The ability to process thin wafers with thicknesses of 20-50um on front- and backside is a key technology for 3D stacked ICs (3Ds-IC). The most obvious reason for thin wafers is the reduced form factor, which is especially important for handheld consumer devices. However, probably even more important is that thinner wafers enable significant cost reduction for TSVs. Consensus has developed on the use of Temporary Bonding / Debonding Technology as the solution of choice for reliably handling thin wafers through backside processing steps. Temporary bonding and debonding comprises several processes for which yield is essential, as costly fully functional device wafers are being processed. The presented temporary bonding process consists of a bi-layer system, a release layer, Dow Corning WL-3001 Bonding Release and an adhesive layer, Dow Corning WL-4030 or WL-4050 Bonding Adhesive, processed on EVG's 850XT universal temporary bonding and debonding platform. Furthermore, this bi-layer spin coated material allows a room temperature bonding-debonding process increase process throughput which translates to low cost of ownership for high volume manufacturing. As such, this bi-layer approach features high chemical stability exposed to phosphoric acid, nitric acid, organic solvents and other chemicals familiar to TSV fabrication. Besides chemical stability this adhesive system provides also a high thermal stability when exposed to temperatures up to 300 °C. The temporary bonding process yield has a major impact on the overall Cost of Ownership (CoO). On the other hand, throughput of the individual process steps like spin coating, bonding, cure, debonding and cleaning processes is the second determining factor for improved CoO. In this presentation, we will present a study of the total thickness variation (TTV) and the evolution of TTV at different stages of the process. High resolution in-line metrology is an enabling tool to trace the bond integrity and yield throughout backside processing. As TTV is a major determining factor of the overall process yield, understanding its impact over the bonded wafer pair carries major importance. Especially, non-continuity of the edge region, showing an inherent edge bead after coating, and edge die yield will be focus of our contribution. Finally, our experimental results will be transferred into a cost of ownership model, discussing the pros and cons for high volume production.