Interfacial Debonding Research Articles

Long-term properties evolution and life prediction of glass fiber reinforced thermoplastic bending bars exposed in concrete alkaline environment

Glass fiber reinforced polypropylene (GFRPP) bending bars have many advantages, such as high toughness, high durability, repeated molding and recycling, which can be used in concrete structures to replace steel stirrup for solving the problems of corrosion and service life. However, the changes in the properties of GFRPP bending bars during long-term use in alkaline concrete environments require further investigation. In the present study, GFRPP bending bars were immersed in alkaline solution at 20 °C, 40 °C, and 60 °C for as long as 180 d. The water absorption, hydrolysis, mechanical properties, and microscopic properties of the bending bars were evaluated to understand the long-term performance and mechanism of degradation. The bending bars had a higher saturated water absorption percentage and time along with a lower diffusion rate than the straight bars due to the presence of pores and micro-cracks formed during the bending process. The dissolution of the glass fibers in alkaline solution led to the partial mass loss of the GFRPP bars. Compared to the control, the tensile strength retention of the bending bars was 20.6%–56.0 %. The tensile failure mode changed from fiber bursting before immersion to shear fracture after immersion due to the decreased interfacial bonding strength and increased glass fiber brittleness. The primary degradation mechanisms were the etching of glass fibers, interface debonding, and increased void volume (∼23.7 %). The bending bars were more seriously eroded than the straight bars due to the twisting of the fibers and imperfect interfaces. The predicted degradation times of the GFRPP bending bars ranged from 1.7 years (Haikou) to 3.9 years (Harbin), corresponding to a stable tensile strength retention of 22.13 %. The results provide a basis for evaluating the durability and service life of GFRPP bending bars and promote the application of GFRPP composite stirrups in concrete structures.

Experimental and Numerical Simulation Investigation of Cement Sheath Integrity during Multi-Stage Fracturing in Offshore Tight Oil Reservoir

The integrity of the cement sheath is susceptible to failure during multi-stage fracturing. In this study, the failure mechanisms of cement sheath integrity during multi-stage fracturing in the A offshore tight oil reservoir wells were investigated. The cement samples were subject to triaxial compression test (TCT), triaxial cyclic loading test (TCLT), and permeability test. A full-scale device was constructed for cement sheath integrity experiments. Additionally, a 3-D finite element model was developed to simulate the interface debonding and the subsequent growth of micro-annuli throughout multi-stage fracturing. The results revealed that TCLT induced cumulative plastic deformation in the cement samples, resulting in a 10.7% decrease in triaxial compressive strength, an 8.3% decrease in elastic modulus, and a 150% increase in permeability. Despite these significant variations, no serious damage was caused to the cement sheath matrix. It was observed that gas leakage occurred at the 8th, 10th, and 14th cycles under cyclic loading with upper limits of 70 MPa, 80 MPa, and 90 MPa, respectively. After 15 cycles, the experimentally measured widths of micro-annuli were 117 μm, 178 μm, and 212 μm, which were in good agreement with simulation results of 130 μm, 165 μm, and 205 μm, respectively. These findings elucidate the causes of cement sheath integrity failure, providing insights into the failure mechanisms of cement sheath integrity during multi-stage fracturing.

Interfacial debonding in a thin plate bonded to a rigid substrate with a circular hole

Mode I fracture is a prevalent failure mode in adhesively bonded joints. This paper presents analytical and numerical solutions for the mechanical interaction of a thin plate bonded to a rigid substrate with a circular hole. Utilizing the bilinear cohesive law, the proposed solution is designed for the bonded joints subjected to uniformly distributed load and point load, respectively. The interfacial normal stress distribution and load-displacement response undergo three distinct stages: the initial elastic stage, followed by the elastic-softening stage, and culminating in the elastic-softening-debonding stage. The load-displacement response of the joints subjected to uniformly distributed load and point load diverges after debonding occurs. The load-carrying capacity of the former decreases rapidly, while the latter exhibits an opposite trend. Finite element (FE) simulation is conducted for numerical validation, demonstrating excellent agreement between the proposed model and FE results. The paper concludes by discussing the influences of hole radius, bond length, and the properties of the adhesive layer and thin plate on load-displacement response and the ultimate load. The findings suggest that higher bond strength and larger fracture energy of the adhesive, along with thicker and stiffer thin plates, contribute to achieving higher load-carrying capacity in bonded joints. Additionally, a longer bond length improves the load-carrying capacity for the joint subjected to the point load, with minimal impact for uniformly distributed loads once the bond length exceeds the effective bond length.

