Low-voltage Excitation Research Articles

An Adaptive Noise Reduction Method for High Temperature and Low Voltage Electromagnetic Detection Signals Based on SVMD Combined with ICEEMDAN.

In view of the low signal-to-noise ratio (SNR) of shear wave electromagnetic acoustic transducers (EMAT) in the detection of high-temperature equipment, the use of low excitation voltage (LEV) further deteriorates the detection results, resulting in the echo signal containing defects being drowned in noise. For the extraction of the EMAT signal, an adaptive noise reduction method is proposed. Firstly, the minimum envelope entropy is taken as the fitness function for the Harris Hawks Optimizer (HHO), and the optimal successive variational mode decomposition (SVMD) balance parameter is searched by HHO adaptive iteration to decompose LEV EMAT signals at high temperatures. Then the filter is carried out according to the excitation center frequency and correlation coefficient threshold function. Then, improved complete ensemble empirical mode decomposition with adaptive noise (ICEEMDAN) is used to decompose the filtered signal and combine the kurtosis factor to select the appropriate intrinsic mode functions. Finally, the signal is extracted by the Hilbert transform. In order to verify the effectiveness of the method, it is applied to the low-voltage detection of 40Cr from 25 °C to 700 °C. The results show that the method not only suppresses the background noise and clutter noise but also significantly improves the SNR of EMAT signals, and most importantly, it is able to detect and extract the 2 mm small defects from the echo signals. It has great application prospects and value in the LEV detection of high-temperature equipment.

Investigation of Chemiresisitive Electronic Nose for the Analysis of Multiple Analytes Using Pattern Recognition Algorithm

The multiple analytes produced during the operation of nuclear facilities are required to monitor the smooth operation of the plant in the environment of high temperature and radioactivity in real time. A chemiresisitive electronic nose was investigated and developed to analyze the multiple analytes generated in the nuclear reactor/allied facilities. An electronic nose consists of chemiresisitive sensor, array, housing, hardware, software, and pattern recognition algorithm. The sensor and array of different semiconductor metal oxides were prepared, processed, and developed to sense the multiple analytes. The hardware and data acquisition software (DAS) was designed and developed to acquire the dynamic responses from the array of four sensors. The hardware provides a low excitation voltage for measurement of the dynamic response of four sensors towards the improvement of the life of the sensor. The various experiments were conducted with multiple analytes at different temperatures to study the analysis of analytes. The performance of the hardware and DAS were tested and evaluated with the sensor array responses towards three analytes, viz., hydrogen (H2), formaldehyde (HCHO), and hydrazine (NH2NH2). Different features evaluated from the response traces were processed to teach the instrument using pattern recognition algorithms. The training and real-time testing of the sensor array realized the qualitative discrimination and quantitative estimation of the analytes.

Ultrastable Luminol-OH--(Ni-WOx-CNT) ECL System with High Strength and Its Applications in Sensing.

In traditional luminol electrochemiluminescence (ECL) systems, hydrogen peroxide (H2O2) and dissolved oxygen (DO) are the commonly used coreactants to generate reactive oxygen species (ROS) for ECL emission. However, the self-decomposition of hydrogen peroxide and the limited solubility and content of oxygen in solution undoubtedly restrict the luminescence efficiency and stability of the luminol ECL system. Inspired by the ROS-mediated ECL mechanism, we pioneered hydroxide ion as an advanced luminol ECL coreactant using nickel-doped and carbon nanotube-modified tungsten oxide (Ni-WOx-CNT) as the coreactant accelerator. Owing to the excellent catalytic activity of Ni-WOx-CNT, amounts of ROS were generated from OH- at a low excitation voltage, which subsequently reacted with luminol anion radicals and triggered intense ECL signals. Experiments confirmed an impressive ECL behavior in terms of high luminescent intensity (85,563 a.u.) and super stability over 1300 consecutive tests; both are superior to those recently reported luminol-H2O2 and luminol-DO systems with smaller ECL intensities and consecutive tests less than 25 times. To validate the feasibility and versatility of the developed system in sensor, traditional three-electrodes system and closed bipolar electrodes system with various sensing strategies of direct oxidation, "gate-effect" of molecularly imprinted polymer, immune reaction, and enzyme-catalyzed reaction were proposed to monitor uric acid (UA), C-reactive protein (CRP), immunoglobulin G (IgG), and glucose (Glu). The superior sensing performances confirmed the great application potential of the developed ROS-mediated ECL system.

