Low-pressure Process Research Articles

Batch Settling and Low-Pressure Consolidation Behaviors of Dredged Mud Slurry: Steady-State Evaluation and Mechanism Study

Since the exploration of the characteristics of dredged mud slurry during batch settlement and low-pressure consolidation (less than 100 kPa) is still insufficient, the determination of the optimal time to start the vacuum preloading method (VPM) on dredged-fill foundations is still empirically oriented (due to a lack of enough scientific basis). To further explore the characteristics of dredged mud slurry during batch settlement and low-pressure consolidation, samples from typical dredged-fill land projects were obtained and used to conduct batch sedimentation model experiments and low-pressure (less than 100 kPa) consolidation tests. The results of experiments and analyses showed the following: (1) the clay (d < 0.005 mm) content is a main factor affecting the batch settlement and consolidation characteristics of dredged mud slurry, which is not conducive to the consolidation effect of dredged-fill foundations. (2) For dredged mud slurry whose clay content is within 40% to 60%, the cumulative change rate of the average porosity ratio of 60% to 75% is suitable for evaluating the steady state of its batch sedimentation process, i.e., the optimal starting time of VPM. Finally, based on the experimental analyses, a settlement prediction method that considers both the batch sedimentation and the low-pressure consolidation processes was developed and validated.

Identification of Intermetallic Phases Limiting the Growth of Austenite Grains in the Low-Pressure Carburizing Process

This article presents the results of a study to identify intermetallic phases whose role is to limit austenite grain growth in the low-pressure carburizing process. A drawback of high-temperature low-pressure carburizing is the austenite grain growth during the process. Using low-pressure carburizing with pre-nitriding technology (PreNitLPC®) offers the possibility of reducing austenite grain growth. This technology involves the application of doses of ammonia during the heating stage of the steel, at the carburizing temperature, to introduce nitrogen into the surface layer of the steel and to form nitrides. It is these phases that cause restrictions on austenite grain growth during carburizing. The research carried out in this article was aimed at identifying these phases. The research was carried out on one of the basic steels used for carburizing—16MnCr5 steel. The carburizing of this steel with and without pre-nitriding was performed, followed by an evaluation of the austenite grain size after these processes and the identification of the intermetallic phases present in the surface layer of the steel.

Implementation of a Sensitive Method to Assess High Virus Retention Performance of Low-Pressure Reverse Osmosis Process.

Human enteric viruses are important etiological agents of waterborne diseases. Environmental waters are usually contaminated with low virus concentration requiring large concentration factors for effective detection by (RT)-qPCR. Low-pressure reverse osmosis is often used to remove water contaminants, but very few studies focused on the effective virus removal of reverse osmosis treatment with feed concentrations as close as possible to environmental concentrations and principally relied on theoretical virus removal. The very low viral concentrations usually reported in the permeates (i.e. at least 5 log of removal rate) mean that very large volumes of water need to be analysed to have sufficient sensitivity and assess the process efficiency. This study evaluates two methods for the concentration of adenoviruses, enteroviruses and MS2 bacteriophages at different viral concentrations in large (< 200 L) and very large (> 200 L) volumes. The first method is composed of two ultrafiltration membranes with low-molecular weight cut-offs while the second method primarily relies on adsorption and elution phases using electropositive-charged filters. The recovery rates were assessed for both methods. For the ultrafiltration-based protocol, recovery rates were similar for each virus studied: 80% on average at high virus concentrations (106-107 viruses L-1) and 50% at low virus concentrations (103-104 viruses L-1). For the electropositive-charged filter-based method, the average recoveries obtained were about 36% for ADV 41, 57% for CV-B5 and 1.6% for MS2. The ultrafiltration-based method was then used to evaluate the performance of a low-pressure reverse osmosis lab-scale pilot plant. The retentions by reverse osmosis were similar for all studied viruses and the validated recovery rates applied to the system confirmed the reliability of the concentration method. This method was effective in concentrating all three viruses over a wide range of viral concentrations. Moreover, the second concentration method using electropositive-charged filters was studied, allowing the filtration of larger volumes of permeate from a semi-industrial low-pressure reverse osmosis pilot plant. This reference method was used because of the inability of the UF method to filter volumes on the order of one cubic metre.

