Injection Experiments Research Articles

Physical Variability in Meter-Scale Laboratory CO2 Injections in Faulted Geometries

Carbon, capture, and storage (CCS) is an important bridging technology to combat climate change in the transition toward net-zero. The FluidFlower concept has been developed to visualize and study CO2 flow and storage mechanisms in sedimentary systems in a laboratory setting. Meter-scale multiphase flow in two geological geometries, including normal faults with and without smearing, is studied. The experimental protocols developed to provide key input parameters for numerical simulations are detailed, including an evaluation of operational parameters for the FluidFlower benchmark study. Variability in CO2 migration patterns for two different geometries is quantified, both between 16 repeated laboratory runs and between history-matched models and a CO2 injection experiment. The predicative capability of a history-matched model is then evaluated in a different geological setting.

Core-Shell Structured Nanozyme with PDA-Mediated Enhanced Antioxidant Efficiency to Treat Early Intervertebral Disc Degeneration.

Early intervention during intervertebral disc degeneration (IDD) plays a vital role in inhibiting its deterioration and activating the regenerative process. Aiming at the high oxidative stress (OS) in the IDD microenvironment, a core-shell structured nanozyme composed of Co-doped NiO nanoparticle (CNO) as the core encapsulated with a polydopamine (PDA) shell, named PDA@CNO, was constructed, hoping to regulate the pathological environment. The results indicated that the coexistence of abundant Ni3+/Ni2+and Co3+/Co2+redox couples in CNO provided rich catalytic sites; meanwhile, the quinone and catechol groups in the PDA shell could enable the proton-coupled electron transfer, thus endowing the PDA@CNO nanozyme with multiple antioxidative enzyme-like activities to scavenge •O2-, H2O2, and •OH efficiently. Under OS conditions in vitro, PDA@CNO could effectively reduce the intracellular ROS in nucleus pulposus (NP) into friendly H2O and O2, to protect NP cells from stagnant proliferation, abnormal metabolism (senescence, mitochondria dysfunction, and impaired redox homeostasis), and inflammation, thereby reconstructing the extracellular matrix (ECM) homeostasis. The in vivo local injection experiments further proved the desirable therapeutic effects of the PDA@CNO nanozyme in a rat IDD model, suggesting great potential in prohibiting IDD from deterioration.

Migration behavior of fugitive methane in porous media: Multi-phase numerical modelling of bench-scale gas injection experiments

Two-dimensional multi-phase numerical simulations based on detailed laboratory experiments are used to provide insight into the key processes of methane migration in porous media and to analyze the suitability of a continuum approach for modelling gas migration at the intermediate bench-scale. The simulations were conducted using the multi-phase numerical model DuMux, including groundwater flow, transport of free-phase methane subject to capillary and buoyancy forces, kinetic-controlled dissolution of methane into the flowing groundwater, and advective-diffusive transport of dissolved-phase methane. Mass transfer kinetics are controlled by the water-gas interfacial area, avoiding the assumption of thermodynamic equilibrium which was shown not applicable under these conditions of high aqueous velocity in sandy materials.The model is applied to a series of 2D laboratory experiments in which gas-phase methane was injected near the bottom of a 1.5 m square vertical flow cell under a background flow gradient and with homogeneous and heterogeneous configurations. Simulations are compared to the observed behavior with respect to gas-phase mass distribution over time, gas-phase saturations, and to breakthrough of the dissolved-phase methane at selected monitoring points. In this first comparative study (simulations vs real data), insights are provided into the role of spatial property distributions on methane migration, in particular gas-phase pooling below low-permeability layers. Similar to the laboratory results, the simulations confirmed that the concentrations of dissolved-phase methane are strongly dependent on the structure of the gas-phase plume which in turn is influenced by the geology. We show that at the local metre-scale, kinetic-controlled mass transfer is needed to reproduce the dissolved-phase methane concentrations. Nevertheless, an assessment of capillary parameter values typically encountered in sandy aquifer materials suggests that an equilibrium approach could still be suitable for field-scale simulations.