A New Denoising Method VSCE for High-Temperature Shear Wave Electromagnetic Ultrasonic Defect Detection at a Low Excitation Voltage

A New Denoising Method VSCE for High-Temperature Shear Wave Electromagnetic Ultrasonic Defect Detection at a Low Excitation Voltage

Nanoelectrical monitoring the nonvolatile behavior of VO2 under multi-field stimulate by conductive atomic force microscopy

The ability to control the metal–insulator phase transition is crucial for future neuromorphic and memristive technologies. The key goal of this implementation is to understand and control the nanoscale mechanisms that support these two fundamental switching modalities (volatile and non-volatile states). Here, by adjusting the temperature (60 °C) close to the metal–insulator transition temperature, external application of low voltage (1 V) and laser excitation (18.6 mw · cm−2) can complete the metal–insulator transition of vanadium dioxide (VO2). The nonvolatile behavior of the VO2 devices was nanoelectrically monitored using conductive atomic force microscopy (C-AFM). Using this technique, we were able to reversibly transform the local switching response from volatile to nonvolatile, providing a unique approach for nanoelectrical monitoring in phase transition materials.

Vortex-Enhanced Microfluidic Chip for Efficient Mixing and Particle Capturing Combining Acoustics with Inertia.

Vortex-based microfluidics has received significant attention for its unique characteristics of high efficiency, flexible control, and label-free properties for the past decades. Herein, we present a vortex-based acousto-inertial chip that allows both fluid and particle manipulation within a significantly wider flow range and lower excitation voltage. Composed of contraction-expansion array structures and vibrating microstructures combined with bubbles and sharp edges, such a configuration results in more vigorous vortical fluid motions. The overall improvement in device performance comes from the synergistic effect of acoustics and inertia, as well as the positive feedback loop formed by vibrating bubbles and sharp edges. We characterize flow patterns in the microchannels by fluorescence particle tracer experiments and uncover single- and double-vortex modes over a range of sample flow rates and excitation voltages. On this basis, the ability of rapid and efficient sample homogenization up to a flow rate of 200 μL/min under an excitation voltage of 15 Vpp is verified by a two-fluid fluorescence mixing experiment. Moreover, the recirculation motion of particles in microvortices is investigated by using a high-speed imaging system. We also quantitatively measure the particle velocity variation on the trajectory and illustrate the capturing mechanism, which results from the interaction of the microvortices, particle dynamics, and composite microstructure perturbations. Further utilizing the shear forces derived by microvortices, our acousto-inertial chip is demonstrated to lysis red blood cells (RBCs) in a continuous, reagent-free manner. The high controllability and multifunction of this technology allow for the development of multistep miniaturized "lab-on-chip" analytical systems, which could significantly broaden the application of microvortex technology in biological, chemical, and clinical applications.

Wearable Ultrasound System Using Low-Voltage Time Delay Spectrometry for Dynamic Tissue Imaging.

Wearable ultrasound is emerging as a new paradigm of real-time imaging in freely moving humans and has wide applications from cardiovascular health monitoring to human gesture recognition. However, current wearable ultrasound devices have typically employed pulse-echo imaging which requires high excitation voltages and sampling rates, posing safety risks, and requiring specialized hardware. Our objective was to develop and evaluate a wearable ultrasound system based on time delay spectrometry (TDS) that utilizes low-voltage excitation and significantly simplified instrumentation. We developed a TDS-based ultrasound system that utilizes continuous, frequency-modulated sweeps at low excitation voltages. By mixing the transmit and receive signals, the system digitizes the ultrasound signal at audio frequency (kHz) sampling rates. Wearable ultrasound transducers were developed, and the system was characterized in terms of imaging performance, acoustic output, thermal characteristics, and applications in musculoskeletal imaging. The prototype TDS system is capable of imaging up to 6cm of depth with signal-to-noise ratio of up to 42dB at a spatial resolution of 0.33mm. Acoustic and thermal radiation measurements were within clinically safe limits for continuous ultrasound imaging. We demonstrated the ability to use a 4-channel wearable system for dynamic imaging of muscle activity. We developed a wearable ultrasound imaging system using TDS to mitigate challenges with pulse echo-based wearable ultrasound imaging systems. Our device is capable of high-resolution, dynamic imaging of deep-seated tissue structures and is safe for long-term use. This work paves the way for low-voltage wearable ultrasound imaging devices with significantly reduced hardware complexity.

