Large Working Distance Research Articles

Exploring the pyro-phototronic effect for giant lateral photoresponse in an ITO/CdS/Si heterojunction position-sensitive detector

The demand for a high-performance position sensitive detector (PSD), a novel type of photoelectric sensor, is increasing due to advancements in digitization and automation technology. Cadmium sulfide (CdS), a non-centrosymmetric material, holds significant potential in photoelectric devices. However, the pyroelectric effect of CdS in PSDs and its influence on lateral photoresponse are still unknown. In this work, we fabricated an ITO/CdS/Si heterojunction using chemical bath deposition (CBD) and investigated the pyro-phototronic effect under nonuniform illumination. The theory of electron-hole pairs’ generation, separation, and carrier diffusion was carefully considered to understand the underlying mechanisms. Our experimental findings revealed that the device exhibited an exceptionally high position sensitivity (PS) of 1061.3 mV/mm, surpassing the generally observed PS of 655.1 mV/mm induced by single photovoltaic effect by 160.5%. Meanwhile, the PSD demonstrated rapid response times of 0.01 and 0.04 ms, respectively. Moreover, the influence of ambient temperature and electrode distance on the pyro-phototronic effect was well analyzed. Notably, the PSD exhibited remarkable stability even at ambient temperatures up to 150 °C. Despite the considerable working distance of 11 mm, the PS of the PSD remained at 128.99 mV/mm. These findings provide valuable theoretical and experimental foundations for optimizing the design and implementation of high-performance large working distance PSDs.

Optical design of Fery imaging spectrometer with large working distance and long slit length

This article demonstrates a imaging spectrometer using Fery prism with large working distance and long slit length. Two spherical lenses are inserted between the double-convex lens and the Fery prism to enlarge the clearance distance. Using this method, an imaging spectrometer with a 37.2° field of view and F# 2.2 is designed, and the measured spectrum ranges from 400 nm to 900 nm. The performance is analyzed and evaluated. Laboratory testing results prove the excellent optical performance. This compact, cost-effective spectrometer with high performance and less stray light has a huge potential for broadband space exploration.

Methods for extending working distance using modified photonic crystal for near-field lithography

Near-field lithography has evident advantages in fabricating super-resolution nano-patterns. However, the working distance (WD) is limited due to the exponential decay characteristic of the evanescent waves. Here, we proposed a novel photolithography method based on a modified photonic crystal (PC), where a defect layer is embedded into the all-dielectric multilayer structure. It is shown that this design can amend the photonic band gap and enhance the desired high-k waves dramatically, then the WD in air conditions could be extended greatly, which would drastically relax the engineering challenges for introducing the near-field lithography into real-world manufacturing applications. Typically, deep subwavelength patterns with a half-pitch of 32 nm (i.e., λ/6) could be formed in photoresist layer at an air WD of 100 nm. Moreover, it is revealed that diversified two-dimensional patterns could be produced with a single exposure using linear polarized light. The analyses indicate that this improved dielectric PC is applicable for near-field lithography to produce super-resolution periodic patterns with large WD, strong field intensity, and great uniformity.

Stable nanodepth and nanogram level material removal in electrochemically induced chemical etching of fused quartz

The minimum and stability of material removal are critical determinants of the accuracy limitations in precision engineering. This study explores electrochemically induced chemical etching (ECICE) as a method to achieve nanogram-level, low-cost, stress-free, and stable material removal of fused quartz. A modeling analysis of the etching process coupled with testing of the current, potential, and etching pit topography reveals the key factors affecting removal minimum and stability. It is discovered that the removal minimum and stability are determined by both generation and diffusion of the etching active species HF2−. Due to concentration variation of the electrochemically active species NO2−, the generation rate of HF2− is unstable under constant potential processing. In contrast, constant current processing can produce stable HF2− and thus stable etching. Additionally, a large working distance and small insulation layer radius contribute to achieve precision and stable removal through accelerated diffusion of H+ and HF2−, which decreases the generation rate and concentration of HF2−. The processing current is linearly related to the mass removal over such a small nA-level current range. The proposed method achieves precision stable removal with a 40 nm for maximal etching depth and minimum material removal of 6 ± 0.5 ng at the nanogram level. This work can improve the capability for high-precision fused quartz parts without stress, thermal effects, and sediment contamination.