Gas heating by inductively coupled low-pressure chlorine process plasmas

The mechanism of gas heating in low-pressure inductively coupled chlorine plasma is analyzed using a self-consistent two-dimensional axisymmetric fluid plasma model that is coupled with the compressible Navier–Stokes equations. For gas pressures of 10 and 20 mTorr and the discharge power in the range 0.1–1.3 kW, the main reactions contributing to gas heating were the ion–ion recombination reactions and the quenching of electronically excited chlorine atoms. At the same time, the energy released by the electron impact dissociation reaction of molecular chlorine is negligible due to its high degree of dissociation within the plasma bulk. The comparison between the results of our simulations and the fitting equation proposed in the literature show qualitative agreement, although there is significant quantitative discrepancy.

Catalytic and non-catalytic low-pressure hydrothermal liquefaction of pinewood sawdust, polyolefin plastics and their mixtures

Hydrothermal co-liquefaction of biomass and polyolefin plastic feedstocks offers the advantage of potential synergistic reaction environments for producing liquid products of high fuel quality. In this present study, hydrothermal liquefaction and co-liquefaction of sawdust, low-density polyethylene and high-density polyethylene were investigated in a batch reactor from 350 °C to 450 °C and autogenic pressures below 30 bar. The novel low-pressure hydrothermal processing method was carried out with and without low-cost Ni–Cu/Al2O3 bimetallic catalyst. Thermal degradation of the sawdust started at 350 °C, whereas the plastics could only completely degrade at 450 °C, which was then chosen as the optimum reaction temperature. The catalysed process led to an increase in oil yield from the sawdust, with carbon enrichment by 16.3% and 22% deoxygenation. Furthermore, the catalyst promoted the formation of ketones and aromatic hydrocarbons, while consuming phenols and furfural in the sawdust-derived bio-oils. For the plastics, the catalyst, gave slight decreases in oils yield in favour of gas and/or char formation, with the promotion of in situ hydrogenation to enhance the yields of alkanes over alkenes. Results from hydrothermal co-liquefaction tests showed that synergistic interactions occurred between the degradation products of sawdust and the plastics. The observed synergy was further promoted by the presence of the catalyst, leading to dramatic deoxygenation of the oil products to produce hydrocarbon-rich fuels with less than 4 wt% oxygen contents (≈90% deoxygenation). This low-pressure hydrothermal co-liquefaction process is an efficient and cost-effective pathway for single-loop conversion of widely available biomass and plastics feedstocks into highly deoxygenated oils for use as sustainable fuels.

Optimal design and multicriteria comparison of extractive distillation processes for separating of a quaternary low-boiling solvent mixture

This article mainly explores the eco-efficient separation of a complex quaternary azeotropic mixture of methanol, n-hexane, ethyl acetate and ethanol from a pharmaceutical enterprise via extractive distillation. To this end, aniline (AN) and ethylene glycol (EG) are selected as two alternative entrainers based on the relative volatility curve. Two conventional processes with AN and EG (AN-CED and EG-CED) are proposed and optimized with total annual costs (TAC) as a goal by simulated annealing algorithm. To improve energetic and economic performance, two optimal strengthening processes, that is, low-pressure side-stream extractive distillation process with AN (AN-SSED) and dividing-wall extractive distillation process with EG (EG-EDWC) are also developed for the first time. Finally, the four processes are compared in terms of economics, CO2 emissions and inherent safety. The results show that the AN-SSED process is recommended due to the best economic, environmental and inherent safety properties, as reflected by the lowest TAC, CO2 emission and process route index (PRI). It can reduce TAC by 9.38%, CO2 emission by 26.34% and PRI by 38.02% relative to the EG-EDWC process. Remarkably, the EG-EDWC process can reduce TAC by 11.12% than AN-CED process and 6.9% than the EG-CED process, but it is inferior to the two conventional processes in terms of CO2 emissions and inherent safety.

Simulation and Experimental of Infiltration and Solidification Process for Al2O3(3D)/5083Al Interpenetrating Phase Composite for High Speed Train Prepared by Low-Pressure Infiltration.

