Low Strain Rates Research Articles

The nonlinear analysis of Portevin-Le Chatelier (PLC) effect: An application to medium Mn steel

The instability of plastic flow in medium manganese steel was investigated through uniaxial tensile tests conducted at room temperature across various strain rates. The Portvin-Le Chatelier (PLC) effect was analyzed using statistical methods and a multifractal approach. The findings indicate that the zigzag stress–strain curves associated with instability plastic flow exhibit typical multifractal characteristics. Furthermore, the multifractal analysis quantifies the influence of strain rate and initial phase composition on the instability characteristics of the stress–strain curves. Specifically, it was observed that lower strain rates and austenite content correspond to a chaotic state, whereas higher strain rates and austenite content result in self-organizing critical dynamics. Finally, the underlying physical mechanisms driving these differing modes of behavior are discussed, with a focus on their relationship to strain rate and the initial austenitic phase fraction.

A unified model of tensile and creep deformation for use in niobium alloy materials selection and design for high-temperature applications

There is renewed interest in refractory alloys that possess higher service temperatures than incumbent Ni-based superalloys (e.g., ⪆1100 °C). This study provides a review of the high-temperature constitutive responses of Nb-alloys measured over a wide range of temperatures (≈860 °C < T < ≈1760 °C) and strain rates (≈10–9 s-1< ε˙ < ≈10–1 s-1). Nevertheless, the extant data is sparse and informed materials selection decisions require constitutive expressions to interpolate and reliably extrapolate. The Larson-Miller parameter approach to describe creep-life provides a conservative estimate of material response at the highest temperatures and lowest strain rates, whereas the Sellars-Tegart model describes both steady-state creep and high-temperature tensile test data with a single, universal equation. A minimum flow stress based on the combination of these two models is proposed for design considerations to address the overprediction of strength that can arise from applying one or the other independently. This effort highlights the fact that refractory alloys exhibit strain rate sensitive flow strengths in the temperature range of interest for applications. The roles of alloying, thermomechanical processing, and impurity levels are discussed, and highlight the fact that these advanced Nb-alloys evidence Class 1 (Class A) solute drag controlled creep behavior, except the carbide precipitation strengthened alloy, D-43. In addition, the high-temperature strengths are confirmed to be strongly correlated with alloy melting point.

Strain rate-dependency of thermal infrared radiation of sandstone subjected to dynamic loading: Insights from a lab testing

Rocks are generally deformed and fractured upon various scales of strain rates. Understanding the strain rate effects on the thermal infrared radiation (IR) characteristics of rock materials is crucial for predicting and detecting rock failure. In the study, uniaxial compression experiments were conducted on sandstone samples at different strain rates using an Instron hydraulic servo testing machine and a split Hopkinson pressure bar (SHPB) system. Meanwhile, a thermal infrared camera was utilized to capture and record the changes in the IR temperature on the rock surface. The spatial and temporal evolution of thermograms, IR temperature distribution histograms, and average IR temperature (AIRT) during testing were obtained and analyzed. A quantitative correlation between strain rate and the variation in AIRT (ΔT) was established. Furthermore, the dissipation of heat energy (Q) in the sandstone samples during SHPB tests was estimated. Results indicated that at relatively lower strain rates (ranging from 10−6 to 10−2 s−1), the ΔT of rock sample exhibited slight dependence on strain rate. However, a significant rate sensitivity emerged when the strain rate exceeded a specific threshold (approximately 137.09 s−1 for the tested sandstone). The rate-dependent behavior of ΔT across the investigated range of strain rate (up to 102) can be characterized by an allometric power model. Notably, during SHPB testing, the proportion of Q was negligible despite the pronounced rate dependency of heat energy. The abrupt rises in ΔT and Q under dynamic loading conditions can be elucidated by the increasing occurrence of shear cracks and energy-level jumps stimulated by impact disturbance.