Fault roughness controls injection-induced seismicity

Surface roughness ubiquitously prevails in natural faults across various length scales. Despite extensive studies highlighting the important role of fault geometry in the dynamics of tectonic earthquakes, whether and how fault roughness affects fluid-induced seismicity remains elusive. Here, we investigate the effects of fault geometry and stress heterogeneity on fluid-induced fault slip and associated seismicity characteristics using laboratory experiments and numerical modeling. We perform fluid injection experiments on quartz-rich sandstone samples containing either a smooth or a rough fault. We find that geometrical roughness slows down injection-induced fault slip and reduces macroscopic slip velocities and fault slip-weakening rates. Stress heterogeneity and roughness control hypocenter distribution, frequency-magnitude characteristics, and source mechanisms of injection-induced acoustic emissions (AEs) (analogous to natural seismicity). In contrast to smooth faults where injection-induced AEs are uniformly distributed, slip on rough faults produces spatially localized AEs with pronounced non-double-couple source mechanisms. We demonstrate that these clustered AEs occur around highly stressed asperities where induced local slip rates are higher, accompanied by lower Gutenberg-Richter b-values. Our findings suggest that real-time monitoring of induced microseismicity during fluid injection may allow identifying progressive localization of seismic activity and improve forecasting of runaway events.

A self-supervised learning framework based on physics-informed and convolutional neural networks to identify local anisotropic permeability tensor from textiles 2D images for filling pattern prediction

In liquid composite molding processes, variabilities in material and process conditions can lead to distorted flow patterns during filling. These distortions appear not only within the same part but also from one part to another. Notably, minor deviations in the dry fibrous textiles cause local permeability changes, resulting in flow distortions and potential defects. Traditional permeability models fall short in predicting these localized fluctuations, especially for anisotropic textiles, whereas reliance on homogeneous permeability models creates substantial discrepancies between forecasted and observed filling patterns. This study presents a self-supervised framework that determines in-plane permeability tensor field of textiles from an image of that textile in dry state. Data from central injection experiments is used for training, including flow images and pressure inlet data. This work demonstrates that this model proficiently predicts flow patterns in unobserved experiments and captures local flow distortions, even when trained on a relatively small dataset of experiments.

Development and Application of the Large‐Scale Simulation Experimental System for the In Situ Long‐Term Injection and Production of EGS

With the proposal of the double carbon target, the exploration, development, and efficient utilization of geothermal energy is an important field for the energy development. Meanwhile, there also exists a series of challenges. With regard to the injection and production process of enhanced geothermal system, researchers mainly focus on the numerical simulation. As the conceptual model is developed based on several assumptions, the results are unable to truly reflect the heat transfer and seepage process of the fluid. Unfortunately, there are few reports on the large‐scale physical simulation experiments. Considering the present research situation, we have developed a large‐scale physical simulation experiment system in which the in situ long‐term injection and production process of hot dry rock (HDR) can be simulated. The experimental system includes several components: high‐temperature and high‐pressure true triaxial chamber and loading system, multiwell injection system, acoustic emission monitoring system, and flow and temperature monitoring system. By designing the experiments, the performance evaluation of the temperature variation, fluid flow, and heat energy extraction in the long‐term HDR injection and production process can be completed. Taking the granite outcrop rock sample, which is from the Gonghe Basin in Qinghai Province, as an example, we have conducted the long‐term injection and production experiment. The production temperature and flow rate were monitored and discussed. The results showed that the experimental system can simulate the heat transfer and seepage process of the fluid. More working conditions can be designed for the research of the long‐term injection and production process. Hopefully, this will provide an experimental platform for the efficient development of HDR.