A prediction method of wellhead movement with consideration of interface debonding

The cementing cement all returns to the wellhead in offshore heavy oil thermal recovery wells, and the wellhead movement (WHM) still occurs frequently, indicating serious interface debonding between the casing and cement sheath during steam stimulation. Hence, a method for evaluating the bonding performance at the casing-cement sheath interface (CS interface) is proposed, by which the axial bonding strength, radial bonding strength, and friction coefficient at the CS interface are obtained. An elastic-plastic mechanical model of the casing-cement sheath-formation (CSF) system under temperature-pressure coupling is established to clarify the axial and radial bonding failure mechanisms at the CS interface. Based on the experimental results and mechanical model of the CSF system, the calculation method for the free casing and WHM model are established with consideration of cement return height (non-cementing section), cementing quality (poorly cemented section), axial bonding failure and radial bonding failure at the CS interface, by which the accuracy and reliability of this model have been verified by on-site data. The research results could provide a theoretical basis for real-time, intelligent, and scientific prediction of WHM.

Near-zero thermal expansion ZrW2O8/SiO2f wave-transparent composites: Interfacial anti-debonding structures based on polymeric films

The thermal stability of fiber-optic gyroscopes (FOGs) limits their application in harsh environments. This work utilized the unique water-retention properties of hyaluronic acid and the low-temperature cold sintering process combined to fabricate near-zero thermal expansion ZrW2O8/SiO2f composites with thermal resistance. Based on this novel process, the interface debonding of the composites is effectively suppressed and the mechanical and thermal properties of the composites are significantly improved (flexural strength increased by 69.47 %). Moreover, the interface anti-debonding structure reduces the interfacial polarization and reflection loss of the composites, and enhances the wave-transparent properties in the 2–18 GHz frequency range, with a minimum reflection loss of −0.21 dB. Furthermore, the interface anti-debonding structure of the composite provides creep resistance with enhanced sintering densities (increased by 13.61 %). Simultaneously, the composites achieve a controllable coefficient of thermal expansion (CTE) by regulating the liquid phase content and reach near-zero CTE (−0.246 × 10−6 °C−1 [30–300 °C]). Finally, finite element analysis and thermal shock experiments show that the anti-debonding interfacial structure has excellent thermal resistance, and the densest ZrW2O8/SiO2f composites exhibit the best thermal resistance due to minimal thermal strain during thermal shock, which is expected to meet the requirements of FOGs applications.

Temperature-dependent debonding behavior of adhesively bonded CFRP-UHPC interface

The adhesively bonded structure, comprising carbon fiber-reinforced polymer (CFRP) and ultra-high-performance concrete (UHPC), enhances structural strength while reducing brittleness and strain softening behavior. However, the adhesively bonded structure is inevitably influenced by temperature variations throughout its service life. When the adhesive layer's temperature surpasses the glass transition temperature (Tg), significant damage occurs to the bond layer joint. To investigate the debonding behavior of the CFRP-UHPC interface at various temperatures, a series of three-point-bending tests were conducted at room temperature, 120 %Tg, 150 %Tg, and 160 %Tg. This study introduced a temperature degradation factor, employing a proposed maximum load capacity prediction formula to adjust both the test results and data from other researchers. By adjusting the cohesion parameters with the temperature degradation factor, a temperature-dependent mixed-mode cohesive zone model (CZM) was developed. The model's validity was confirmed through finite element (FE) analysis, considering two distinct experimental scenarios. The paper concludes that the proposed model effectively simulates interface debonding behavior across varying temperatures.