Thermo-mechanical processing characteristics and strain-rate-sensitive degradation properties of Mg-Er-Ni alloys

Hot deformation behavior, the corresponding microstructure evolution, and degradation properties of a weak-textured Mg-Er-Ni alloy containing a high-volume fraction of Ni-LPSO phases, have been investigated. Hot deformation behavior has been carried out in the temperatures range of 370 ∼ 460 °C and strain rates range of 0.001 ∼ 1 s−1. Flow stress-strain curves of high strain rate cases show a continuous increase trend without a steady or a peak stage, while that of low strain rate cases show an obvious dynamic softening after peak stress. Based on flow stress-strain curves, materials constants calculated by an Arrhenius-type constitutive equation, show a high n and Q compared to those of high-volume fraction α-Mg matrix Mg alloys. Optimal processing windows, based on the dynamic material model, is determined as high temperature domains. As for microstructure evolution, a complete recrystallization and dispersive Ni-LPSO fragments for high temperature & low strain rates while a restricted recrystallization and a streamline distribution LPSO phase for high temperature & high strain rates are observed. Varying degrees of continuous dynamic recrystallization, particle induced nucleation mechanism, as well as coordinated deformation of LPSO through kinking and bending account for the strain-rate-dependence hot deformation mechanism. As a result, dispersive Ni-LPSO fragments at low strain rates provide more degradation channels for the α-Mg matrix and thus possess better a degradation rate than the streamlined LPSO at high strain rates.

On the Use of Pad Mechanical Properties as a Proxy for Conditioning Response

A proliferation of pad materials in recent years, coupled with the increasing complexity of process integration and limited resources available for process development, has highlighted the need for a more in depth understanding of conditioning interactions and better predictive tools for process and consumable design. We have previously noted a range of conditioning response as illustrated in Figure 1. As the figure illustrates, on some materials the surface height distribution imparted by the pad conditioner is shifted to the left relative to the exponential signature of the pad native porosity which is used as a reference. Denoted regime 1, these surfaces are characterized by the prevalence of “eyelid” features which obscure the line-of-sight path to the bottoms of the pores. In regime 2, the surface height distribution is more balanced, with a smooth transition between the exponential porosity signature and the conditioning signature. In regime 3, there is an abrupt disconnect between the exponential porosity signature and the conditioner signature. Such surfaces are characterized by deep gouges.We are investigating pad material tensile properties as a proxy to help understand and predict these conditioning responses. Figure 2 illustrates the range of typical tensile behavior for polymers. While Figure 2 invokes temperature as the variable that drives these behaviors, note that strain rate can also drive tensile behavior across this range with high temperature being analogous to low strain rate and vice versa.Figure 3 and Table 1 summarize some results from our testing of IC1000, VP5000, VP6000, IK4250H and IK4350L. We have determined that grooved pad materials at their nominal dimensions are adequate for testing according to ASTM D638: Standard Test Method for Tensile Properties of Plastics. Typical delivered pad thickness is within the specifications for sample thickness, and as long as the grooves are oriented to be substantially parallel with the strain axis (pulling direction) reproducible results can be obtained. A range of properties spanning at least about 2x is observed in these pads.Figure 4 gives one example of how this information can be directly applied. The figure illustrates a manifestation of the threshold behavior that is typically observed when conditioning with a pad conditioner with uniform tip height, where all the cutting points are controlled within a height range of about 10 µm. As opposed to a conventional conditioning platform, where there is a much wider range of tip heights, the uniform height-controlled conditioner exhibits a threshold behavior where no measurable cutting occurs below a limiting condition down-force (cdf). Figure 4 illustrates the disconnect between a high down-force, accelerated cutting test, using 14 lbs cdf and designed to return the “CR” value for a conditioner, and typical process cdf levels, in the range of 5 lbs cdf. Note that CR values are generally about an order of magnitude higher than comparable polishing tool level pad wear rates. Whereas conventional platforms yield a linear response between CR and tool level pad wear rates, the uniform height design exhibits an offset, such that at low CR levels, low pad wear rates are observed. The position of this threshold is a function of pad type. These data suggest that this threshold can be correlated with the mechanical strength of the pad material, as determined by the tensile test results.We have also explored the effect of strain rate on tensile response. Strain rates in a typical CMP process may be as high as 105 s-1, and as shown in Figure 2, strain rate can have a significant effect on material behavior. Figure 5 illustrates typical results, illustrating the extremes of response for this group of pads, and Figure 6 shows the normalized response of offset yield and tensile strength as a function of strain rate. Of these materials, only IK4350L exhibits a divergent response, and as shown in Figure 7, IK4350L typically exhibits the most abrupt transition between the exponential porosity signature and the conditioner cutting signature, indicating a tendency towards the gross over-conditioning behavior characteristic of regime 3.Over the range of strain rates explored here, all of these materials can be characterized as “rubbery”. This rubbery behavior can be understood in the context of reported property measurements of CMP pads, which indicate distinct glass transitions related to the soft and hard phases of the polyurethane from which the pad is made. This analysis suggests that pad behavior is dominated by the “rubbery plateau” of the soft segment of the polymer, with the glass transition of the hard segment occurring above typical polishing temperatures. Figure 1