Single-Bit Reception With Coded Excitation for Lightweight Advanced Ultrasonic Imaging Systems.

The demand for an efficient and reliable ultrasonic phased array imaging system is not unique to a single industry. Today's imaging systems can be enhanced in a number of areas including; improving scanning and processing times, reducing data storage requirements, simplifying hardware, and prolonging probe lifespan. In this work, it is shown that by combining the use of coded excitation with single-bit data capture, a number of these areas can be improved. Despite using single-bit receive data, resolution can be recovered through the coded excitation pulse compression process, and shown to produce high signal-to-noise ratio (SNR) images of phase coherence imaging (PCI) and total focusing method (TFM) of tip diffraction in a carbon steel sample. Comparison with conventional single-cycle transmission pulses has shown that little imaging performance degradation is seen despite a significant reduction in data resolution and size. This has also been shown to be effective at low excitation voltages with gain compensation due to the obsolescence of signal saturation concerns when considering single-bit receive data. The ability to compute high-resolution ultrasonic images from low-resolution input data at low transmission voltages has important implications for data compression, acquisition and imaging performance, operator safety, and hardware simplification for ultrasonic imaging systems across industrial and medical fields.

Efficient Zero-Sequence Impedance Measurement in Autotransformers Using Low-Voltage Excitation

In accordance with the IEEE standard, the zero-sequence impedance test of transformers necessitates an open or short circuit test on the high-voltage side winding. Power source excitation is applied to the high-voltage test winding using a high-capacity test power supply. To circumvent the need for a large-capacity, high-voltage test power supply in field tests, this paper proposes a method for measuring zero-sequence impedance in autotransformers based on low-voltage excitation and disconnection testing. By applying a three-phase power supply to the lowest voltage side of the autotransformer and creating a disconnection condition, an unbalanced test scenario is established. Subsequently, the composite sequence network equivalent circuit for one-phase and two-phase disconnections between the high-voltage side and the low-voltage side of the transformer is formulated. Calculation formulas for the zero-sequence impedance of the autotransformer under various conditions are derived. The accuracy of the zero-sequence impedance is verified using MATLAB/Simulink simulation software 2018b, evaluating double-winding and three-winding autotransformers in breaking tests under different connection modes. The error is found to be less than 3%. The results of this study affirm the high accuracy of the proposed method.

Electro‐Driven, Predefined Carbon Nanotube‐Based Phase Change Composite as a Lifting‐Jack

AbstractShape change materials or actuators that are capable of shrinking, bending or rotation under external stimuli (especially, by electricity), have attracted tremendous research interest in past years. Controlled shape change with large output capacity under low excitation voltage remains a challenging task in this field. Here, an electro‐driven carbon nanotube sponge/paraffin wax bulk composite (CS@PW) that can perform various shape change functions such as, in particular, jacking and lifting heavy objects (up to 668.3 times of composite weight) under lower voltages (4–8 V) with fast response and high reversibility is presented. This unique and superior jacking performance is attributed to the predefined original CS shape, the deformability and resilience derived from 3D porous CS@PW, and efficient Joule heat transfer from conductive CS to the coaxially wrapped PW layer; the latter, by reversible phase change solidification/melting, can fix or release carbon nanotube network to enable controlled fixation/motion. Additional advantages include hydrophobicity, anti‐leakage, wide operating temperature, and diverse reversible shape change modes based on CS@PW and commercial polyethylene tapes, are also demonstrated. The designed electro‐driven nanocomposites, combining resilient carbon nanotube networks with low‐cost organic phase‐change material, have wide applications in areas such as robust artificial muscles, intelligent morphing, and energy management.