Towards a better comprehension of reactive transport coupling experimental and numerical approaches

In this work we focus on further understanding reactive transport in carbonate rocks, in particular limestones characterized by a bimodal pore size distribution. To this end, we performed injection experiments with CO2-saturated water on a sample of Euville limestone and monitored the experiments with a medical CT scanner. Microscanner imaging was performed before and after alteration. Experiments showed that permeability increased by nearly two decades due to the alteration process. This increase could be attributed to the formation of a preferential dissolution path visualized on the CT images. Microscanner images show that preferential dissolution areas are characterized by the presence of numerous enlarged macropores. The preferential dissolution path created therefore retains a porous structure and does not correspond to a wormhole-type channel. To provide further knowledge of the small-scale physics of reactive transport, we performed Lattice-Boltzmann simulations of flow in a numerically generated model 2D porous medium having geometrical and topological features designed to approach Euville limestone. We showed that the fluid velocity increased in nearly percolating paths of macropores. Considering the experiments, this means that the CO2-saturated water starts to enter high-velocity zones earlier than low-velocity zones, inducing an earlier onset of the alteration process and a more pronounced local dissolution. However, numerical results showed that the alteration of non-connected macropores leads to an increase of permeability much smaller than the experimentally observed one. To explain this fact we used effective medium modelling that permits predicting the variation in permeability as a function of the fraction of macropores and consequently as a function of alteration. It proved that as long as there is no alteration-induced percolating path consisting of macropores, the increase in permeability is relatively low as shown by the Lattice-Boltzmann simulations. An increase in permeability of several orders of magnitude is only observed when the macroporosity is close to the percolation threshold. This fact is in accordance with the experimentally observed results.

Regulating scramjet combustor mode transition using fuel distribution control

Dual-mode scramjets can operate efficiently over a range of flight speeds from moderate supersonic to hypersonic conditions. Depending on the fueling and flight conditions, the combustion mode operates in either a thermally-choked mode or a supersonic combustion mode. Direct-connect experiments were conducted using a laboratory-scale scramjet combustor with hydrogen as fuel, and its combustion mode transition behavior was characterized over various equivalence ratios. It was observed that the combustor became susceptible to combustion instability when mode transition was occurring naturally. To explore the possibility of actively triggering combustion mode transition while alleviating the combustion instability concerns, a new strategy of changing fuel injection distribution was formulated and a series of spatially distributed fuel injection experiments were conducted. The results showed that the critical amount of fueling for mode transition depends on the degree of fuel distribution. Subsequent experiments demonstrated that the combustion mode transition timing could be effectively controlled by scheduling spatial distribution of fuel injection. When fuel was injected at one location, most of heat release was concentrated near the cavity flame-holder, leading to thermal choking at a relatively low equivalence ratio. With distributed fuel injection, heat release became more evenly distributed across the expanding portion of the combustor, effectively delaying the mode transition to a higher equivalence ratio. Through the use of fast-acting solenoid valves, it was shown that changing fuel injection distribution could be used to trigger a timely combustor mode transition while holding the total fuel flow rate unchanged. When mode transition was actively triggered, the entire transition process occurred over a significantly shorter time scale compared to the natural mode transition process. The results indicate that combustion mode transition process could be controlled at the desired timing by actively scheduling fuel injection distribution, with reduced risks of encountering combustion instabilities while transitioning.

Phosphofructokinase family genes in grass carp: Molecular identification and tissue-specific expression in response to glucose, insulin and glucagon.

