Pure shear tests of textured magnesium AZ31B sheet samples were carried out using a 5 kN Kammrath & Weiss in situ tension-compression stage in a scanning electron microscope in combination with real-time electron backscatter diffraction lattice orientation mapping. The sample design was optimized to produce a pure shear stress in the central gauge zone. Distributions of the deformation twins were correlated with finite element simulations using a linear-elastic constitutive law considering large deformations to show that twins form in areas where the principal compressive stress σ3* is a maximum and that they form normal to the trajectories of that minor principal stress. Mappings of the same area at different load values revealed the formation and growth of individual twins and their relationship to the internal elastic strain of individual grains as indicated by the internal grain disorientation. All twins observed were of the extension type, with an 86.3° disorientation with respect to the parent grains. A more detailed study was conducted using transmission electron microscopy to correlate with the EBSD observations and to further elucidate the twin structures within samples.
Read full abstract