Videocapillaroscopic monitoring of microcirculation in rats during photodynamic therapy

The proposed approach to microcirculation assessment is non-invasive, informative, and can be implemented during photoactivation, and thus is perspective both for research tasks and clinical practice. The functional principles of the vasculature response to photodynamic exposure, identified using this technique, also foster the efficiency and safety of photodynamic therapy. The developed setup allows simultaneous photodynamic exposure and studying the microcirculation parameters by videocapillaroscopy and photoplethysmography techniques. Photodynamic action is carried out by 662 nm laser radiation with a power density of 15 mW/cm2 in continuous and pulsed modes. The imaging system of the setup consists of a large working distance microscope, an optical filter, and a monochrome camera. The illumination system is based on LED with a central wavelength of 532 nm. The acquired images were processed in order to obtain morphometric and hemodynamic microcirculation data in the inspected skin area. To compare the proposed approach with existing methods, we measured blood flow parameters by a laser Doppler flowmeter. We tested the developed setup on rats injected with a photosensitizer and obtained active vessel maps, photoplethysmograms, and skin vessel density values before, during, and after photoactivation in both generation modes. The proposed approach allows to reveal differences in the microcirculation response to photodynamic effects of low power densities in different modes, in particular, the discrepancy between the time from the start of exposure to the cessation of blood flow and the start of the recovery period.

Polarized tip-enhanced Raman spectroscopy at liquid He temperature in ultrahigh vacuum using an off-axis parabolic mirror.

Tip-enhanced Raman spectroscopy (TERS) combines inelastic light scattering well below the diffraction limit down to the nanometer range and scanning probe microscopy and, possibly, spectroscopy. In this way, topographic and spectroscopic as well as single- and two-particle information may simultaneously be collected. While single molecules can now be studied successfully, bulk solids are still not meaningfully accessible. It is the purpose of the work presented here to outline approaches toward this objective. We describe a home-built, liquid helium cooled, ultrahigh vacuum TERS. The setup is based on a scanning tunneling microscope and, as an innovation, an off-axis parabolic mirror having a high numerical aperture of ∼0.85 and a large working distance. The system is equipped with a fast load-lock chamber, a chamber for the in situ preparation of tips, substrates, and samples, and a TERS chamber. Base pressure and temperature in the TERS chamber were ∼3 × 10-11 mbar and 15K, respectively. Polarization dependent tip-enhanced Raman spectra of the vibration modes of carbon nanotubes were successfully acquired at cryogenic temperature. The new features described here including very low pressure and temperature and the external access to the light polarizations, thus the selection rules, may pave the way toward the investigation of bulk and surface materials.

Design method and construction of the Schwarzschild microscope with high numerical aperture for secondary ion mass spectrometry.

The Schwarzschild microscope is suitable for sample navigation in secondary ion mass spectrometry (SIMS) because of its advantages of a simple structure, large working distance, and good coordination with the ion extraction system. The high numerical aperture (NA) of the microscope significantly reduces diffraction effects, but the resulting high-order geometric aberrations seriously affect the imaging quality. In this paper, a novel design method of the Schwarzschild microscope with a high NA (0.47) was proposed. The aberration distributions and compensation methods were investigated through tolerance analysis. The results showed that the tilt and decenter tolerances become the dominant factors limiting the spatial resolution, which could only be improved by ensuring the alignment accuracy of mirrors. Finally, the spatial resolution of the microscope in the home-built SIMS reached 2.19 µm.