It is widely acknowledged that glucose serves as the primary energy source for organisms. However, fish exhibit persistent postprandial hyperglycemia and are thought to have low glucose tolerance. Glycolysis serves as the ubiquitous pathway for glucose catabolism, with phosphofructokinase (PFK) acting as a crucial rate-limiting enzyme in this process and playing an indispensable role. PFK is classified into three isoforms based on their major expression sites, i.e., PFKM (skeletal muscle type), PFKL (liver type) and PFKP (platelet type). In this study, grass carp (Ctenopharyngodon idella) was used as animal model and the open reading frame (ORF) sequences of six PFK genetic isoforms of grass carp were cloned. Real-time PCR was used to detect its tissue distribution, and expression changes in oral glucose tolerance test (OGTT), insulin and glucagon injection experiments. The results showed that the ORF of pfkla, pfklb, pfkma, pfkmb, pfkpa and pfkpb genes was 2343, 2340, 2355, 2331, 2364 and 2349bp in length, respectively. The results of tissue distribution showed that pfkla and pfklb, homologous to mammalian pfkl, exhibited low expression levels in the liver of grass carp, but were expressed at the highest level in the brain. Muscle-type pfkma and pfkmb mRNA were found to be highly expressed in both red and white muscle, with pfkmb also exhibiting high expression levels in the heart, while platelet type pfkpa and pfkpb showed high mRNA abundances in the brain and heart. Oral glucose administration stimulated pfkma and pfkmb mRNA expression in the red muscle, and up-regulated pfklb mRNA levels in the liver at 3h post treatment, but it suppressed liver-type and platelet-type PFK genes expression in the brain. The expression of pfkmb in white muscle and pfkmb and pfkpb in heart were promoted by insulin, whereas the expression of pfkla and pfkpb in the brain, pfkma and pfkmb in the red muscle, pfkma in the white muscle, and pfklb in the liver was suppressed by insulin. As for glucagon, it inhibited pfkma and pfkmb mRNA expression in the red muscle, as well as pfklb in the liver, but it up-regulated PFK genes expression in most tissues detected, such as brain (pfklb, pfkpa and pfkpb), white muscle (pfkma and pfkmb), liver (pfkla) and heart (pfkmb and pfkpb). Our results suggest that PFK family genes have different or even opposite expression patterns in response to glucose, insulin and glucagon stimulation in various tissues of grass carp, which may contribute to glucose intolerance in fish.

A ONE-WAY COUPLED APPROACH FOR MULTISCALE CHARACTERIZATION OF FILLING OF DUAL-SCALE FIBROUS REINFORCEMENTS CONSIDERING AIR COMPRESSIBILITY AND DISSOLUTION IN LUMPED FASHION

The filling characterization of dual-scale fibrous reinforcements is challenging due to the presence of subdomains with dissimilar permeabilities, existence of wicking effects, and combination of air compressibility and dissolution phenomena. These factors cause flow imbalances inside the representative unitary cell (RUC), which lead to void formation and influence the behavior of macroscopic field variables, affecting the parts manufacturing by liquid composite molding (LCM). Here, the filling characterization of woven fabrics used in LCM is done using one-way coupled simulations. Once RUC geometry is characterized by scanning-electron microscopy (SEM), and stereomicroscopy, standard thickness test, and resin viscosity are measured, the multiphase finite volume method-volume of fluid (FVM-VOF) model of ANSYS Fluent is used for the three-dimensional filling of the RUC, incorporating an experimentally calibrated air entrapment parameter (λ) to consider air compressibility and dissolution; then, a lumped function for the coupling term with macroscopic equations is obtained in terms of volume-averaged variables. This function is used in the equivalent Darcy macroscopic model, which is solved using a dual-reciprocity boundary element method (DR-BEM) algorithm. By considering a single value of λ during the simulation, neglecting wicking effects, and normalizing physical variables, unified injection pressure-independent results for the local tows saturation and normalized pressure fields at mesoscopic scale were obtained, as well as for global tows saturation and normalized pressure and fluid front profiles at macroscopic scale, thus simplifying the filling characterization of reinforcements. Numerical results are coherent with unidirectional injection experiments at both scales.

Generic Soft Error Data and Control Flow Error Detection by Instruction Duplication

Transient faults or soft errors are considered one of the most daunting reliability challenges for microprocessors. Software solutions for soft error protection are attractive because they can provide flexible and effective error protection. For instance, nZDC [1] state-of-the-art instruction duplication error protection scheme achieves a high degree of error detection by verifying the results of memory write operations and utilizes an effective control-flow checking mechanism. However, nZDC control-flow checking mechanism is architecture-dependent and suffers from some vulnerability holes. In this work, we address these issues by substituting nZDC control-flow checking mechanism with a general (ISA-independent) scheme and propose two transformations, coarse-grained scheduling, and asymmetric control-flow signatures, for hard-to-detect control flow errors. Fault injection experiments on different hardware components of synthesizable Verilog description of an OpenRISC-based microprocessor reveal that the proposed transformation shows 85% less silent data corruptions compared to nZDC. In addition, programs protected by the proposed scheme run on average around 37% faster than nZDC-protected programs.