Understanding the infiltration and solidification processes of liquid 5083Al alloy into Al2O3 three-dimensional reticulated porous ceramic (Al2O3(3D) RPC) is essential for optimizing the microstructure and properties of Al2O3(3D)/5083Al interpenetrating phase composites (IPCs) prepared by low-pressure infiltration process (LPIP). This study employs ProCAST software to simulate the infiltration and solidification processes of liquid 5083Al with pouring velocities (PV) of 0.4 m/s infiltrating into Al2O3(3D) RPC preforms with varying porosities at different pouring temperatures (PT) to prepare Al2O3(3D)/5083Al IPCs using LPIP. The results demonstrate that pore diameter of Al2O3(3D) RPC preforms and PT of liquid 5083Al significantly influence the of the infiltration. Solidification process analysis reveals that the Al2O3(3D) RPC preform with smaller pore diameters allows the lower pouring velocity of 5083Al to solidify faster compared to the preform with larger pore diameters. Al2O3(3D)/5083Al IPCs were prepared successfully from Al2O3(3D) RPC porosity of 15 PPI with liquid 5083Al at PV 0.4 m/s and PT 800 °C using LPIP, resulting in nearly fully dense composites, where both Al2O3(3D) RPCs and 5083Al interpenetrate throughout the microstructure. The infiltration and solidification defects were reduced under air pressure of 0.3 MPa (corresponding to PV of 0.4 m/s) during LPIP. Finite volume method simulations are in good agreement with experimental data, validating the suitability of the simplified model for Al2O3(3D) RPCs in the infiltration simulation.

Effects of body-armor-like grinding wheel parameters on surface quality and material removal rate in high-shear and low-pressure grinding process

Effects of body-armor-like grinding wheel parameters on surface quality and material removal rate in high-shear and low-pressure grinding process

Low-Pressure Hydrothermal Processing of Disposable Face Masks into Oils

A total of 5.4 million tons of face masks were generated worldwide annually in 2021. Most of these used masks went to landfills or entered the environment, posing serious risks to wildlife, humans, and ecosystems. In this study, batch low-pressure hydrothermal processing (LP-HTP) methods are developed to convert disposable face masks into oils. Three different materials from face masks were studied to find optimal processing conditions for converting full face masks into oil. The oil and gas yields, as well as oil compositions, depend on the feedstock composition, particle size, and reaction conditions. Yields of 82 wt.% oil, 17 wt.% gas, and minimal char (~1 wt.%) were obtained from full masks. LP-HTP methods for converting face masks have higher oil yields than pyrolysis methods in the literature and have lower operating pressures than supercritical water liquefaction. LP-HTP methods for face masks can increase net energy returns by 3.4 times and reduce GHG emissions by 95% compared to incineration. LP-HTP has the potential to divert 5.4 million tons of waste masks annually from landfills and the environment, producing approximately 4.4 million tons of oil.

Multi-Objective Optimization of The Low-Pressure Casting of Large-Size Aluminum Alloy Wheels through a Systematic Optimization Idea.

The process parameters in the low-pressure casting of large-size aluminum alloy wheels are systematically optimized in this work using numerical casting simulation, response surface methodology (RSM), and genetic algorithm (NSGA-II). A nonlinear input-output relationship was established based on the Box-Behnken experimental design (BBD) for the crucial casting parameters (pouring temperature, mold temperature, holding pressure, holding time), and response indicators (defect volume fraction, spokes large plane mean secondary dendrite spacing (SDAS)), and a mathematical model was developed by regression analysis. The Isight 2017 Design Gateway and NSGA-II algorithm were used to increase the population and look for the best overall solution for the casting parameters. The significance and predictive power of the model were assessed using ANOVA. Casting numerical simulation was used to confirm the best option. To accomplish systematic optimization in its low-pressure casting process, the mold cooling process parameters were adjusted following the local solidification rate. The results showed that the mathematical model was reliable. The optimal solutions were a pouring temperature of 703 °C, mold temperature of 409 °C, holding pressure of 1086 mb, and holding time of 249 s. The mold cooling process was further optimized, and the sequence solidification of the optimal solution was realized under the optimized cooling process. Finally, the wheel hub was manufactured on a trial basis. The X-ray detection, mechanical property analysis, and metallographic observation showed that the wheel hub had no X-ray defects and its mechanical properties were well strengthened. The effectiveness of the system optimization process scheme was verified.