Research on Short-Circuit Impedance Analysis Method of Auto-transformer for Side Column Voltage Regulation

In order to realize the accurate analysis of the impedance of transformers with complex connection relations, this paper derives the impedance calculation method of low-voltage excitation side column linear voltage regulating autotransformer by using the power method. The transformer network with different taps is analyzed, and the calculation formulas of transformer HV-MV impedance, HV-LV impedance and MV-LV impedance are derived. The analysis is simplified to the solution of concentric column coil impedance and magnetic potential of each coil. By comparing the calculated data of actual products with the measured data, the calculation deviation of this method is controlled within 2.03%; By using the finite element method, the impedance of the transformer with the measures to control the magnetic shielding is analyzed and calculated. By comparing the impedance of the transformer with different measures, it can be confirmed that the magnetic leakage measures have an impact on the impedance of the transformer.

Deep learning for exploring ultra-thin ferroelectrics with highly improved sensitivity of piezoresponse force microscopy

Hafnium oxide-based ferroelectrics have been extensively studied because of their existing ferroelectricity, even in ultra-thin film form. However, studying the weak response from ultra-thin film requires improved measurement sensitivity. In general, resonance-enhanced piezoresponse force microscopy (PFM) has been used to characterize ferroelectricity by fitting a simple harmonic oscillation model with the resonance spectrum. However, an iterative approach, such as traditional least squares (LS) fitting, is sensitive to noise and can result in the misunderstanding of weak responses. In this study, we developed the deep neural network (DNN) hybrid with deep denoising autoencoder (DDA) and principal component analysis (PCA) to extract resonance information. The DDA/PCA-DNN improves the PFM sensitivity down to 0.3 pm, allowing measurement of weak piezoresponse with low excitation voltage in 10-nm-thick Hf0.5Zr0.5O2 thin films. Our hybrid approaches could provide more chances to explore the low piezoresponse of the ultra-thin ferroelectrics and could be applied to other microscopic techniques.

High-performance paper-based humidity sensors with Nafion/AgNWs hybrid electrodes.

In the past decade, the development of medical health and human-computer interfaces has put forward requirements for the non-contact application of flexible electronics. Among them, flexible humidity sensors play an important role in the field of non-contact sensing by virtue of their rapid response to humidity changes. In this paper, a flexible paper-based humidity sensor with high performance was fabricated by embedded Au@AgNWs electrodes on filter paper through spraying and electroplating (EP) methods. Benefitting from the moisture-sensitive properties of the paper and the tight integration of the electrodes into the filter paper, the sensor shows the humidity monitoring range of 33-100% RH, large response value of I/I0 = 1958, excellent linearity of R2 = 0.99662 and hysteresis performance under the low excitation voltage of only DC 1 V. In addition, the good biocompatibility of the paper-based humidity sensor endows it with multifunctional applications for breath detection, non-contact applications and food security monitoring. Easy access to raw materials and convenient preparation methods of this work provide new ideas for the development and commercialization of flexible humidity sensors.

A multi-scale MXene coating method for preparing washable conductive cotton yarn and fabric

An efficient and simple functional processing method for cotton fabric has been always needed to broaden the application field of cotton fiber. Coating small MXene (S-MXene) and large MXene (L-MXene) on cotton yarn or fabric in turn (SL-MXene) is conducive to the construction of conductive path and improve bonding fastness. SL-MXene coated cotton yarn with fineness of 60 s/2 not only has the best washing resistance, but also has good electrical and mechanical properties. Similarly, the cotton woven fabric coated with S L -MXene (SL-MF), has an electromagnetic shielding efficiency of 42.7 dB with conductivity of 2020 S/m and remains at 33.6 dB or 30.9 dB after washing 50 times or annealing at 250 ℃. Besides, excellent conductivity also enables SL-MF to produce different thermal effects under low voltage excitation, and the temperature can be raised to 122 ℃ under 5 V. This work provides a new design method for cotton fiber functionalization processing, which not only improves the bonding fastness between functional filler and cotton fiber, but also maintains the original flexibility and air permeability of cotton fabric. • MXene with different sheet sizes and multi-scale coated SL-MF were prepared. • SL-MF can reach conductivity of 2020 S/m. • SL-MF has an average SE T of 42.7 dB and remains at 33.6 dB after washing 50 times. • The temperature of SL-MF can be raised to 122 ℃ under 5 V voltage.

