Internal Voids Research Articles

Influence of the mass percentage of binders on the properties of LHC

This paper investigates the effects on the physical and mechanical properties and microstructure of lime-hemp concrete (LHC) materials at different binder mass ratios. A mixture of three cementitious materials, slaked lime, cement, and coal gangue powder, was used as binder, and hemp shives were used as concrete aggregate, and five test groups were designed, i.e., binder/hemp shives (B/H) mass ratios of 1.2, 1.4, 1.6, 1.8, and 2.0. The physical properties of LHC, including density, drying rate, water absorption, thermal conductivity coefficients, and mechanical properties (compressive strength and flexural strength) with different binder ratios were investigated. In addition, the microstructural properties of 56d LHC were investigated by SEM, XRD, and TG-DTG micro-scale analysis methods. The results showed that with the increase in binder content, the drying speed of LHC became faster, the thermal conductivity coefficients, compressive strength, and flexural strength increased, and the water absorption was just the opposite. With a fit ratio of 2.0, the strength is the greatest and the toughness is the best; with a fit ratio of 1.2, the thermal conductivity coefficient is the smallest and the insulation effect is the best. In addition, the hydration of the binder produced different forms of hydration products (CaCO3 and C-S-H), and the hydration products increased in quantity with the increase of the binder, resulting in stronger CaCO3 and C-S-H diffraction peaks. The hydration products produce a better bond with the rough cannabis particle surface, filling the internal voids of the LHC, improving the density of the material, and enhancing the mechanical properties of the material.

Effect of Waste PET Fiber on the Mechanical Properties and Chloride Ion Penetration of Emergency Repair Concrete for Road Pavement.

This study evaluated the effects of adding waste PET fibers on the mechanical properties and chloride ion penetration of latex-modified ultra-rapid hardening cement concrete used for emergency road pavement repairs. The primary experimental variable was the content of waste PET fibers. The mechanical properties of the concrete were evaluated through compressive strength, flexural strength, and splitting tensile strength tests. Its durability was evaluated through chloride ion penetration, surface resistivity, and abrasion resistance tests. The experimental results were compared with the quality standards for emergency repair concrete set by the Korea Expressway Corporation. As a result, this study has enhanced the strength and resistance to chloride ions of latex-modified concrete by incorporating waste PET fibers. In the mixture with 3.84 kg/m3 of waste PET fibers, the compressive strength was 29.9 MPa at 4 h and 42.5 MPa at 28 curing days. The flexural strength was 6.0 MPa at 4 curing hours and 7.0 MPa at 28 days, and the splitting tensile strength was 4.5 MPa at 28 days of curing. The chloride ion permeability amount and abrasion depth were 1081C and 0.82 mm, respectively. The mixture with 3.84 kg/m3 of waste PET fibers has superior compressive strength, flexural strength, splitting tensile strength, chloride ion penetration, and surface resistivity compared to the mixture with 7.68 kg/m3. This result means that the waste PET fibers caused poor dispersion and fiber-balling within the concrete, leading to loose internal void structures when incorporated at 3.84 kg/m3. However, the abrasion resistance test showed better results for the mixture with 7.68 kg/m3 of waste PET fibers than the 3.84 kg/m3 mixture. Therefore, the test results indicated that 3.84 kg/m3 of waste PET fibers is the most effective for latex-modified concrete used in emergency road pavement repairs.

Study on hydrophobic floc structure of coal particles based on fractal simulation

Utilizing the Matlab platform, two-dimensional diffusion-limited aggregation and three-dimensional diffusion-limited cluster aggregation models were established to simulate the hydrophobic flocculation of coal particles. The formation process of flocs aggregated by monomer particles and small groups was simulated from both plane and space perspectives. The gyration radius fractal dimension increased from 1.401 to 1.539 in the DLA model and from 1.623 to 1.729 in the DLCA model, indicating that the floc morphology gradually stabilized and the structure became increasingly regular during the hydrophobic flocculation process. The porosity of DLA increased from 0.762 to 0.851, indicating that the dendritic structure of flocs formed a spatial shielding effect on the planar structure, which prevented the particles from entering the flocs. In contrast, the porosity of DLCA first increased from 0.506 to 0.611 and then decreased, stabilizing at approximately 0.53, indicating that small groups filled the internal voids of flocs in the spatial structure, leading to a gradual increase in floc density. The surface fractal dimension and density of flocs were calculated using the surface fractal and hydrostatic sedimentation-terminal velocity theories, respectively, confirming the conclusions drawn from the simulation analysis.

