Liquid chromatography with diode array detection (DAD) or ultraviolet spectroscopic (UV) detection as the most important analytical technique for the accurate quantification of impurities in bisphenol compounds normally requires long analysis time for baseline separation of all components as well as highly concentrated sample solutions for the detection of trace levels. To expand the application possibilities to all stages of polymerisation processes, an easy and robust reversed phase separation for 7 known impurities of bisphenol-A (BPA) including 4-isopropenylphenol and its dimeric isomers, o, p-bisphenol-A and trisphenol was established in this work. The method has been validated for the detection with triple quadrupole mass spectrometry (qqqMS) and DAD. In the investigated concentration range 0.5 – 100 mg/kg, the linearity is verified for both detection techniques. The limit of quantification (LOQ) for each impurity is with 0.5 – 1.5 mg/kg for qqqMS and 15 mg/kg for DAD sufficient for the evaluation of BPA as a raw material for polymerisation processes. The separation time for all impurities is 10 min whereas earlier reported methods need a minimum of 25 to 40 min. In addition the necessary sample concentration of BPA could be reduced to 5 mg/mL compared to existing methods where the sample concentration typically is > 50 mg/mL. For all those reasons the validated method can be efficiently applied for frequent process monitoring. Furthermore, 4 additional impurities were detected and identified. Mainly these are reaction products from the isopropenylphenol structure in combination with confirmed impurities as trisphenol or chroman. The quantification of these structures was established with trisphenol as reference and two structures were detected in all BPA qualities of this study in a concentration range from 20 – 400 mg/kg.