Дослідження впливу температури газу процесу холодного газодинамічного напилювання на адгезійну міцність нікелевмісних покриттів

The subject of the research is the influence of low-pressure cold spraying process parameters on the adhesive strength of the coatings. The goal is to ensure the maximum values of the adhesive strength of nickel-based coatings deposited by cold spraying by controlling the gas temperature at the nozzle inlet. The task is to investigate the effect of the temperature mode of the DYMET-405 machine on the adhesive strength of the coatings obtained from the Ni+Zn+Al2O3 powder mixture at constant other spraying parameters. Research methods. The experimental study of the adhesive strength was conducted on the tear using adhesive method in accordance with DSTU 2639-94. The metal-matrix composite powder mixture Ni+Zn+Al2O3 was used as powder material. VT3-1 titanium alloy was chosen as substrate material. Coatings were deposited using DYMET-405 low-pressure cold spraying machine. Temperature regulation at the nozzle inlet was performed by turning on the required temperature mode on the equipment control panel. Other spraying parameters remained constant during coating deposition process. The results. It was established that with an increase in the temperature of the gas in the nozzle, an increase in the adhesive strength of coatings is observed, on average from 9.5 MPa to 28.7 MPa. This can be explained by the fact that an increase in gas temperature leads to an increase in the velocity of the gas flow and, accordingly, of the powder particles in this flow. Higher particle impact velocity has a positive effect on the process of their deforming, filling of pores, densifying of coating layers, and finally increasing the adhesive and cohesive strength. The scientific novelty of the obtained results is that the dependence of the gas temperature at the nozzle inlet during low-pressure cold spraying on the adhesive strength of Ni+Zn+Al2O3 powder mixture coatings deposited on VT3-1 titanium alloy substrates was obtained. Conclusions. The practical value of the obtained results is that the obtained dependences of adhesive strength on gas temperature can be used for the development of cold spraying recommendations for the deposition of restorative coatings on parts made of titanium alloys, in particular in aircraft engines to eliminate operational defects.

Process steam generation from low-grade waste heat in a direct- contact adsorption heat pump based on superhydrophobic surface-modified Zeolite 13X

ABSTRACT Adsorption heat pump (AdHP) is a potential technology to recover and storage low-temperature waste heat. This paper presents an experimental research on direct low-pressure process steam generation from hot water based on superhydrophobic surface-modified zeolite 13X. The measured water contact angle of the modified zeolite is larger than 150°, which restricts free water entering the pores inside the zeolite particles. Cyclic experiments are conducted for performance evaluation. High-temperature steam (205–229°C, 0.1–0.3 MPa) is generated from hot water (72°C) in the AdHP driven by dry air (130°C). The temperature of generated steam is promoted with increasing preset steam pressure, among which the temperature is raised by about 23°C at 0.3 MPa. As the boiling point of water rises simultaneously, the sensible heat demand is increased. Thus, the mass of the steam is accordingly decreased. GTL (gross temperature lift) reaches 130°C. When the preset pressure is increased, COPh (coefficient of performance for heating) and SHP (specific heat power) for direct steam generation are decreased by 36% and 39%, respectively. One feasible option to elevate these two indicators is to increase the inlet water to near boiling water to match the change in the preset pressure. However, the GTL will be decreased based on the option. Balance should be made based on the choice of design for practical application.

Effects of Different Cooking Methods on Glycemic Index, Physicochemical Indexes, and Digestive Characteristics of Two Kinds of Rice

Diets including rice and rice-cooking methods influence digestive processes and blood glucose control. In this research, the effects of three different treatments (high-temperature and low-pressure plasma cooking, high-temperature cooking at atmospheric pressure (traditional method), and high-temperature cooking at high pressure) on the texture, color, molecular structure, infrared spectrum, microstructure, debranching enzyme activity, amylopectin content, glycemic index (GI), and in vitro starch digestibility of two rice varieties were studied. The results showed that the hardness, elasticity, viscosity, and chewability of rice after the high-temperature and low-pressure plasma treatment had no obvious changes compared with the traditional cooking method. A SEM analysis showed that the physical properties of the hydrophilicity on the surface of the rice increased after the high-temperature and low-pressure plasma treatment; the debranching enzyme activity reached 3.88 U/g (Xiantao rice) and 3.81 U/g (Heyuan rice), respectively, the amylose content of raw rice reached 68.77 mg/mL (Xiantao rice) and 64.92 mg/mL (Heyuan rice), which increased by 43.31 mg/mL and 39.46 mg/mL, respectively, and the GI was within the medium glycemic index of 56–69. The resistant starch in the Heyuan and Xiantao rice varieties amounted to 88.60 ± 3.10% and 89.40 ± 3.58%, respectively, after the high-temperature and low-pressure plasma processing method. The results showed positive effects and application potential for the cooking method in respect of diabetic consumers.