Optimization of Steaming Conditions for Bellflower Root (Platycodon grandiflorus) Using K-Means Clustering-Based Morphological Grading System

Bellflower roots were categorized into three clusters (class 0, class 1, and class 2) using K-means clustering based on their morphological factors: length (282.8 ± 29.53, 138.75 ± 26.8, and 209.89 ± 20.49 mm), thickness (16.25 ± 2.82, 16.77 ± 3.35, and 16.52 ± 3.05 mm), and body shape coefficient (5.80 ± 1.15, 12.73 ± 4.82, and 7.95 ± 1.71). Internal void formation, a key quality factor for bellflower root, was analyzed under pre-steaming conditions, identifying temperatures between 20 and 25 °C as optimal for storage. Within the clustered class, steaming for a prolonged duration increased the formation of internal voids and caused a decrease in normal stress values, total dissolved solids (TDS), and pectin content. Class 0, with larger and thicker roots, exhibited higher internal voids (57% void rate) due to uneven heat distribution and incomplete starch gelatinization. Class 2 roots demonstrated better structural integrity, with a void rate of 26% and a stress value of 48 kN/m2. These findings highlight the importance of morphological classification and optimal storage temperatures to improve the quality of steamed bellflower roots.

Three-Dimensional Internal Voids and Marginal Adaptation in Deep Margin Elevation Technique: Efficiency of Highly Filled Flowable Composites.

To evaluate interfacial three-dimensional adaptation and internal voids of different flowable materials before and after cyclic fatigue in a simulated deep-margin elevation scenario. Eighty (n = 80) extracted premolars were selected and two Class II cavities were prepared. The mesial one with cervical margin 1 mm above the cementum-enamel junction (CEJ) and the distal one with cervical margin 1 mm below the CEJ. After performing adhesive procedures, specimens were divided into four groups according to the employed materials for 2 mm horizontal deep-margin relocation: nanohybrid composite (Clearfil ES2, Kuraray); conventional viscosity flowable composite (Tetric Flow, Ivoclar); medium viscosity flowable composite (Majesty ES2 Low Flow, Kuraray); high viscosity flowable composite (Majesty ES2 Super Low Flow, Kuraray). All restorations were finalized by oblique layering with nanohybrid composite (Clearfil ES2, Kuraray). To reveal interfacial and internal gap progression, specimens were scanned with a micro-CT (SkyScan 1172), before and after 500,000 cycles of mechanical chewing simulation (50 N, 1 Hz). Data were imported into Mimics software after smoothing and region growing. Only the 2 mm margin relocation volumes were considered. Obtained masks were analyzed for noise removal and volume calculation. At baseline, interfacial gap progression and internal voids, expressed in mm3, were collected and statistically analyzed with two-way ANOVA (α 0.05) for the variables substrate and restorative materials followed by Tukey post-hoc test. An additional two-way ANOVA test, followed by Tukey post-hoc test, was performed to evaluate variation in interfacial gap progression after mechanical aging. At baseline, the ANOVA test showed a significant difference for the variable restorative materials (p = 0.01). More specifically, the Tukey post-hoc test revealed that the highly filled medium viscosity composite performed better than the conventional viscosity composite at baseline for the interfacial gap. The internal voids ANOVA test at baseline reported no significant differences for the variable tested. Analysis of variance for internal gap progression after thermocycling showed no differences for both substrate and restorative material employed. Highly filled medium viscosity composite performed significantly better than the conventional viscosity flowable composite for what concern baseline interfacial gaps. Artificial aging with a chewing simulator and thermocycling did not affect interfacial gap progression on enamel and dentin. The tested restorative materials performed equally after aging.

3D structural analysis of the biodegradability of banana pseudostem nanocellulose bioplastics

X-Ray micro-computed tomography (XCT) is used to reveal the micro-structural changes of banana pseudostem nanocellulose bioplastic due to a biodegradation process initiated in a formulated composting media that allowed the growth of aerobic microflora. The bioplastic itself was made of nanocellulose, which was isolated from banana pseudostem using the 2,2,6,6-Tetramethyl-1-piperidinyloxy (TEMPO) mediated oxidation method, and polyethylene glycol (PEG) as plasticiser. XCT provided insights into the 3D structural change of the bioplastic identifying the degradation process at two scales. The results showed that the local thickness and roughness of the bioplastic increased after degradation, while the density of the material decreased. Enlarged voids and tunnels were observed in the material after degradation. The formation of these tunnels is attributed to the popping of internal PEG-containing voids because of the generation of gases, which after forming may further accelerate biodegradation by microbial activity.