Experimental analysis of 3D printed continuous carbon/glass hybrid fiber reinforced PLA composites: Revealing synergistic mechanical properties and failure mechanisms

AbstractThis study investigates the mechanical properties of continuous carbon/glass hybrid fiber‐reinforced polylactic acid (PLA) composites (HFRC) produced through the three dimensions (3D) printing process, comparing them with single carbon fiber‐reinforced PLA composites (CFRC). Initially, composite prepreg filaments are prepared using an impregnation device, followed by fabrication using a 3D printer. The mechanical performance results reveal a 13% increase in tensile strength for HFRC compared with CFRC. Due to differing elongation rates of carbon and glass fibers, HFRC exhibits two strength peaks, while CFRC demonstrates a 37% higher bending strength than HFRC. Scanning electron microscope images indicate that the tensile failure mechanism involves fiber brittle fracture and fiber‐matrix interface debonding, while the bending failure mechanism includes fiber pullout, fiber debonding, fiber cluster buckling, and interlayer interface failure.Highlights To realize the moldless rapid manufacturing of continuous hybrid fiber‐reinforced PLA composites. The stress–strain curves of single fiber‐reinforced composites and hybrid fiber‐reinforced composites are obviously different. Elucidating the effect of single fiber/hybrid fiber in composites on mechanical properties and failure mechanism according to micro‐morphology.

Experimental measurement and molecular dynamics simulation analysis of thermal aging performance in composite solid propellants

As a complex mixed system, the aging mechanism of high-energy composite materials involves the aging of each component itself, interactions between components, and transformation of microstructural and thermodynamic properties. The study of a single component or performance parameter has great limitations for elaborating the cognitive complexity of aging processes, making it difficult to reveal the underlying principles of physicochemical property transformation. Thus, it can only be applied as an empirical summary. In view of this, this study comprehensively utilized numerical analysis and experimental detection to explore the evolution of micromolecular conformation and changes in macro aging performance from four aspects of composite systems, including binder aging, plasticizer migration, bond interface debonding, and mechanical property transformation. There was good consistency observed between molecular simulation and thermal aging experiments, indicating that there was basically no post curing process for HTPB propellants using TDI as the curing agent. In the early stage of aging, scission chain was the main process and, in the later stage of aging, oxidation crosslinking the main process. Oxidative crosslinking increased the mean square radius of gyration and glass transition temperature of the binder system, reduced the peak value of radial distribution function, and revealed the reason for the change of propellant hardness and CC and CO double bond content. However, chain degradation increased the number of polar groups, enhanced intermolecular polarity, reduced the solubility parameter, and increased the free volume fraction of the mixed system and the dioctyl sebacate diffusion coefficient. This resulted in an increase in the tangent value of the HTPB propellant loss angle from 0.43 to 0.44° and a decrease in the glass transition temperature from 203.3 to 202.0 K. The binding energy at the interfaces of AP/HTPB and Al/HTPB increased first and then decreased, which was consistent with SEM images of bonding interfaces. The joint effect of binding energy and mechanical properties of the binder system promoted the transformation of the stress-strain curve of aging propellant.

Tensile strength of particle reinforced composite with interfacial debonding

Strength prediction of a particle reinforced polymer composite (PRPC) is still challenging. Although a PRPC is overall isotropic, it is more difficult to predict its tensile strength accurately than a continuous fiber reinforced composite (CFRC). One reason for this difficulty is that the calculation of stress fields of the constituents in a PRPC are complicated. The other reason is that the strength of a PRPC is significantly affected by interfacial strength, which is hard to be measured directly. In our research, the discount of the composite strength after debonding is attributed to the intensifying stress concentration. Two stress concentration factors (SCFs) are derived respectively to characterize the stress fluctuations in the matrix caused by the embedded particle before and after debonding. Based on the micromechanics Bridging Model and the matrix true stress theory, these two SCFs can be applied to evaluate the interface strength and the ultimate tensile strength of the composite from the properties of its component materials. Illustrations are presented to verify the efficiency of our theory and analyze the main influencing factors on the strength of the PRPC, including mechanical properties of component materials, particle size and volume fraction.