Rate effect of rocks: Insights from DEM modeling

Rocks are subjected to different loading rates at different construction stages and engineering applications. The strength of rock usually increases with loading rate. This rate dependency is one of the time-dependent behaviors of rock, whereby the micro-mechanisms are believed to be the subcritical crack growth due to stress corrosions. However, no evidence is provided yet. This study investigated rate effects of rocks through a novel implementation of Parallel-Bonded Stress Corrosion (PSC) model in Discrete Element Method (DEM). Long-term microparameters in PSC are first calibrated through creep test. Then, a series of uniaxial compressive strength, direct tensile strength, and triaxial compressive strength tests are performed, with strain rates ranging from 1×10−7/s to 1×10−3/s. Results show that the uniaxial compressive strength is highly dependent on strain rates which quantitatively matches with the experimental data. At lower strain rate, more subcritical cracks propagate due to longer stress-corrosion reaction time, resulting in a lower strength. Besides, strain rate also influences the failure patterns in post-peak, with single failure plane at lower strain rates and multiple failure planes at higher strain rates. Rate effects are also observed in direct tensile strength tests, with similar rate of increase in strength and a transition in cracking pattern, which align with the experimental data, indicating tension-induced subcritical cracking is the unified underlying micro-mechanism of rate effects for both cases. However, in triaxial compressive strength tests, rate effects become less obvious with increasing confining pressure, consistent with experimental findings, as subcritical crack growth is suppressed in shearing processes.

Gradient ceramic structures via multi-material direct ink writing

Dense boron carbide-silicon carbide specimens with composition tailored at the mesoscale were produced by direct ink write additive manufacturing in three configurations: I, 2 % and II, 10 % compositional layer-to-layer steps, and III, homogeneous composition throughout. Flexural strength, indicative of tensile failure, is the highest for the Type-II design (366 MPa) due to its compressive residual stress state in the surface layers. Analysis of thermally-induced residual stresses predicts the ranking of the flexural strengths obtained for Type-II (highest), Type-I (intermediate), and Type-III (lowest) specimens. Compressive strength is load-orientation independent, highly strain-rate dependent, and reduced for specimens with thermal residual stress. Mechanical tests were performed in cube and dumbbell geometries. Dumbbell geometry compression specimens have a compressive strength that is 68 % (quasistatic) and 86 % (dynamic) higher than that of cube geometry and show a greater strain rate dependence. The rate dependency is attributed to the competition between crack propagation and loading velocities. Type-I dumbbells show the highest mean compressive strength of 3.96 GPa (quasi-static) and 5.11 GPa (dynamic). The failure mode evolves from mixed intergranular/transgranular at low strain rates to transgranular at high strain rates. High-speed video analysis indicates that dumbbell geometry specimens fail in compression due to microcrack growth and coalescence, while cubes fail due to the axial macrocracks that develop at the specimen/load platen interface and propagate into the specimen parallel to the loading direction (end splitting). This work demonstrates the impact of compositional variation, tailored by additive manufacturing, on the mechanical performance of ceramic composites.