Variational Wavelet Ensemble Empirical (VWEE) Denoising Method for Electromagnetic Ultrasonic Signal in High-Temperature Environment with Low-Voltage Excitation

Low excitation voltage for an electromagnetic acoustic transducer (EMAT) is necessary for the petrochemical equipment and facilities inspection, which work at high-temperatures, to avoid potential explosion. However, low excitation voltage causes low signal-to-noise ratio (SNR) signals that are difficult to extract features, especially in a high-temperature environment, which causes high noise. In this study, a denoising method called the variational wavelet ensemble empirical (VWEE) method was proposed by combining the advantages of the variational modal decomposition (VMD), wavelet threshold (WT) denoising, and ensemble empirical mode decomposition (EEMD) methods. To validate the VWEE method, EMAT signals obtained in the temperature range of 25 to 700 °C were analyzed. The results show that, compared with VMD, WT and empirical mode decomposition denoising methods, the SNR of proposed method is improved more than two times. The VWEE method dramatically improved the SNR of a high-temperature EMAT signal and enhanced the accuracy of defect echos extraction.

Fabrication and flow rate characterization of a DRIE process based valveless piezoelectric micropump

Micropumps have become one of the major research topics in the field of microfluidics. Different actuators have been used in active micropumps including piezoelectric ones, which convert electrical energy to mechanical energy. In this study, a piezoelectric disc was designed as an actuator and was integrated into a fabricated piezoelectric micropump. Unlike wet etching methods, which is generally used to etch layers of relatively high thickness in the silicon wafer, dry etching was used in this study. Aluminum was used as a mask material during the fabrications-steps, and the fabrication process was shortened with the use of the masking steps. The etching process of the slot, in which the piezoelectric disc was placed, and etching of the inlet/outlet channels were performed simultaneously. Thus, the processing time was significantly shortened. The fabrication of this silicon-based valveless micropump was accomplished by using the DRIE (deep reaction-ion etching) technique, which provided controlled etching. Experiments were conducted on the fabricated micropump with the use of the bulk micromachining technology to deliver the desired pumping action. The leakage and the air entrapment between the consecutive micropump structural layers were satisfactorily eliminated. This micropump is capable of delivering a promising flow rate of 52 (µl min−1) for deionized water, which corresponds to a 150 [Hz] square wave type and a peak-to-peak voltage of 60 (V) Vp -p . No moving mechanical valves were included so that the risks of clogging, reduced performance, and reduced reliability due to wear and fatigue were minimized. Not only gases and liquids but also fluids containing particles could be used as the working fluid for this micropump. The piezoelectric micropump design was optimized to achieve a high time-averaged flow rate (>50 (µl min−1)) with a relatively low excitation voltage (<100 (V) Vp -p ) as opposed to the use of a high excitation voltage.

High-Performance Flexible Heater With Command-Responding Function Attained by Direct Laser Writing on Nomex Paper

Multifunctional flexible electronics have been a hot spot in scientific research and technology development. From the view of practical application, high-performance flexible heating devices with the capability to respond to commands are an urgent need for thermal management. Herein, we propose a strategy for multifunctional integration by assembling two pieces of laser-scribed Nomex paper, thus enabling the combination of heating and sensing modules. On account of the good electrothermal and piezoresistive properties of laser-induced graphene, the device can generate high steady-state temperature with a low voltage excitation and recognize valid commands from users finger to switch between operating states. Besides, the fast and efficient fabrication method entirely based on direct laser writing technology is another unique advantage.