Fully planar laser-generated focused ultrasound transmitter

Laser-generated focused ultrasound (LGFU) has been attracting great interest due to its great potential in high-resolution ultrasound imaging and high-precision therapy. However, the existing methods suffer from distinct issues such as complicated film coating control, difficult technical transfer toward device miniaturization, and limited output acoustic pressure as well as operation condition. In order to explore an effective solution for LGFU working under more universal excitation conditions with a single nanosecond pulsed laser, a new strategy based on directly patterning the flat photoacoustic (PA) source is developed in this paper. For proof of concept demonstration, a planar PA transmitter is constructed using a chromium mask with transparent rings as the substrate. Considering the broadband nature of the generated PA signal, the effects of the ring structure on focusing characteristics are explored experimentally for the first time. Besides, its capability to provide a X-wave like focused acoustic field with output pressure at MPa level and a small lateral size of several hundred micrometers yet large focal depth of a few centimeters has been successfully demonstrated, which would benefit applications requiring large ultrasound working distance. Based on the same concept, various methods can also be involved to increase its adaptability and applicability further. • A planar ring-shape photoacoustic transmitter is used for focused ultrasound. • The effects of the ring parameters on the focusing characteristics are revealed. • X-wave like focused acoustic field with extended focal depth has been demonstrated.

Module for zooming in extended depth of focus in digital holographic microscopy

Microscopes with continuous magnification and a quick zoom reaction time are much needed for imaging of biological specimen. Here, we are proposing a module consisting of two electrically tunable lenses (ETL) to facilitate the digital holographic microscopy with a continuous variable zoom/magnification within the extended depth of focus of the microscope objective. The proposed module provides a large working distance for the movement of the sample as well as the elimination of break-off while switching objectives. The major benefit is that the image plane remains stationary throughout the zooming range within the extended focal depth. The range of both ETL currents for the continuous zoom operation is discussed. Post experimental calculations, over a 3.5 mm expanded focal depth, the zoom precision is determined to be 12 µm with a response time of ∼7 ms. The zoom ratio has been found to be in the range -28.75X to -122.5X experimentally. In the expanded depth of focus, the zoom ratios at different focus planes are presented with simulation and experimental results. Moreover, the quantitative information of micro samples at deep depths with high zoom ratios without sacrificing resolution over a field of view of 1.77° is provided. The results are provided for human red blood cells and a standard USAF chart present at different depths to demonstrate the feasibility of utilizing the proposed configuration for zooming into extended focal depths of objective for optically transparent samples.

Multifunctional high-performance position sensitive detector based on a Sb2Se3-nanorod/CdS core-shell heterojunction.

Sb2Se3 exhibits fascinating optical and electrical properties owing to its unique one-dimensional crystal structure. In this study, a Sb2Se3-nanorod/CdS core-shell heterostructure was successfully constructed, and the lateral photovoltaic effect (LPE), as well as the lateral photocurrent and photoresistance effects, were first studied. The measurements indicate that this heterojunction exhibits excellent lateral photoelectric performance in a broad range of 405-1064 nm with the best position sensitivities (PSs) of 525.9 mV/mm, 79.1 µA/mm, and 25.6 kΩ/mm for the lateral photovoltage, photocurrent, and photoresistance, respectively, while the nonlinearity is maintained below 7%, demonstrating its great potential in a novel high-performance multifunctional position sensitive detector (PSD). Moreover, this PSD could work well at different frequencies with good stability and repeatability, and the rise and fall times were deduced to be 48 and 180 µs, respectively. Besides, large linear working distances are achieved in this heterojunction PSD, and the PS can still reach 75.5 mV/mm even at an ultra-large working distance of 9 mm. These outstanding performances can be attributed to the high-quality Sb2Se3 nanorod arrays and the fast charge-carrier separation and transport properties of this core-shell heterojunction. This study provides important ideas for developing high-performance, broadband, large working distances, and ultrafast multifunctional PSDs based on the new core-shell heterostructure.

Design and Testing of a Compact Optical Angle Sensor for Pitch Deviation Measurement of a Scale Grating with a Small Angle of Diffraction

The design and testing of different optical heads were performed to evaluate the pitch deviation of a diffraction scale grating with a small diffraction angle. Based on the proposed pitch deviation evaluation method employing optical angle sensors based on laser autocollimation, a modified optical head with position-sensitive detectors (PSDs) is first designed and constructed by following the conventional optical configuration. Owing to the small angle of diffraction of the first-order diffracted beams, the modified optical head has a large working distance, resulting in poor sensor stability. Therefore, a novel and compact optical head employing a pair of small prisms is designed and developed to shorten the working distance of the optical head. An additional modification was also made to the developed compact optical head in such a way that collimator objectives (COs) in the laser autocollimation units are removed to improve the sensor sensitivity. Experimental comparisons were conducted using the three types of optical heads to verify the feasibility of the developed optical angle sensor with PSDs.

