as potential grain refiners. This study systematically examined the impact of adding different amounts of LaB6 nanoparticles (ranging from 0.0 to 1.0 wt.%) on the microstructure, phase composition, grain size, and mechanical properties of the composite material. The results demonstrate that the addition of 0.5 wt.% LaB6 significantly reduces the average grain size from 10.3 μm to 9 μm, leading to a significant grain refinement effect. Furthermore, the tensile strength and fracture strain of the LaB6-modified A2024 alloy reach 251 ± 2 MPa and 1.58 ± 0.12%, respectively. These findings indicate that the addition of appropriate amounts of LaB6 nanoparticles can effectively refine the grains of 2024 aluminum alloy, thereby enhancing its mechanical properties. This discovery provides important support for the broader application of 2024 aluminum alloy in the aerospace industry and other high-performance fields.

Recycling and reuse of waste banded iron formation as fine aggregate in the production of lightweight foamed concrete: Fresh-state, mechanical, thermal, microstructure and durability properties assessment

This study investigates the possibility of using BIFs as sustainable fine aggregates to produce lightweight foam concrete (LWFC) by replacing sand with 5, 10, 15, 20, and 25 % banded iron formations (BIFs). The fresh concrete properties, such as slump flow, density, and setting time, as well as its mechanical properties, including compressive strength, splitting strength, and flexural strength, were investigated. The thermal conductivity, specific heat, porosity, gas permeability, pore distribution, and sorptivity were measured to determine durability and thermal performance. Microstructural analysis of the mixes was performed using SEM, energy-dispersive X-ray spectroscopy (EDX), and mapping. The results recommended a 10 % replacement ratio to achieve an increased compressive strength ratio of 55.88 % compared to the control mix at 7 days (d). The strength at later ages increased compared to that of the control mix by 33.9 %, 30 %, 42.48 %, and 42.4 % at 14, 28, 56, and 180 d, respectively. In addition, the flexure increased by 42.7 % at 7 d, 49.6 % at 14 d, and 45.6 % at 28 d compared to the control mix. In addition, the UPV also increased gradually from 2757 to 3699 km/s with increase in BIFs content. Furthermore, the porosity decreased at 7 d, 14 d, 28 d, and 90 d. Moreover, chloride penetration decreased by 2.5 %, where an improvement in thermal conductivity was achieved with BIFs to 0.342 W/mK compared to that of the control mix. In addition, a reduction in the specific heat of the material from 1042 J/kg K to 1007 J/kg K was observed. SEM showed a better arrangement of pores when BIFs were utilized compared with that of control mix without BIFs. In conclusion, the incorporation of waste BIFs as fine aggregates in lightweight foam concrete demonstrates a promising potential for enhancing the mechanical and thermal properties of construction materials, paving the way for durable building materials in the construction industry.

Toughness Evolution of Flax-Fiber-Reinforced Composites under Repeated Salt Fog-Dry Aging Cycles.

This research examined the response of flax-fiber-reinforced composites (FFRCs) to simulated outdoor conditions involving repeated exposure to salt fog and drying. The study investigated the effect of cycles on the toughness of the FFRCs. To achieve this, the composites were exposed to humidity (salt fog) for 10 days, followed by 18 days of drying in cycles. A total of up to 3 cycles, each lasting 4 weeks, were conducted over a 12-week period. Throughout this process, changes in the material's weight, water absorption, and mechanical properties were monitored by water uptake and three-point bending tests. The findings revealed the significant impact of these humid-dry cycles on the mechanical response of the FFRCs. When exposed to humid environments without drying, the composite's toughness increased significantly, due to a weakening effect more pronounced for stiffness, with strength reductions of about 20%. However, subsequent drying partially restored the material's performance. After 18 days of drying, the composite regained most of its initial performance.

Dynamic fracture of hen’s eggshell under impact loading: A combined experimental, theoretical and numerical study

As a typical biological material from nature, the eggshell possesses a smooth macroscale appearance with various curvatures and hierarchical microscale morphology, which contribute to the superior mechanical properties of this lightweight brittle material. The research on the biomimicry of the eggshell has attracted much attention. For both biological reproduction and the poultry industry, the dynamic fracture of the eggshell is a key issue and quite complex due to the thin-walled structure of the eggshell and the strong fluid-solid interaction between the eggshell and its content. In our work, the dynamic fracture of hen’s eggshells under the impact and the influence of the content are thoroughly investigated experimentally, numerically, and theoretically. The responses of eggshells are similar no matter what the content is and exhibit four stages under the same input kinetic energy. It is found that there are two self-protection mechanisms of an egg when subjected to impact, which serves as significant inspiration for the design of novel structures. Under the influence of curvatures, the non-simultaneous propagation of cracks in the thickness direction induces the hinge pattern and the spider-web-like crack network. In addition to its role in biology, the viscosity of the albumen can provide resistance to damage and protect the eggshell during the impact. It is suggested that exterior curvature and interior content can be optimized to absorb dynamic impact energy when designing a thin-walled structure.

Shear Strengthening of Stone Masonry Walls Using Textile-Reinforced Sarooj Mortar

Most historical buildings and structures in Oman were built using unreinforced stone masonry. These structures have deteriorated due to the aging of materials, environmental degradation, and lack of maintenance. This research investigates the physical, chemical, and mechanical properties of the local building materials. It also presents the findings of an experimental study on the in-plane shear effectiveness of a modern strengthening technique applied to existing stone masonry walls. The technique consists of the application of a textile-reinforced mortar (TRM) on one or two faces of the walls. Shear loading tests of full-scale masonry samples (1000 mm width, 1000 mm height, and 350 mm depth) were carried out on one unreinforced specimen and six different cases of reinforced specimens. The performances of the unreinforced and reinforced specimens were analyzed and compared. We found that strengthened specimens can resist in-plane shear stresses 1.5–2.1 times greater than those of the unreinforced specimen; moreover, they demonstrate ductility rather than sudden failure, due to the presence of fiberglass and basalt meshes, which restrict the opening of cracks.