Single-layer piezoelectric transformers with a unique design of polarization topologies

Piezoelectric transformers (PTs) are usually designed in multilayers to obtain a large voltage transformation ratio while reducing the driving voltage. In contrast to the complex manufacturing process of multilayer PTs, this study proposes a single-layer PT that works in planar expansion mode and can achieve different step-up ratios. In this method, the topological structures of the electrode division and the polarization region are designed cleverly in piezoelectric ceramics with different shapes (i.e., rectangle and circle). Therefore, a high voltage output with different step-up ratios can be obtained under low voltage excitation. This study also discusses the working principle of the two shapes of single-layer PTs and deduces the optimal inner and outer radius ratios of circular PTs. Then, combined with three-dimensional modeling, finite element software is utilized for the multi-physics simulation of the PTs. Lastly, single-layer rectangular and circular PTs with different step-up ratios are fabricated. The actual step-up ratios and working efficiencies are measured experimentally. The experimental results are consistent with theoretical analysis and simulation data, thus verifying the feasibility of the single-layer PT design with different step-up ratios.

Inorganic luminescent pigments

Abstract Inorganic luminescent pigments (luminescent materials, luminophores, phosphors) as synthetically generated crystalline compositions absorb energy followed by emission of light with lower energy, respectively, longer wavelengths. The light emission occurs often in the visible spectral range. External energy is necessary to enable luminescent materials to generate light. Luminescent pigments are divided into fluorescent and phosphorescent pigments. This classification goes back to different energy transitions. Emission based on allowed optical transitions, with decay times in the order of µs or faster is defined as fluorescence. Emission with longer decay times is called phosphorescence. The occurrence of fluorescence or phosphorescence as well as the decay time depend on structure and composition of a specific luminophore. There are four luminescence mechanisms discussed for inorganic luminescent materials: center luminescence, charge-transfer luminescence, donor–acceptor pair luminescence, and long-afterglow phosphorescence. The emission of luminescent light can have its origin in different excitation mechanisms such as optical excitation (UV radiation or even visible light), high-voltage or low-voltage electroluminescence and excitation with high energy particles (X-rays, γ-rays). Inorganic luminescent pigments are used mainly in fluorescent lamps, cathode-ray tubes, projection television tubes, plasma display panels, light-emitting diodes (LEDs) and for X-ray and γ-ray detection. The pigment particles are dispersed for the applications in specific binder systems. They are applied in form of thin layers and by means of luminophore/solvent suspensions, containing adhesive agents, on a substrate.

Abstract P782: Bioimpedance as a Means to Quantify Clot Composition and Guide Selection of Thrombectomy Devices

Introduction: Recent studies suggest that suction based thrombectomy leads to better recanalization with RBC-rich clots while stent-retrievers perform better with fibrin-rich clots. The ability to determine real-time histology of clots, in the setting of large vessel occlusion (LVO), could potentially lead to improved recanalization and better clinical outcomes while simultaneously reducing procedural costs. There is an unmet need for technology that would allow for accurate assessment of real-time clot histology in LVOs. Hypothesis: Bioimpedance measurements can be used to predict real-time clot histology. Methods: We constructed an in vitro test bed to measure the bioimpedance of clot analogs with different RBC percentages. The test bed includes a cylindrical chamber with a gold electrode embedded at the bottom. A mixture of human RBCs and plasma was injected into the chamber and coagulation was induced by adding calcium chloride solution. After coagulation, another gold electrode was used to sandwich the clot. Both electrodes were connected to an inductance, capacitance, and resistance (LCR) meter and a low-voltage (10 mV) excitation was sent to the clot at 1 to 201 kHz. We fabricated 5 types of clot analogs by mixing human RBCs and plasma with different RBC percentages (10%, 30%, 50%, 70%, and 90%). Clot types were measured 3 times. The Pearson correlation coefficient was calculated and used to evaluate the relationship between clot bioimpedance and RBC percentage. Results and Conclusions: Clot impedance decreases with the excitation frequency and clots with higher RBC percentages had higher impedance at all excitation frequencies (Fig. 1). The impedance was strongly and positively related to the RBC percentage ( r = .996, p = .0004). By minimizing the electrode size and integrating them into catheters, stents, or wires, such technology could inform clinicians of clot composition and guide device selection for optimum recanalization.