Curved Polymeric Sandwich Composites Subjected to Air Shock: An Experimental Investigation

BackgroundThe vulnerability of polymeric composite sandwich structures in marine applications to air explosions highlights a significant gap in our understanding of the dynamic behavior of the curved sandwich structures, which is essential for design improvements.ObjectiveThis study aims to explore the dynamic response and failure mechanisms of curved sandwich composite panels subjected to air-blast loading, providing insights into their structural integrity under such conditions.MethodsExperiments were performed using laboratory-simulated air shocks generated by a shock tube, employing high-speed photography and digital image correlation to measure deflections on the back surface of the panels. The panels, made with PVC closed-cell foam cores of two densities (H45 and H130), were tested across three curved geometries (radii of 112 mm, 305 mm, and infinity) under various boundary conditions.ResultsFindings indicate an increase in deformation with a decreased radius of curvature under simple support conditions, a trend that reverses under arrested displacement conditions. Moreover, a reduced radius significantly enhances panel strength and resistance to interfacial damage, with the primary failure mode transitioning from core shear cracking to interfacial debonding as core density increases.ConclusionsThe study reveals that the radius of curvature, boundary conditions, and core density significantly affect curved sandwich panels’ dynamic response and performance. Panels with smaller radii and higher core densities exhibit increased strength, though boundary conditions introduce variable effects on deformation behavior.

Evaluation of Performance of Cotton Fiber Reinforced Epoxy Composites

This experimental study explored the impact of varying weight proportions (5%, 10%, 15%, and 20%) of cotton fiber reinforcement in epoxy composites on compressive strength, Charpy impact strength, and water absorption characteristics. Concurrently, the interfacial properties were examined using Scanning Electron Microscopy (SEM). The inclusion of 15 wt.% cotton fiber notably enhanced compressive strength, displaying consistent improvement as cotton content increased until reaching 15 wt.%. Beyond this point, further increases yielded diminishing enhancements in compressive properties. EC20 demonstrated superior impact strength and energy absorption. Increased cotton concentrations improved impact properties due to the fibrous nature of cotton, enhancing energy dissipation and crack resistance within the epoxy matrix. Higher cotton content correlated with increased water absorption, aligning with cotton’s hydrophilic properties. The EC20 composite exhibited heightened water uptake and permeability, indicating the influence of elevated cotton concentrations. SEM analysis of fracture surfaces identified crucial features such as fiber pull-out, matrix cracking, interfacial debonding, and surface irregularities. These findings contribute significantly to understanding the inherent failure mechanisms in these composite materials.

The first composite increment: Dependency on placement technique for interaction behavior with maturing dentin-adhesive bond at pulpal floors in deep occlusal cavities – A comprehensive review

Abstract Introduction: When the traditional incremental technique is used for direct placement of composite resin in a deep occlusal cavity, each increment (2 mm or thicker) is individually cured where it undergoes hardening and shrinkage. As increments are bonded to all cavity walls, a constrained shrinkage develops in tooth, composite, and/or interfaces. In the first composite increment, this constrained shrinkage generates tensile stresses which are distributed in a nonuniform pattern within that increment, resulting in premature stressing of the dentin bond of the hybrid layer at the pulpal floor before it reaches full maturation. This premature stressing leads to initiation of interfacial debonding and propagation to form a microgap. This behavior is associated with persistent postoperative sensitivity and tooth pain, over the time, which subsequently results in restoration failure. Aims: This paper provides a comprehensive review on the first composite increment and its dependency on placement technique for the interaction behavior with the maturing dentin-adhesive bond at pulpal floors in deep occlusal cavities. Materials and Methods: The dental database was searched, and 59 articles were collected and included in this review, spanning the years from 1984 to 2023. Results and Discussion: Three biomimetic direct restorative techniques were reported in the literature for incrementally restoring large occlusal cavities. These techniques are the decoupling with time, the decoupling with fiber, and the decoupling with split-increment. They all aim at minimizing the generated shrinkage stresses in the first composite increment for protecting the developing dentin bond of the hybrid layer until it reaches full maturation and thus preventing the initiation and propagation of interfacial defects at pulpal floors of deep occlusal cavities. Finally, the restoration is completed by placing and curing successive increments of 1.5 mm each to fill the cavity; their number depends on the cavity depth. These increments can each be cured immediately following placement. Conclusions: In deep occlusal cavities, the interaction behavior between the first composite increment and the maturing dentin-adhesive bond at the pulpal floor depends on the technique used for the increment placement. This behavior is either favorable with the direct biomimetic techniques or unfavorable with the traditional incremental technique. With the direct biomimetic techniques, no premature shrinkage stressing of the dentin bond is induced at the pulpal floor. This prevents the initiation of interfacial debonding and propagation to form microgaps and results in the absence of postoperative sensitivity and persistent tooth pain.