Molten pool behaviors and printability of tungsten anti-scattering grids with extremely thin wall thickness fabricated via laser powder bed fusion

It is challenging for laser powder bed fusion (LPBF) technique to fabricate metal parts with a wall thickness below 100 μm. This work investigated the critical conditions for achieving extremely thin wall thickness in tungsten grids fabricated via LPBF. Specifically, the impact of low energy density on the printability of tungsten single tracks and grids via LPBF was comprehensively examined. A computational fluid dynamics approach was employed to develop a thermal fluid flow model for single tracks with multilayers in LPBF. The findings demonstrate that at low energy densities, single tracks exhibit four different morphologies, i.e., balling, discontinuity and winding, discontinuity but straightness, as well as continuity and straightness. The simulation model effectively elucidates the continuity of single tracks and provides insights into the governing mechanism of molten pool defects. Due to high thermal diffusion properties of tungsten, the continuity of its track relies on the connection of neighboring molten pools and is sensitive to scanning speed. The tungsten molten pools with low energy density can be categorized into shallow flows affected by surface morphology and deep flows influenced by internal voids of the powder bed. After multi-layer stacking, the track fluctuations and defects in single tracks accumulated into greater surface roughness and deteriorate thin-walled morphology. The critical conditions required for printing extremely thin walls were achieved, ensuring minimal merging of tracks between two layers by maintaining the energy density of 57J/mm3. Based on these findings, an ultra-thin-walled anti-scattering tungsten grid with a wall thickness of 86 μm and a wall roughness below 3.3 μm (Ra) was fabricated by LPBF. This work provides valuable theoretical insights and presents a viable methodology for determining the minimum energy density threshold and wall thickness essential for LPBF processing of thin-walled components.

3D-printed gummies with programmable internal voids as delivery systems for customized amounts of micronutrients

This paper explores the co-design and development of customizable 3D printed gummies as delivery systems for micronutrients. A virtual instrument, VI, enabling the consumers to select the main morphological properties and to indicate their own requirements of micronutrients was designed and developed. Such digital information was utilised to design gummies containing a void space to be filled with customised amounts of micronutrients. The starch-agar gel used for the printing experiments carried out at 50 °C through a narrow nozzle of 0.4 mm, showed a good printability performance obtaining a precise replica of the digital model. However, slight printing inaccuracies were observed through 2D/3D microtomographic images due to an improper solidification of the ink-gel during the closing movements of the voids. The 3D-printed gummies were described for the main texture properties showing low hardness (<6.87N), cohesiveness, and springiness which changed as a function of time.

Effect of nano-Al2O3 on the mechanical and microstructural properties of cement-based grouting material

The mechanical properties and microstructure of cement-based grouting materials are important parameters affecting the quality of geotechnical engineering, which are limited by the properties of added materials. At present, the exploration of nanomaterials has become the development trend of cement-based grouting materials. The results showed that NA can significantly improve the strength of NCBS. The most pronounced effect was observed when the dosage of NA was 1 %; compared with the control group, the strength increased by up to 45.2 %. NA particles accelerate the hydration reaction rate between cement and fly ash, generating a large amount of hydration products to fill the internal voids of NCBS. When the content of NA was 2–4 %, the strength gradually decreased with an increase in the amount of NA addition. The catalytic and microaggregate effect of the NA particles were the primary contributors to the improved NCBS mechanical properties. Aggregated NA particles were the main cause of the decrease in strength. Acicular ettringite, fibrous calcium silicate hydrate, and NA particles are the dominant components that effect the strength and microstructure of NCBSs. By comparing the relationship between NA and the strength of NCBS and the relationship between the curing age and the strength of NCBS, it was found that NA can better reflect the compressive strength of NCBS, and the correlation degree of NA to the strength of NCBS is 76 % higher than that of the curing age.