Structural, microstructural, and textural modifications of meringues induced by low-pressure baking process

This study aims to explore the structure of the French meringue using non-conventional baking equipment able to modify the external pressure during baking. A systematic approach with pressure variations (from atmospheric pressure Patm = 101 kPa to absolute pressure Pabs = 41 kPa) was used to determine the meringue structural, microstructural, and mechanical properties. The structural and microstructural parameters were characterized using X-Ray microtomography and compression tests. Observations from microtomography show that as the pressure decreased toward 51 kPa, meringues were less dense with larger cavities. These variations also implied differences in mechanical parameters, allowing the creation of new and innovative textures.As a final consideration, we propose mechanisms based on variations in pressure, temperature, and water evaporation to explain these findings.Thus, this systematic approach shows linearity modifications of structural and microstructural properties, establishing relationships between structure and texture.

Optimization of residual stress in low-pressure casting of ZL205A alloys

ZL205A alloys are prone to generate serious residual stress due to the long solidification intervals and multi-phase composition. In this study, the low-pressure casting process for ZL205A alloy hemisphere shell casting was investigated and continuously optimized. In the initial process, the knockout time, pouring temperature, preheating temperature of the sand mould, dwelling pressure, and filling rate were 3 h, 710 °C, 30 °C, 65 kPa, and 0.33 kPa·s−1, respectively. Macroscopic properties and microstructural features were simulated using a combination of ProCAST and Thermal-Calc software. Additionally, a series of experimental procedures, including EBSD, SEM, EDS, and XRD tests, were conducted to investigate the formation, morphology, and distribution of the microstructure. Current findings demonstrate that during the solidification process, the maximum temperature difference exceeds 220 °C, the maximum undercooling reaches 49.56 °C, and the maximum effective stress peaks at 301.7 MPa. The residual stress ranges from 20 to 200 MPa. Furthermore, there is no significant texture and preferred grain orientation during nucleation and solidification, and the structure field exhibits an equiaxed crystal but inhomogeneous pattern. Moreover, the finer and more homogeneous the grains and the smaller the deviation in grain orientation, the lower the residual stress. Specifically, two analytical models are developed: one between the casting parameters and the residual stress, and another between the shrinkage defects and the casting parameters. The lowest residual stress is achieved when the knockout time, pouring temperature, preheating temperature of the sand mould, dwelling pressure, and filling rate are 6 h, 725 °C, 250 °C, 95 kPa, and 1.67 kPa·s−1 respectively.

A study on high-shear and low-pressure grinding with body-armour-like abrasive tool (BAAT) for Inconel 718 superalloys

A novel body-armour-like abrasive tool (BAAT) was developed for the high-shear and low-pressure grinding of super alloys with an aim to reduce the ratio of normal force to tangential force. A composite process model was developed based on finite element method (FEM) method whereby. Shear thickening fluid (STF) inside the BAAT was set as variable viscosity through TABULAR approach. An experimental platform was established to explore the effects of high-shear and low-pressure grinding process on Inconel 718 specimens. The surface roughness and surface morphology of Inconel 718 specimens were examined. The experimental results were validated against the developed process model outcomes to demonstrate the efficacy. It was determined that the force ratio increased from 0.12 to 0.48 with the computational model while the force ratio experimentally enhanced from 0.298 to 0.577. The results from the computational model was consistent with the experimental outcomes which signifies the effectiveness of developed process model. Even from experimental results, it was evaluated that the surface roughness (Ra) reduced from 0.744 μm to 0.201 μm after removal of horizontal scratches and elimination of vertical processing texture. Inconel 718 specimens exhibited fine surface quality which represented that BAAT acquired desirable characteristics of processing under high-shear and low-pressure environment with excellent grinding performance.

Two-dimensional computational fluid dynamics modeling of slip-flow heat transfer in the hot filament chemical vapor deposition process

The computational fluid dynamics (CFD) modeling on the hot filament chemical vapor deposition (HFCVD) process used to produce a diamond film has been conducted to anticipate the heat transfer and calculate the generation of H. The effect in the slip-flow regime owing to the low-pressure process should be considered to simulate the heat transfer accurately. In addition, a heterogeneous reaction occurring on the filament should be included to calculate the generation of H. The parameters to simulate such microscopic phenomena were applied in the present work and validated by comparing the results with the previous work. The thermal accommodation coefficient (TAC) for H2 was determined as 0.3, at which the calculated mass fraction and H concentration showed good agreement. In addition, It was confirmed that the value could be applied over various filament temperatures and operating pressure. Further, the behavior of H is analyzed above the substrate; the analysis results indicate that there is a correlation between the gas temperature and the gradient of H concentration on the substrate. The high gas temperature caused a severe gradient; thus, a non-uniform film may be deposited. The developed modeling method suggested that microscopic phenomena could be simulated without experimental materials. This fact implied that it is possible to anticipate the temperature and H concentration regardless of the structural design.