Design of a real-time fiber-optic infrared imaging system with wide-angle and large depth of field

A key limitation in the observation of instruments used in operations and heart sutures during a procedure is the scattering and absorption during optical imaging in the presence of blood. Therefore, we propose a novel real-time fiber-optic infrared imaging system simultaneously capturing a flexible wide field of view (FOV) and large depth of field infrared image in real time. The assessment criteria for imaging quality of the objective and coupling lens have been optimized and evaluated. Furthermore, the feasibility of manufacturing and assembly has been demonstrated with tolerance sensitivity and the Monte Carlo analysis. The simulated results show that the optical system can achieve a large working distance of 8 to 25 mm, a wide FOV of 120°, and the relative illuminance is over 0.98 in the overall FOV. To achieve high imaging quality in the proposed system, the modulation transfer function is over 0.661 at 16.7 lp/mm for a 320×256 short wavelength infrared camera sensor with a pixel size of 30 µm.

Long working distance high resolution reflective sample imaging via structured embedded speckle illumination

Imaging beyond the diffraction limit at longer working distances using enhanced microscopic configurations has always been a challenge for biological and engineering samples. Even though multiple techniques have been widely used for sub-diffraction limit resolution imaging, the achievable resolution was relying on the use of objective lenses with a high numerical aperture (NA). In the case of engineering samples, in addition to sustaining higher resolutions at large working distances, improving the signal-to-noise ratio (SNR) is also critical. In this context, we propose and demonstrate a concept for high-resolution imaging at large working distances, termed as structured illumination embedded speckle microscopy. An imaging resolution of ~ 310 ± 5 nm was achieved with a microscope objective (0.55 NA; 50X) having 11 mm long working distance using a Siemen's star as the test sample. The demonstrated microscopy is therefore envisaged for engineering applications that demands high-resolution, high SNR imaging at long working distances.

Imprinted Polymer-Based Guided Mode Resonance Grating Strain Sensors.

Optical sensors based on guided mode resonance (GMR) realized in polymers are promising candidates for sensitive and cost effective strain sensors. The benefit of GMR grating sensors is the non-contact, easy optical read-out with large working distance, avoiding costly alignment and packaging procedures. The GMR gratings with resonance around 850–900 nm are fabricated using electron beam lithography and replicated using a soft stamp based imprinting technique on 175 m-thick foils to make them suitable for optical strain sensing. For the strain measurements, foils are realized with both GMR gratings and waveguides with Bragg gratings. The latter are used as reference sensors and allow extracting the absolute strain sensitivity of the GMR sensor foils. Following this method, it is shown that GMR gratings have an absolute strain sensitivity of 1.02 ± 0.05 at 870 nm.

The Diamond I13 full-field transmission X-ray microscope: a Zernike phase-contrast setup for material sciences

The I13 transmission X-ray microscope at Diamond Light Source (DLS) has been designed to cover a broad range of energies and field of views. The beamline operates on an undulator source, and a multilayer monochromator can be used to work at a larger bandwidth to enable faster acquisitions. The experimental design includes large working distances for the optics to allow installing in situ sample environments. This paper presents the current state of the experimental system and shows some of the latest results.

Inductive Position and Speed Sensors.

Magnetic position and speed sensors are rugged and durable. While DC magnetic sensors use permanent magnets as a field source and usually have only mm or cm range, inductive sensors use electromagnetic induction and they may work up to a distance of 20 m. Eddy current inductive sensors equipped with magnetoresistive sensors instead of inductive coils can operate at low frequencies, allowing detection through a conductive wall. In this paper, we make an overview of existing systems and we present new results in eddy current velocity and position measurements. We also present several types of inductive position sensors developed in our laboratories for industrial applications in pneumatic and hydraulic cylinders, underground drilling, large mining machines, and for detecting ferromagnetic objects on conveyors. While the most precise inductive position sensors have a resolution of 10 nm and linearity of 0.2%, precision requirements on the industrial sensors which we develop are less demanding, but they should have large working distance and large resistance to environmental conditions and interference.