Influence of mixing time and coarse aggregate content on the flowability, setting time, and mechanical properties of cemented backfill

Ensuring the even mixing of filling slurry is crucial for the performance of cemented backfill, and mixing time is a key factor in this process. This study comprehensively investigates the effects of mixing time and coarse aggregate content on the fluidity, setting time, and mechanical properties of coarse aggregate backfill through extensive experiments. The results indicate no significant regularity in the vibration diffusion of the filling slurry at different regions of the mixing shaft, and positional variations do not impact the slurry's fluidity. Vibration diffusion initially increases and then decreases with prolonged mixing time, suggesting an optimal mixing time of within 9 minutes. The setting time of the filling slurry shows no significant variation across different regions of the mixing shaft. However, the setting time decreases with longer mixing times and increases with higher coarse aggregate content. The uniaxial compressive strength (UCS) of the backfill improves with extended mixing time, particularly benefiting early UCS. Incorporating an optimal amount of coarse aggregate, around 60 %, also enhances the UCS. Both extending the mixing time and adding an appropriate amount of coarse aggregate help suppress the expansion of destructive cracks and reduce internal void structures, thereby improving the overall mechanical properties of the backfill.

Characteristics of Open-Graded Friction Course Macrotexture and Macrostructure and Its Effect on Skid Resistance under Rainfall.

An Open-Graded Friction Course (OGFC) presents a rough surface and a porous structure and provides skid resistance under wet conditions, differing from that of a dense graded mixture. This study explored the distribution of surface macrotexture with depth in OGFC. Using cross-sectional images and semantic image segmentation techniques, the internal structure, porosity, and void size distribution were analyzed to assess the effectiveness of rainfall drainage. Skid resistance was evaluated with a British Pendulum Tester, focusing on the influence of surface macrotexture and internal macrostructure, particularly with regard to contact depth. Results show that finer gradations increase surface roughness peaks, which are concentrated near the top surface. In contrast, coarser mixtures exhibit a greater effective contact depth and more peaks with higher curvature. Finer gradations also result in lower porosity, greater void dispersion, and smaller average void diameters. During heavy rainfall, OGFC-13 exhibits the highest friction coefficient due to its effective contact, surface roughness, and internal voids, which facilitate water expulsion. This research provides insights into the skid resistance mechanism of OGFC in wet conditions and offers practical guidance for selecting the optimal gradation.

Localized surface plasmon resonance-enhanced photoelectrochemical immunoassay based on high-entropy yolk-shell Au@(ZnCdMnGaCu)xS

The yolk-shell structure has become a research hotspot in the field of photocatalysis in recent years due to its stability, movable yolk, and internal voids. However, yolk-shell has not been fully explored and applied in photoelectrochemical (PEC) immunoassays. In this work, a smartphone-based portable PEC immunoassay was constructed by using high-entropy yolk-shell Au@(ZnCdMnGaCu)xS as a photosensitive material, showing satisfactory detection with the assistance of localized surface plasmon resonance (LSPR). Specifically, a typical sandwich reaction introduces a detection antibody modified and labeled with gold nanoparticles (Au NPs) of alkaline phosphatase (ALP) into the system with the presence of prostate-specific antigen (PSA). Ascorbic acid (AA) content increased with increasing PSA and showed a linear enhancement of photocurrent at PSA concentrations of 0.01–50 ng mL−1 with a limit of detection of 8.94 pg mL−1. Additionally, the proposed assay technology not only provides a portable detection system for the immediate detection of tumor markers, but also offers a promising paradigm for the development of high-entropy materials.

Microwave self-healing characteristics of the internal voids in steel slag asphalt mixture subjected to salt-freeze-thaw cycles

Microwave heating technology can be used to repair freeze-thaw (F-T) cycle damage and cracks caused by the use of snow melting salts and de-icers in winter. This study utilized three different gradations of asphalt mixtures: AC-13, SMA-13, and OGFC-13, and enhanced their microwave absorption performance with steel slag (SS). The heating uniformity was evaluated through surface and internal temperature tests. Additionally, the mechanisms of damage and healing of the asphalt mixtures under salt freeze-thaw (S-F-T) damage conditions were explored using S-F-T cycles test and X-ray computed tomography scans (CT). The results showed that OGFC-13 exhibits a significantly higher rate of temperature increase compared to the other two types due to its stronger wave absorption capacity. The thermal hysteresis caused by steel slag leads to uneven spatial temperature distribution. The study recommends an optimal microwave heating time of 40 s for SS asphalt mixtures, which has minimal impact on the mixture structure, by defining an evaluation method for the uniformity index and local overheat ratio. After undergoing S-F-T cycles, the porosity of all three asphalt mixtures increased, particularly at the top and bottom of the specimens. Among them, OGFC-13 exhibited the poorest durability under S-F-T conditions, with the S-F-T cycles having a significant impact on medium-sized voids (0.15–0.6 mm). After microwave heating, AC-13 and SMA-13 showed good repair effects, with porosity levels returning to their initial states. For large voids (>2.36 mm) in OGFC, microwave heating may not effectively reduce the number of voids. Additionally, the healing rate of mixture specimens at certain mid-height ranges is higher due to elevated surface temperatures in these areas, making it especially effective in repairing F-T damage. This study shows that microwave heating of SS asphalt mixtures can improve the durability of pavement in cold regions. However, implementation challenges include the need for specialized equipment and potential uneven heating. Future research should explore optimizing microwave heating techniques to minimize local overheating and investigate the long-term performance of microwave-repaired asphalt pavements under various environmental conditions.