Deformation and fracture of SiCp/Al composites under complex loading conditions: A simulation study

An accurate depiction of the deformation and fracture mechanisms of metal matrix composites is the key to their rational structure and property design. In the present work, the Advanced Guerson Tvergaard Needleman (AGTN) constitutive model is firstly combined with an algorithm to reconstruct realistic 3D microstructures within the finite-element framework. We employ this model to probe the elastoplastic response and fracture behaviors of aluminum matrix composites with different volume fractions of reinforcing particles (7, 14, and 21 %) and under various loading conditions (tension, compression and shear). Real microstructures are referred to reconstruct the three-dimensional model of the composites. The AGTN constitutive model is integrated with the micromechanical damage model, which is capable of independently describing the constitutive behavior of various components, including the elastoplastic damage of the metal matrix, particle-enhanced elastic-brittle failure, and the interfacial traction separation. By using the conventional SiCp/Al composite system as a model material, we examine the stress state of the matrix and fracture mechanisms under different loading conditions by using triaxiality, Lode angle and statistical analysis. In general, the damage of SiCp/Al composites can be attributed to interfacial debonding and particle fracture, whereas the latter dominates when the volume fraction of SiCp is high. Furthermore, the critical volume fraction for the transition of damage mechanisms is found to be largely dependent on the loading conditions. Our work provides a comprehensive understanding of particle-reinforced aluminum matrix composite under in-service conditions.

Effect of heat treatment on interface failure behavior in SiCf/PyC/SiC composites reinforced with Cansas-3 fibers

The influence of heat treatment on the correlation between interfacial mechanical properties and microstructure in CVI-SiCf/PyC/SiC composites was systematically investigated. The results reveal a progressive reduction in the average interfacial bond strength, interfacial shear stress, and interfacial debonding energy within the composites as the heat treatment temperature increases, especially beyond 1350 °C. This decline can be attributed to the attenuation of the SiCf/PyC interfacial bond strength arising from the contraction in fiber volume induced by the precipitation of Cansas-3 fibers. After push-in testing, SiCf/PyC/SiC composites heat-treated at or below 1350 °C displayed fibers in a compressed state. Conversely, composites exposed to extended heat treatment at 1400 °C or higher maintained fibers in an ejected state after push-in testing. Moreover, the composites heat-treated at 1450 °C and 1500 °C demonstrated fibers that were spontaneously ejected subsequent to cross-section polishing.

Design, preparation and mechanical properties of novel glass fiber reinforced polypropylene bending bars