AFM-Based Spin-Exchange Microscopy Using Chiral Molecules.

Local magnetic imaging at nanoscale resolution is desirable for basic studies of magnetic materials and for magnetic logic and memories. However, such local imaging is hard to achieve by means of standard magnetic force microscopy. Other techniques require low temperatures, high vacuum, or strict limitations on the sample conditions. A simple and robust method is presented for locally resolved magnetic imaging based on short-range spin-exchange interactions that can be scaled down to atomic resolution. The presented method requires a conventional AFM tip functionalized with a chiral molecule. In proximity to the measured magnetic sample, charge redistribution in the chiral molecule leads to a transient spin state, caused by the chiral-induced spin-selectivity effect, followed by the exchange interaction with the imaged sample. While magnetic force microscopy imaging strongly depends on a large working distance, an accurate image is achieved using the molecular tip in proximity to the sample. The chiral molecules' spin-exchange interaction is found to be 150 meV. Using the tip with the adsorbed chiral molecules, two oppositely magnetized samples are characterized, and a magnetic imaging is performed. This method is simple to perform at room temperature and does not require high-vacuum conditions.

In Vivo Imaging of Cerebrospinal Fluid Transport through the Intact Mouse Skull using Fluorescence Macroscopy.

Cerebrospinal fluid (CSF) flow in rodents has largely been studied using ex vivo quantification of tracers. Techniques such as two-photon microscopy and magnetic resonance imaging (MRI) have enabled in vivo quantification of CSF flow but they are limited by reduced imaging volumes and low spatial resolution, respectively. Recent work has found that CSF enters the brain parenchyma through a network of perivascular spaces surrounding the pial and penetrating arteries of the rodent cortex. This perivascular entry of CSF is a primary driver of the glymphatic system, a pathway implicated in the clearance of toxic metabolic solutes (e.g., amyloid-β). Here, we illustrate a new macroscopic imaging technique that allows real-time, mesoscopic imaging of fluorescent CSF tracers through the intact skull of live mice. This minimally-invasive method facilitates a multitude of experimental designs and enables single or repeated testing of CSF dynamics. Macroscopes have high spatial and temporal resolution and their large gantry and working distance allow for imaging while performing tasks on behavioral devices. This imaging approach has been validated using two-photon imaging and fluorescence measurements obtained from this technique strongly correlate with ex vivo fluorescence and quantification of radio-labeled tracers. In this protocol, we describe how transcranial macroscopic imaging can be used to evaluate glymphatic transport in live mice, offering an accessible alternative to more costly imaging modalities.

Synchronous Vibration Measurements for Shrouded Blades Based on Fiber Optical Sensors with Lenses in a Steam Turbine.

It is important to obtain accurate dynamic vibrations of steam turbine blades for safe operation. Strain gauge (SG) measurements cannot fully obtain vibrations of all blades and nodal diameter (ND) details. The blade tip timing (BTT) technique could resolve this problem because it has the advantage of measuring all blades’ vibrations. This article proposed an improved BTT technique for measuring synchronous vibrations of shrouded blades in a steam turbine based on fiber optical sensors with lenses. The newly developed sensor was equipped with a Plano-convex lens, and the optical path was specifically designed to collimate the beam within a large working distance from 4 to 19 mm and improve the measuring accuracy. A method to search the spectra of all peak vibration amplitudes of all the blades was proposed to obtain the ND details of synchronous vibration. Experimental results validated the efficiency and accuracy of the proposed methods and sensors. Comparison results of BTT measurements with SG measurements showed that the relative errors of normalized frequency and strain were small and acceptable.

Focus on lasers, imaging, and microscopy

Focus on lasers, imaging, and microscopy