Response Patterns of Acoustic Wave Characteristics to Reservoir Petrophysical Parameters in Different Bedding Directions: A Case Study of Low- and Middle-Rank Coals in Xinjiang, China.

The physical properties of coal reservoirs, important parameters for evaluating the production potential of coalbed methane (CBM) resources, can be assessed nondestructively and in real-time using acoustic wave technology. In this study, we collected 48 low- and middle-rank coal samples oriented in different bedding directions from seven typical coal mines, encompassing the Zhunan, Tuha, and Kuqa-Bay coalfields in Xinjiang, China. We clarified the characteristics of the physical parameters (apparent density, fracture, porosity, and permeability) and acoustic wave of coal variations through acoustic wave, porosity, and permeability experiments, revealing the response law of acoustic wave characteristics to the physical parameters of coal. The results indicated that the acoustic wave velocity and dynamic elastic modulus (E d) of coal samples oriented in the perpendicular bedding direction are larger than those oriented in the parallel bedding direction; however, the dynamic Poisson's ratio (μd) of coal samples oriented in different bedding directions does not significantly differ. The existence of fractures significantly reduces the acoustic wave velocity and E d of the coal. The greater the apparent density of coal, the tighter its structure, resulting in a faster acoustic wave velocity. The larger the porosity of coal, the greater its internal voids, leading to a more pronounced attenuation of acoustic energy and a slower acoustic wave velocity. The more developed and interconnected the bedding fractures of coal bodies oriented in the parallel bedding direction, the higher their permeability, resulting in a smaller decrease in acoustic wave velocity. Conversely, the more developed the bedding fractures of coal bodies oriented in the perpendicular bedding direction, the more pronounced their attenuation of acoustic wave velocity. Finally, the regression equations for E d with the square of P-wave velocity (V P 2) and μd with the square ratio of V P to S-wave velocity (V P 2/V S 2) were established for coal. The study findings can help evaluate and predict the reservoir quality of coal seams, assess CBM, and improve the safety and efficiency of its extraction.

Mass Production of Multishell Hollow SiO2 Spheres With Adjustable Void Ratios and Pore Structures.

SiO2 multishell hollow spheres (MHSs) as supports have multiple porous layers and internal voids, which present notable advantages in regulating mass transport and chemical reactions. However, practical applications of SiO2 MHSs are severely hindered because of their high costs and low production efficiency issues. Herein, it is overcome these obstacles by developing a precursor hydrolysis method and demonstrate a cost-effective production of void-ratio tunable SiO2 MHSs on a large scale, which has a much lower cavitation temperature (25°C) and one order of magnitude decrease in cost. In addition, the new method can also be applied to fabricate TiO2 and SnO2 hollow spheres (HSs). In particular, an NH4Cl precipitation-pyrolysis strategy is developed to tune the pore diameters and pore distributions of SiO2 MHSs with different void ratios. SiO2 MHSs with varying void ratios and pore distributions have the broadest controlling release time ranges (30-430h). The precursor hydrolysis method and NH4Cl precipitation-pyrolysis strategy offer adequate stimulus to push forward SiO2 MHSs from laboratory-scale to industry-scale applications.

Internal Space Modulation of Yolk-Shell FeSe2@Carbon Anode with Peanut-Shaped Morphology Enabling Ultra-Stable and Fast Potassium-Ion Storage.

The poor cycling stability and rate performance of transition metal selenides (TMSs) are caused by their intrinsic low conductivity and poor structural stability, which hinders their application in potassium-ion batteries (PIBs). To address this issue, encapsulating TMSs within carbon nanoshells is considered a viable strategy. However, due to the lack and uncontrollability of internal void space, this structure cannot effectively mitigate the volume expansion induced by large K+, resulting in unsatisfactory electrochemical performance. Herein, peanut-shaped FeSe2@carbon yolk-shell capsules are prepared by modulation of the internal space. The active FeSe2 is encapsulated within a robust carbon shell and an optimal void space is retained between them. The outer carbon shell promotes electronic conductivity and avoids FeSe2 aggregation, while the internal void mitigates volume expansion and effectively ensures the structural integrity of the electrode. Consequently, the FeSe2@carbon anode demonstrates exceptional rate performance (242 mAh g-1 at 10 A g-1) and long cycling stability (350 mAh g-1 after 500 cycles at 1 A g-1). Furthermore, the effect of internal space modulation on electrochemical properties is elucidated. Meanwhile, ex situ characterizations elucidate the K+ storage mechanism. This work provides effective guidance for the design and the internal space modulation of advanced TMSs yolk-shell structures.