The Stability of the Layer Nitrided in Low-Pressure Nitriding Process

The kinetics of the nitrided layer thickness growth and its structure depend on the nitrogen flux from the atmosphere to the nitrided surface. A nitrogen flux to the surface is more significant than a diffusion flux into the substrate, during forming surface iron nitrides and the internal nitriding zone. For pure iron, nitrided under low pressure, cutting off the nitriding atmosphere creates a flux from the subsurface layer of nitrides to the surface. The purpose of this paper is to determine the direction of the nitrogen flux in a similar situation for steels containing nitride-forming elements, thus answering the question of the stability of the layer nitrided under such conditions. The surface of X37CrMoV5-1 steel was nitrided under low pressure (of 24 hPa) and annealed in a vacuum or nitrogen. The microstructure, thickness of the nitride layers nitrided layers, the thickness of the internal nitriding zone, surface hardness and stresses were examined. The highest values of the nitrided layer properties were observed for the samples saturated only with nitrogen obtained from ammonia dissociation or additionally heated in nitrogen. It has been shown that using a pure vacuum during the annealing stage leads to unfavourable changes in the structure of the nitrided layer formed and, in particular, to the decomposition of the iron nitride layer formed at the saturation stage and occurrence of the tensile stresses—what excludes practical application of such layer. Ultimately, it has been shown that in the low-pressure nitriding process, the stability of the nitride layer of the nitrided surface strongly depends on the annealing atmosphere during the annealing stage, while the stability of the internal nitriding zone remains mainly at the same level.

Growth of YBa2Cu3O7-δ superconducting films under different atmospheres by pulsed laser deposition

This paper aims to explore the epitaxial growth process for high-temperature superconducting YBa2Cu3O7-δ (YBCO) thin films by pulsed laser deposition (PLD) under different deposition atmospheres. The possibility of depositing YBCO superconducting thin films, under an oxygen-free environment, that was different from the oxygen atmosphere for most deposition processes of YBCO superconducting thin films was studied. Three different atmospheres, with oxygen, nitrous oxide, and nitrogen, were used in the experiment. The influence of atmospheric pressure on the formation and superconductivity of the YBCO phase were studied in detail. The characterization of structure and electrical properties of the thin films showed that YBCO thin films showed highly preferentially growth along the c-axis, had good superconductivity, and could be prepared under all three atmospheres. The formation of the YBCO phase at high temperatures did not need oxygen, and subsequent low-pressure oxygen-annealing process was only required at low temperatures of about 350 ℃. Our findings are of great significance for the preparation and application of YBCO thin films on substrates that were easy to oxidize at high temperatures, such as nickel strips or some electronic printed circuit boards.

A hybrid ultrafiltration membrane process using a low-cost laterite based adsorbent for efficient arsenic removal

Adsorption has proven to be most effective for arsenic removal. But standalone adsorption cannot cater to the need for large-scale treatment in centralized water supply systems. Combining adsorption with other low-pressure membrane processes may aid in scaling up and intensifying the overall arsenic removal. In the present pilot study, a low-cost laterite-derived adsorbent (LDA) has been used in combination with cross-flow ultrafiltration (Ads-UF) to develop a strategy suitable for remediation of arsenic-contaminated water. Effect of adsorbent particles on permeate flux has been assessed at different transmembrane pressure (0.2–0.6 MPa). Two different hybrid configurations, with and without intermediate sand filtration (SF), i.e. Ads–SF–UF and Ads-UF, were considered. Resistance-in-series and combined complete pore block-cake layer models have been used to understand the flux profiles. In the case of arsenic-spiked groundwater, it was observed that flux decline, at 0.6 MPa, was 28% higher with Ads-UF during a 12 h run compared to Ads–SF–UF. Spent LDA retrieved from the sand column was found to retain the elemental composition as that of the unused LDA (as per FT-IR and EDX) and was considered safe for disposal based on Toxicity Characteristic Leaching Procedure (TCLP). Cost estimation for a facility with 200 m3/day treatment capacity has also been presented.