Fiber reinforced thermoplastic composite bars offered the advantages of repeated molding, high toughness, and recyclability, making them a promising alternative to steel bars. For the stirrups applications in concrete structures, it was essential to develop efficient bending technologies for producing high-quality thermoplastic bending bars. In the present paper, the bending properties of glass fiber reinforced polypropylene (GFRPP) composite bars were investigated by experimental and theoretical methods. A novel bending fixture of GFRPP bars was specifically designed for GFRPP bars to ensure the reliable bending of the bars. Finite element simulation was employed to analyze the stress distribution of GFRPP bars, providing valuable insights into their mechanical behavior. Additionally, a bending strength model was developed based on the material mechanics, offering a theoretical framework for understanding and predicting the bending strength of GFRPP bars. Finally, the bending mechanism of bars was further revealed according to experimental and theoretical findings. The results of the study demonstrated that the specially designed bending fixture was successful in minimizing damage to the bending section of the GFRPP bars, leading to a significant improvement in bending strength retention of up to 43.2 %. Furthermore, the theoretical results and experimental test have a good agreement in terms of stress distribution and failure mode. The maximum strain in the transition zone between the straight section and the bending section of the GFRPP bars was nearly double that of the straight section at the same stress levels. With the increase of bending radius to diameter ratio from 3.0 to 7.0, the tensile strength of GFRPP bending bars increased by ∼7.9 %. The study identified the transition area between the bending section and straight section of GFRPP bars as the most critical failure point. The strength degradation mechanism during the bending were attributed to the shrinkage and torsion of inner fibers owing to the compression caused the local stress concentration, which caused the inner resin matrix to crack and interface debonding of fiber/resin, leading to the premature tensile failure.

Post-failure analysis of model resin-composite restorations subjected to different chemomechanical challenges

ObjectiveThe current study aimed to evaluate the effects of different combinations of chemical and mechanical challenges on the failure load, failure mode and composition of the resulting fracture surfaces of resin-composite restorations. MethodsThree resin composites were used to fill dentin disks (2 mm inner diameter, 5 mm outer diameter, and 2 mm thick) made from bovine incisor roots. The model restorations, half of which were preconditioned with a low-pH buffer (48 h under pH 4.5), were subjected to diametral compression with either a monotonically increasing load (fast fracture) or a cyclic load with a continuously increasing amplitude (accelerated fatigue). The load or number of cycles to failure was noted. SEM was performed on the fracture surfaces to determine the proportions of dentin, adhesive, and resin composite. ResultsBoth cyclic fatigue and acid preconditioning significantly reduced the failure load and increased the proportion of interfacial failure in almost all the cases, with cyclic fatigue having a more pronounced effect. Cyclic fatigue also increased the amount of adhesive/hybrid layer present on the fracture surfaces, but the effect of acid preconditioning on the composition of the fracture surfaces varied among the resin composites. SignificanceThe adhesive or hybrid layer was found to be the least resistant against the chemomechanical challenges among the components forming the model restoration. Increasing such resistance of the tooth-restoration interface, or its ability to combat the bacterial actions that lead to secondary caries following interfacial debonding, can enhance the longevity of resin-composite restorations.

Investigation of the effects of volume fraction, aspect ratio and type of fibres on the mechanical properties of short fibre reinforced 3D printed composite materials

AbstractMechanical behaviour of 3D-printed composite parts is affected by the volume fraction, aspect ratio and type of fibre reinforcement. Although in the literature experimental approaches have been used to characterise the effects of the above factors on the mechanical properties of 3D printed parts, time and cost of the manufacturing process as well as the uncertainty associated with a large number of experimental techniques are the key issues. This study aims to address these challenges by developing a methodology based on a multi-scale Finite Element (FE) analysis of representative volume element (RVE) of 3D printed composite parts to predict the effective orthotropic properties. To account for the effects of fibre features, RVEs were modelled considering variables of volume fraction, aspect ratios and type of short fibres. To study the main and interaction effects of the above variables on the mechanical properties of 3D printed composite parts, a structured approach based on the Design of Experiments is used. The FE stress analysis of the RVE provides an understanding about the potential failure modes such as interfacial debonding between fibres and matrix, interlayer and intralayer delamination that may occur in load-bearing 3D printed composite parts. The FE computed mechanical properties are validated against experimental data through a series of mechanical testing of flexure, Iosipescu, and short beam shear which were conducted in conjunction with the Digital Image Correlation technique. As a result, certainty is obtained in using the proposed approach for a fast iterative design of 3D printed composite parts prior to industrial applications.