Optimization of Vibro-Acoustic Characteristics of Cold Rolled Sandwich Steel Cylindrical Shell with Internal Voids Using Response Surface Methodology

Optimization of Vibro-Acoustic Characteristics of Cold Rolled Sandwich Steel Cylindrical Shell with Internal Voids Using Response Surface Methodology

Probing microstructure evolution of Si/C anode for Li-ion batteries via synchrotron transmission X-ray tomographic microscopy

Holding great potentials as an excellent anode for Li-ion batteries, Si has received enormous attention, and its degradation theory has been enriched extensively based on various characterizations over time. To provide a more comprehensive diagnosis for current Si/C anodes, ex situ phase-contrast synchrotron transmission X-ray tomographic microscopy (TXTM) is applied to study a Si/C electrode sampled at representative cycling numbers. Through a series of data segmentations and identifications, three-dimensional Si/C electrodes are described in details with both global and localized structure features, which are rationally linked to the electrochemical characteristics as well as the previous discoveries. This successfully establishes an updated electrode-level failure process for common Si/C anodes where the electrode degradation is primarily initiated by the nonstop Si-phase pulverization with continually-expanded LixSi/electrolyte interface, and manifested as the internal void space expansion and the ever-growing electrode thickness. Bearing this in mind, multiple complementary and synergistic solutions towards limiting the intrinsic Si rupture and electrolyte decomposition should be developed to ensure a high-performance Si-based anode over long-term cycling for Li-ion battery in the near future.

Recent Progress in the Synthesis of 3D Complex Plasmonic Intragap Nanostructures and Their Applications in Surface-Enhanced Raman Scattering.

Plasmonic intragap nanostructures (PINs) have garnered intensive attention in Raman-related analysis due to their exceptional ability to enhance light-matter interactions. Although diverse synthetic strategies have been employed to create these nanostructures, the emphasis has largely been on PINs with simple configurations, which often fall short in achieving effective near-field focusing. Three-dimensional (3D) complex PINs, distinguished by their intricate networks of internal gaps and voids, are emerging as superior structures for effective light trapping. These structures facilitate the generation of hot spots and hot zones that are essential for enhanced near-field focusing. Nevertheless, the synthesis techniques for these complex structures and their specific impacts on near-field focusing are not well-documented. This review discusses the recent advancements in the synthesis of 3D complex PINs and their applications in surface-enhanced Raman scattering (SERS). We begin by describing the foundational methods for fabricating simple PINs, followed by a discussion on the rational design strategies aimed at developing 3D complex PINs with superior near-field focusing capabilities. We also evaluate the SERS performance of various 3D complex PINs, emphasizing their advanced sensing capabilities. Lastly, we explore the future perspective of 3D complex PINs in SERS applications.

Mechanical properties and damage characterization of 310S steel using laser ultrasonic inspection under extreme temperature condition

Abstract To evaluate the mechanical properties of 310S stainless steel under extreme working conditions, and realize the damage characterization function, in this study, the longitudinal wave and Rayleigh wave of materials are measured by the method of coaxial inspection on reverse surface and ipsilateral ectopic inspection, respectively, and surface cracks and internal voids are detected by the scanning laser source technology and transmission scanning detection, respectively. The detection methods are designed based on the energy distribution characteristics of Rayleigh wave and longitudinal waves in laser ultrasound. The laser ultrasonic detection systems coupled with a temperature loading device (high temperature: vacuum chamber; low temperature: refrigerating chamber) developed by the laboratory enable on-site monitoring of laser ultrasonic technology in harsh environments. Experimental results demonstrate that the error in mechanical properties (elastic modulus, shear modulus, Poisson ratio) is less than 5% over a wide temperature range (-180-1000°C). At 1000°C, surface cracks wider than 0.5mm and deeper than 1.9mm as well as internal hole defects larger than 1.0mm can be detected with an error rate below 5%.