Hydrogen embrittlement and strain rate sensitivity of electrodeposited copper: part I – the effect of hydrogen content

Slow strain rate tensile testing was conducted on electrodeposited copper, which is a candidate coating material for used nuclear fuel containers. Embrittlement was observed in electrodeposited copper containing 26.4 ± 1.0 ppm hydrogen, with a strain rate sensitivity such that the embrittlement was exacerbated at lower strain rate (5 × 10−7 s−1). Tensile tests conducted at 100° and 200 °C also intensified embrittlement when compared with tests conducted at room temperature. In contrast, electrodeposited copper containing only 5.25 ± 0.97 ppm hydrogen exhibited ductile behavior at all tested strain rates and temperatures. These findings suggest that a previously unexplained slow strain rate hydrogen embrittlement can operate in electrodeposited copper provided that the hydrogen concentration is sufficiently high. Further analyses revealed that the deformation of embrittled copper is achieved by the formation of internal microcracks which coalesce at the point of failure.

Dynamic compressive behavior of hybrid basalt-polypropylene fibers reinforced coral aggregate concrete

In this study, the effects of strain rate, fiber type, and hybrid fiber content on the dynamic mechanical properties of basalt-polypropylene fiber reinforced coral aggregate concrete (HBPRCAC) under impact loading are investigated using a split-Hopkinson pressure bar (SHPB) with a 75 mm diameter. The results demonstrated that the incorporation of basalt fiber (BF) and polypropylene fiber (PF), particularly when mixed, effectively reduced the failure of HBPRCAC. With an increase in strain rate, the failure of HBPRCAC exhibited a more severe pattern; even at low strain rates, cracks directly passed through the coral aggregate, causing damage. The failure modes of BF and PF were related to the strain rate. The probability of BF and PF being pulled out was higher at low strain rates than at high strain rates, where BF and PF predominantly exhibited snap failures. Additionally, the dynamic increase factor (DIF) of the dynamic compressive strength and dynamic modulus of elasticity for HBPRCAC demonstrated a decimal logarithmic linear increase with strain rate, while the dynamic critical strain and impact toughness of HBPRCAC exhibited a linear increase with strain rate. The mixed addition of BF and PF had varying effects on the strain rate sensitivity of HBPRCAC's dynamic mechanical properties, but the fiber mixing content was significantly positively correlated with the strain rate effects on the dynamic compressive mechanical properties of HBPRCAC. The dynamic compressive strengths of BPCAC-0.1 and BPCAC-0.2 at strain rates of 128–135 s−1 were increased by 78.66 % and 88.47 %, respectively, compared to those at strain rates of 33–36 s−1. The dynamic moduli of elasticity for BPCAC-0.1 and BPCAC-0.2 showed increases of 16.47 % and 13.06 %, respectively, compared to that of coral aggregate concrete. Moreover, the critical strain and impact toughness of BPCAC-0.2 were the highest at all tested strain rates.

Effect of interface type on deformation mechanisms of γ-TiAl alloy under different temperatures and strain rates by molecular dynamics simulation

Crystalline interface plays a significant role in strengthening lamellar γ-TiAl alloys through reconciling the strength and ductility. Herein, the effects of temperature and strain rate on the tensile deformation of three lamellar γ-TiAl interface models are investigated by molecular dynamics simulations. The three interfaces, pseudo twin (PT), rotational boundary (RB), and true twin (TT), exhibit different tensile responses due to the different interface effects: TT interface only acts as a barrier of dislocation traversing to facilitate crack extension; PT interface acts as both dislocation barrier and emission source and has a stronger release of strain energy than TT interface, retarding the crack extension; RB interface can retard and resist crack extension due to the blunting and deflection of the crack tip and the best interface geometry compatibility. The defect evolution indicates that the elevated temperature suppresses dislocation propagation at low strain rate, while the high strain rate causes small lamellar stacking faults and slit-shaped holes along tensile direction at low temperature. In addition, the dual conditions of high strain rate and low temperature induce the phase transition from FCC to BCC and then BCC to HCP. These findings provide a specific insight to understand the atomistic mechanism of interface-mediated deformation.