Constitutive model of die-cast light-alloy thin-walled parts considering geometric imperfection

Replacing steel with aluminum and shifting from forging to casting have become important means of automotive lightweight. Large integrated die-cast parts are gaining popularity among original equipment manufacturers. Engineers often ignore the influence of geometric imperfection on mechanical properties when simulating strength of thin-walled parts, therefore causing a bias. To investigate the relation between geometric imperfections and mechanical properties of die-cast light alloy, quasi-static tensile tests are conducted on the specimens of JDA1b aluminum alloy and JDM1 magnesium alloy. The specimens exhibit varying geometric imperfection factors (from 0 to 90 %) achieved by introducing circular holes with different diameters. The results show that the strength and elongation of JDA1b and JDM1 alloys decrease significantly as the geometric defect factor increases. Even small holes can significantly affect tensile strength. A constitutive model that incorporates the stress limit value and geometric imperfection factors is proposed, which has higher accuracy than the J–C model. Experiments and simulations on a die-cast thin-walled part validated the idea and proposed constitutive model. These findings provide essential insights into the influence of structural holes on the mechanical properties of die-cast light-alloy materials. The proposed constitutive model offers high-precision computational support for simulating the mechanical performance of parts.

The impact of nanoparticle surface topography on the interfacial mechanical behavior and microstructure of polyvinyl alcohol composites

The interfacial mechanical strength between nanoparticle and matrix is one of the key factors affecting the mechanical properties of nanoparticulate-polymer composites. Based on the structural composition of a nanoscale iron particle/polyvinyl alcohol composite, this study employed molecular dynamics simulations to investigate the stress-response behavior and microstructural evolution of Fe/PVA/Fe interface models with different surface morphologies under both tensile and shear deformations. The results indicate that when the particle surfaces exhibit different rough structures, the interfacial tensile strength significantly increases with the absolute value of the interfacial binding energy. The order of tensile strength is Type-cube > Type-pyramid > Type-plane. Furthermore, during the shearing process, the protruding structures on the particle surfaces significantly hinder the deformation and unfolding of the matrix molecular chains. As the volume of the protruding structures increases, the interfacial shear strength decreases markedly. The research findings illuminate the mechanisms by which nanoparticle surface morphology at the microscopic molecular scale influences the mechanical properties of nanoparticle-polymer composite materials. These discoveries aid in selecting nanoparticle fillers that enhance the mechanical performance of polymer nanocomposites to a measurable extent.

Nonlinear resonant responses of a novel FGM sandwich cylindrical shell structure for supersonic flight vehicles based on 1:1 internal resonance between conjugate modes

A new design scheme for the functionally graded material (FGM) sandwich cylindrical shell structure made of ceramic-FGM-carbon fiber composites is proposed, which is geared towards supersonic flight vehicles and has high specific stiffness and high-temperature resistance. We focus on analyzing the nonlinear resonant responses of the novel FGM sandwich cylindrical shell subjected to external excitation and aerodynamic force. Firstly, the mechanical properties of the novel FGM sandwich material are calculated, and then the nonlinear dynamic model of the FGM sandwich cylindrical shell is established based on the first order shear deformation theory (FSDT) and Hamilton's principle. Due to the axisymmetric property of the cylindrical shell, a 1:1 internal resonance between the driven and companion modes always exists in the perfect cylindrical shell. Taking this into consideration, the nonlinear resonant response problems of the FGM sandwich cylindrical shell are numerically simulated by combining the Galerkin method and the pseudo-arc length continuation method. Finally, the effects of complex parameters such as external excitation, aerodynamic force, aspect ratio, gradient index, and skin-core-skin ratio on the nonlinear resonant responses of the FGM sandwich cylindrical shell are investigated.

Hardening properties and microstructure of 3D printed engineered cementitious composites based on limestone calcined clay cement

Comparison of three-dimensional (3D) printing and cast methods on the mechanical properties of cementitious materials is the basis for intelligent construction development. To achieve this, a series of experiments including the uniaxial tensile, compressive, flexural and interlayer bonding tests of mould-cast and 3D printed (3DP) specimens are conducted to investigate the effects of different preparation technologies on the microstructure and hardening properties of limestone calcined clay cement (LC3) based engineered cementitious composites (ECC). Results indicate that the tensile strength and strain capacity of the printed LC3-ECC decrease by 16.6%–22.7 % and 43.3%–54.6 % compared to the cast specimens, while it still possesses a strain capacity of 2 % and multiple cracking behaviour. The compressive and flexural properties of the printed LC3-ECC both show significant anisotropy, the maximum values of which are observed in the Z- and Y- directions, respectively. The interlayer bonding strength increases by 54.3%–91.9 % at 28 d compared to that at 7 d due to the hydration of LC3. The pore structure of the printed LC3-ECC is denser than that of the cast LC3-ECC, with more regular arrangement and finer size of pores. The macro-micro properties correlation analysis proves the better comprehensive performance of printed LC3-ECC relative to casted LC3-ECC, as well as reveals the relationship between pore structure and anisotropy. In terms of material sustainability, 3DP-LC3-ECC has a significant reduction in energy and carbon emissions compared to typical M45-ECC, contributing to the environmental development.