Bond performance of NSM FRP–concrete interfaces with epoxy under chloride‐salt conditioned environments

AbstractConcrete in coastal areas is susceptible to structural damage caused by corrosion and expansion of reinforcement. Near‐surface mounted (NSM) fiber‐reinforced polymer (FRP) bars have become effective for strengthening damaged reinforced concrete structures. The bonding performance of NSM FRP bars in concrete is a key factor limiting their application and promotion in civil engineering. In this study, the influences of the conditioned environment, such as the chloride salt concentration, immersion time, and bond length of the FRP bar, on the bonding performance were investigated experimentally. First, material properties in a conditioned environment were studied. Subsequently, the failure mode, bond stress–slip curve, and bond strength of the NSM FRP bar in concrete were investigated. Finally, the microstructure and chemical composition of the materials were revealed using scanning electron microscopy and energy‐dispersive spectroscopy (EDS) images of the materials under environmental conditions. The transfer mechanism of NSM FRP bars in concrete with epoxy was revealed. The results showed that the failure modes of the pullout specimens can be divided into epoxy splitting failure and basalt fiber‐reinforced polymer (BFRP) pulling failure. The chloride‐salt concentration was a critical factor affecting the bond properties, and the longer the bond length, the lower the bond strength. The microstructure clearly shows that the degradation of the bonding behavior at the interface of the NSM FRP bar in concrete in a conditioned environment is attributable primarily to the resin damage of the epoxy, resulting in pit corrosion. There was no significant damage to the fibers in the FRP bar, and the degradation was primarily due to resin matrix damage and interfacial debonding. The EDS results showed that the degradation of the epoxy resin and BFRP bars was caused by CO bond and SiO bond fractures, respectively.

Mixed experimental-numerical method for quantitative measurement of mode II fibre/matrix interface debonding and comparison of fibre sizings in single short fibre composites

In short fibre composites, debonding cracks usually initiate from fibre tips and their growth is governed by the properties of the fibre/matrix interface. These properties are ideally acquired from a model test similar to the real composite, while excluding the effects of fibre fractures and the induced debonding interactions. Therefore, in this study, debonding growth was examined in detail, using novel single short fibre specimens, which were fabricated using a new methodology. These experiments were further complemented with a continuous fibre case study, where the established single fibre fragmentation specimens were evaluated. The progression of debonding and pull-out damages versus remote stress was studied for two fibre sizings utilizing real-time in-situ polarized light microscopy. A finite element model was built to obtain the fibre/matrix interfacial fracture toughness considering thermal residual stresses, friction and matrix plasticity, and a very good correlation was obtained between the model and the experiments.

Influence of duoplasmatron ion source plasma treatment on multi-axial knitted structure reinforced glass fiber composites

The present study investigates the impact of glow discharge cold plasma-induced duoplasmatron ion source on the mechanical properties of multi-axial knitted structure reinforced glass fiber composites. Analysis of failure location and mode in bending tests was conducted using the acoustic emission method. The results reveal that the tensile and bending strength of the multi-axial structure reinforced glass fiber composites treated with oxygen/nitrogen plasma had increased by 21.84% and 37.28%, respectively. In contrast, when treated with oxygen/argon plasma, the corresponding enhancements were 17.47% and 24.16%, respectively. These results indicate that oxygen/nitrogen plasma treatment yields superior mechanical properties to oxygen/argon treatment. The accumulated acoustic emission energy in the multi-axial structure reinforced glass fiber composites subjected to oxygen/nitrogen and oxygen/argon treatments was 25.49% and 62.39% lower than untreated samples, respectively. The failure mode observed in the untreated composites was matrix cracking, whereas the composites treated with dual plasma exhibited interface debonding. The dual plasma modification enhanced fiber wettability and surface roughness, facilitating increased contact area between the fiber and matrix and promoting the overall bonding performance between the two components. Taken together, our findings suggest that duoplasmatron ion source treatment enhanced the interface bonding and mechanical properties of the multi-axial structure reinforced glass fiber composites.