Effect of Y2O3 on high temperature thermal compression performance of Cu–10W composites and microstructure analysis

In this study, Cu–10W and 2 wt%Y2O3/Cu–10W composites were successfully prepared via mechanical ball milling and spark plasma sintering. Hot compression experiments on the two materials were carried out in the temperature range of 300°C-600 °C and in the strain rate range of 0.01 s−1–10 s−1. The hot deformation activation energy of the two materials was calculated and a constitutive equation was established. The optimum hot deformation process parameters were obtained according to a hot processing map. The effects of Y2O3 on the thermal deformation behavior of the Cu–10W composites and their microstructures were investigated, and the results showed that Y2O3 could enhance the stability of Cu–10W at high temperatures. The activation energies of thermal deformation of Cu–10W and 2 wt%Y2O3/Cu–10W were 159.56 kJ/mol and 129.85 kJ/mol, respectively. Moreover, Y2O3 improved the interfacial bonding strength of Cu and W in the Cu–10W material, effectively preventing the generation of microcracks and pores during the high-temperature compression process; Y2O3 provides more nucleation sites in the recrystallization process, which is favorable for the excitation of recrystallization. A low strain rate at high temperatures favors the occurrence of recrystallization, and the 2 wt%Y2O3/Cu–10W composites tend to exhibit discontinuous dynamic recrystallization (DDRX) under high-Z-value conditions and continuous dynamic recrystallization (CDRX) under low-Z-value conditions.

Research on hot deformation behavior and microstructure evolution mechanism of GH4169 superalloy

The hot deformation behavior and microstructure evolution of GH4169 superalloy were investigated through hot compression experiments with a temperature range of 900–1100 °C and strain rates ranging from 0.01 to 5 s−1. Concurrently, the flow stress curve of the alloy was obtained and constitutive equations were established. Based on the dynamic material model, a hot working diagram was established and the hot working window was optimized. The findings demonstrate that the high-temperature softening mechanism of this alloy primarily involves dynamic recrystallization (DRX), while both discontinuous dynamic recrystallization (DDRX) and continuous dynamic recrystallization (CDRX) exist. According to the hot processing map, the process parameters corresponding to the unstable areas are low temperatures and medium-high strain rates (900–985 °C, 0.15–5 s−1), and high temperatures and high strain rates (1025–1100 °C, 2.5–5 s−1). The reason is that the appearance of deformation bands and flow localization in the microstructure. The optimal hot working parameters for GH4169 are 1000 °C/0.01 s−1 and 1050–1100 °C/0.01–0.1 s−1, where the microstructure consists of uniformly distributed DRX grains. The volume fraction of DRX in GH4169 alloy rises with higher temperatures or lower strain rates. In addition, the reduction of intergranular dislocations promotes the migration of grain boundaries from low angle grain boundaries (LAGBs) to high angle grain boundaries (HAGBs).

The Role of Deformation and Microstructure Evolution on Texture Formation of a TA15 Alloy Subjected to Plane Strain Compression.

In this study, the texture formation mechanism of a TA15 titanium alloy under different plane strain compression conditions was investigated by analyzing the slipping, dynamic recrystallization (DRX) and phase transformation behaviors. The results indicated that the basal texture component basically appears under all conditions, since the dominant basal slip makes the C-axis of the α grain rotate to the normal direction (ND, i.e., compression direction), but it has a different degree of deflection. With an increase in deformation amount, temperature or strain rate, {0001} poles first approach the ND and then deviate from it. Such deviation is mainly caused by a change in slip behaviors and phase transformation. At a smaller deformation amount and higher strain rate, inhomogeneous deformation easily causes a basal slip preferentially arising from the grain with a soft orientation, resulting in a weak basal texture component. A greater deformation amount can increase the principal strain ratio, thereby promoting other slip systems to be activated, and a lower temperature can increase the critical shear stress of the basal slip, further causing a dispersive orientation under these conditions. At a higher temperature and a lower strain rate, apparent phase transformation will induce the occurrence of lamellar α whose orientation obeys the Burgers orientation of the β phase, thereby disturbing and weakening the deformation texture. As for DRX, continuous-type (CDRX) is most common under most conditions, whereas CDRX grains have a similar orientation to deformed grains, so DRX has little effect on overall texture. Moreover, the microhardness of samples is basically inversely proportional to the grain size, and it can be significantly improved as lamellar α occurs. In addition, deformed samples with a weaker texture present a higher microhardness due to the smaller Schmidt factors of the activated prism slip at ambient loading.

Investigation of constitutive models and microstructure evolution during hot deformation and solution treatment of Al–Zn–Mg–Cu alloy

In this paper, isothermal thermal compression tests were carried out on Al–Zn–Mg–Cu alloys at varying deformation temperatures (360°C∼440°C) and strain rates (0.001s−1∼10s−1) using a Gleeble-3500C thermal simulation tester. Based on the true strain stress data obtained from the tests, the flow behavior of Al–Zn–Mg–Cu alloys during thermal deformation was investigated. Through a comprehensive consideration of deformation temperature, strain rate, and strain compensation, a high-precision constitutive model was established. Additionally, the specimens subjected to hot compression were further treated with solution annealing for different durations (0 h–2 h) to investigate the static recrystallization (SRX) behavior and the associated microstructural evolution of the alloy during the solution treatment process. Electron Backscatter Diffraction (EBSD) was employed to characterize the microstructure evolution of Al–Zn–Mg–Cu alloy under various deformation and solution treatment conditions. The EBSD data were further processed and analyzed using the MTEX toolbox. The results revealed that dynamic recovery (DRV) is the predominant softening mechanism during the deformation process, accompanied by a small amount of dynamic recrystallization (DRX). The dynamically recrystallized grains exhibit a random crystallographic orientation. Further investigation showed that low temperature and high strain rate conditions are unfavorable for the occurrence of dynamic recovery and dynamic recrystallization during the thermomechanical processing. However, dislocations accumulated during deformation provided sufficient stored energy for the growth of static recrystallized grains during subsequent solution treatment, with static recrystallized grains predominantly forming at grain boundaries.

Predicting peak tensile stress in mesoscale concrete considering size effects: A data-physical hybrid-driven approach

The size effect and strength discreteness observed in concrete stem primarily from its mesoscopic heterogeneity. Despite this understanding, establishing a clear relationship between the macroscopic and mesoscopic mechanical behaviors remains a considerable challenge. While some advancements have been made in studying the size effect of concrete, particularly regarding the rate effect, there has been relatively less emphasis on addressing the influence of random meso-component distribution. To investigate the tensile behaviors of concrete across varying low strain rates (10−5 s−1∼10−1 s−1) and model sizes, a meso-model dataset was established comprising double edge notched concrete with mortar matrix, coarse aggregate, and interface transition zone. A convolutional neural network introducing physical parameters was implemented to capture the potential non-linear relationship of concrete from meso-structure, strain rate and model size to tensile peak stress. Subsequently, the data-driven solution for the “Static and Dynamic unified” Size Effect Law (SD-SEL) in concrete tensile strength was developed by deconstructing the back propagation (BP) neural network to enhance its rationality, followed by the verification of the proposed formula. The findings indicate that the Data-Physical Hybrid-Driven approach effectively analyzes the mechanical response of concrete without the need for complex mechanical derivations, offering a promising tool for studying the size effect of composite materials.

The mechanism of low strain rate and moderate principal stress effects in triaxial prestressed marble under lateral impulsive load

Stress waves have a significant impact on the strength and deformation characteristics of deep rock masses at a certain distance from the epicenter or explosion source. In order to study the dynamic responses of deep-buried marble under the disturbance condition, the true triaxial compression test (TTC), the true triaxial disturbed compression test with lateral impulsive load (TTDC) and the synchronous acoustic emission monitoring on the marble were respectively conducted to simulate the influencing process of the seismic wave. The test results show that under lateral impulsive load, a ‘short-range plateau’ phenomenon occurs in the stress-strain curves of the marble samples. With the increase of intermediate principal stress σ2, the ‘short-range plateau’ of ε2 and ε3 curves gradually shrinks and even disappears, and the anisotropy of sample deformation becomes more obvious. The σ2 significantly affects the microfracture activity and the evolution of energy inside the samples under the impulsive load in the whole process of true triaxial disturbed compression. The lateral impulsive load weakens the marble strength which shows an obvious low strain-rate disturbance effect. The marble samples under the impulsive load have a high sensitivity to axial load and are liable to form local brittle fracture. This fracture induced by local stress concentration and strain energy release becomes more pronounced when the axial load is further applied to the samples. By contrast, the impulsive load in σ2 direction has a protective effect on limiting the lateral deformation of the samples and improving its axial deformation capacity, which greatly changes the action mechanism of σ2 on the sample lateral deformation. The variation of marble mechanical properties under lateral impulsive load is the result of the interaction between the low strain-rate disturbance and the intermediate principal stress effect.

Effect of strain rate on tensile characteristics and failure behavior of Al/steel welded joint producing by a laser-MIG composite heating source

Studies on dynamic tensile characteristics for Al/steel dissimilar materials are crucial to ensure the integrity and dependability of light-weight structures. In this study, the tensile characteristics and failure behaviors of Al/steel laser-MIG welded-brazed joints were studied. The dynamic fracture mechanisms of the joints are discussed. With the increase in strain rate, the fracture mode and tensile properties of Al/steel joints with reinforcement changed. The joints exhibited two failure modes of heat-affected zone failure at lower strain rates and interface failure at higher strain rates. When the strain rate was 1000 s−1, the increase in dislocation density in the weld reinforcement and diversion of cracks in the intermetallic compound layer significantly enhanced the joint’s properties. The tensile and yield strengths reached 222.6 and 166.6 MPa, 6.5 % and 17.9 % higher than those at a stain rate of 1 s−1, respectively. For Al/steel joints without reinforcement, as the strain rate increased, the crack gradually grew to the Al8Fe2Si phase, leading to a notable enhancement in the joint’s performance. At a strain rate of 500 s−1, the maximum strength of the joint reached 238.3 MPa, representing an increase of 58.9 % in comparison to the strain rate of 1 s−1.

Experimental study on impact behaviour of normal strength mortar at cryogenic temperatures and after freeze-thaw cycles

Concrete structures employed for the storage of Liquefied Natural Gases (LNG) currently undergo temperature as low as −170 °C. These critical engineering structures may also experience dynamic loads such as impact or explosion during service life. Therefore, it is crucial to explore the mechanical response of concrete at intermediate to high strain rates together with low temperatures or cryogenic freeze-thaw (FT) cycles. This study presents experimental research into the combined effects of low temperatures and strain rate on normal strength mortar, providing a preliminary analysis of the dynamic performance of concrete at low and cryogenic temperatures. A Split Hopkinson Pressure Bar (SHPB) device was used to investigate the characteristics of dynamic compression (at strain rates of 40, 80, 120 and 160 s−1) and dynamic split tension (at strain rates of 20, 40, 60 and 80 s−1) of Normal Strength Mortar (NSM) at different low temperatures. In addition, the dynamic compression (at strain rates of 80, 130 and 180 s−1) after cryogenic FT cycles was also explored. The findings revealed that the failure pattern of NSM samples exposed to coupled low temperature or cryogenic FT cycles and high strain rate loading notably varied from that observed under room temperature condition. Both the dynamic compressive and split tensile strengths of NSM increased with the strain rates at all temperatures. At −160 °C, the dynamic compressive and splitting tensile strengths of NSM specimens were greater than those at room temperature (by 10.94 % and 28.29 %, respectively) and −70 °C (by 3.13 % and 4.12 %, respectively). Cryogenic freeze-thaw cycles evidently impacted the material static and dynamic performance. An empirical model was developed to predict the dynamic increase factors (DIFs) for both dynamic compression and splitting tensile strengths of NSM at low/cryogenic temperatures and after freeze-thaw cycles. Scanning electron microscopy (SEM) technique was performed to study and comprehend the microscopic processes and microstructural changes after FT cycles.

Reappraising the seismogenic potential of a low-strain rate region: Active faulting in the eastern Siena Basin (southern Tuscany, Italy)

We investigated the active tectonics and earthquake potential of the eastern Siena Basin, a slowly deforming portion of southern Tuscany in the inner Northern Apennines. This region hosts several historical settlements and valuable cultural heritage, but also frequent background seismicity and rare damaging earthquakes in the Mw range 5.0–6.2. We describe in detail an active, capable, and seismogenic fault system that we identified in the eastern Siena Basin, a few kilometers south-east of the city of Siena, thanks to the presence of an active quarry (Cava Capanni) that exploits travertines of Middle Pleistocene-Holocene age. Travertines are unique rock masses that may preserve living evidence of active and seismogenic faulting, thus providing remarkable seismotectonic insight. The active fault system consists of at least two segments rupturing travertines younger than 45 ka, with a cumulative vertical displacement of 111 cm, and an estimated minimum slip rate of 0.02–0.03 mm/y. We maintain that this displacement is the result of at least three coseismic movements accompanied by clastic dykes injected within the fault damage zone due to liquefaction phenomena. The fault system is seen to extend east of the quarry, affecting Pliocene and Mesozoic deposits.The Cava Capanni fault system is evidence of a poorly understood but potentially seismogenic tectonic mechanism of regional extent. Its orientation and kinematics are compatible with the activity of faults that are oriented obliquely or orthogonally to the main chain axis, in contrast with the setting of the axial and outer zone of the Northern Apennines, where extension and compression are accommodated by Apennines-parallel faults.

Preparation, Deformation Behavior and Irradiation Damage of Refractory Metal Single Crystals for Nuclear Applications: A Review.

Refractory metal single crystals have been applied in key high-temperature structural components of advanced nuclear reactor power systems, due to their excellent high-temperature properties and outstanding compatibility with nuclear fuels. Although electron beam floating zone melting and plasma arc melting techniques can prepare large-size oriented refractory metals and their alloy single crystals, both have difficulty producing perfect defect-free single crystals because of the high-temperature gradient. The mechanical properties of refractory metal single crystals under different loads all exhibit strong temperature and crystal orientation dependence. Slip and twinning are the two basic deformation mechanisms of refractory metal single crystals, in which low temperatures or high strain rates are more likely to induce twinning. Recrystallization is always induced by the combined action of deformation and annealing, exhibiting a strong crystal orientation dependence. The irradiation hardening and neutron embrittlement appear after exposure to irradiation damage and degrade the material properties, attributed to vacancies, dislocation loops, precipitates, and other irradiation defects, hindering dislocation motion. This paper reviews the research progress of refractory metal single crystals from three aspects, preparation technology, deformation behavior, and irradiation damage, and highlights key directions for future research. Finally, future research directions are prospected to provide a reference for the design and development of refractory metal single crystals for nuclear applications.