Coupled Transport, Reactivity, and Mechanics in Fractured Shale Caprocks

AbstractShales are low‐permeability caprocks that confine fluid, such as CO2, nuclear waste, and hydrogen, in storage formations. Stress‐induced fractures in shale caprocks provide pathways for fluid to leak and potentially contaminate fresh water aquifers. Fractured shales are also increasingly considered as resources for CO2 sequestration, enhanced geothermal, and unconventional energy recovery. Injecting reactive fluids into shales introduces chemical disequilibrium, causing an onset of a series of dissolution, precipitation, and fines mobilization mechanisms. The reactions have rapid kinetics and significant impact on porosity and permeability; consequently, flow and storage properties of caprocks. While previous research has explored the separate effects of these reactions, this study aims to uncover their simultaneous occurrence and collective influence. This study unveils these highly coupled transport and reactivity mechanisms by tracking and visualizing the reaction‐induced alterations in the matrix, microcracks, and fractures of shales over time. We conducted brine injection experiments sequentially at pH 4 and 2 in a naturally fractured Wolfcamp shale sample while simultaneously imaging the dynamic processes using X‐ray computed tomography (CT). CT images are validated by finer resolution images obtained using micro‐CT and scanning electron microscopy. We also tracked the sample permeability and fluid chemistry using brine permeability and inductively coupled plasma mass spectrometry, respectively. Findings show that fluid primarily flowed through fractures, dissolving reactive minerals and mobilizing fines on fracture surfaces. Dissolution of fracture asperities under confining stress resulted in the closing of fractures. Clogging in narrow fracture pathways, caused by fines accumulation, diverted fluid flow into matrix pores.

Study of Orbit Motion of Hydrogen and Deuterium Beam Ions Toward Neutral Beam Injection Experiment in Thailand Tokamak-1

Thailand Tokamak-1 (TT-1) is a small tokamak under the operation of the Thailand Institute of Nuclear Technology. In our future plans, TT-1 has the feasibility of being equipped with external heating systems to achieve high-performance plasma operation and conduct physics associated with fast ions generated by the external heating system. One of the potential external heating systems under consideration is a positive-ion-source-based neutral beam injection (NBI) heating system. The primary source of fast ions for the NBI can be either hydrogen or deuterium-doped hydrogen beams. This study examines how hydrogen and deuterium ions, namely protons and deuterons, respectively, move in orbits, using the Lorentz orbit (LORBIT) code to track their full gyromotion. The energy of the ions has been varied between 200 eV and 40 keV. Three trajectory motions have been characterized, i.e., counter-passing ion, co-passing ion, and trapped ion. The average Larmor radius, dependent on the ion energies, has been investigated. The Larmor radius significantly increases with increasing ion energy in the case of trapped ions, while in the case of counter- and co-passing ions, the Larmor radius exhibits a slight increase with increasing ion energy. Furthermore, the pitch angle range of the lost ion in the TT-1 has been investigated. The results demonstrate the feasibility of utilizing a deuterium-doped hydrogen beam in TT-1 to study fast ion physics. To avoid a large number of lost ions, it is possible to use a deuterium-doped hydrogen beam with an energy not exceeding approximately 10 keV in the TT-1.

Lectin diversity and their positive roles in WSSV replication through regulation of calreticulin expression and inhibiting ALFs expression

In biological evolution, gene duplication (GD) generates new genes to facilitate new functions. C-type lectins (CTLs) in crayfish have been extended by GD to expand their family members. In this study, four CTL genes generated by GD were identified from Procambarus clarkii (PcLec1–4). Among these four genes, PcLec1 can also generate new isoforms with different numbers of tandem repeats through DNA slip mispairing. PcLec1–4 was widely expressed in multiple tissues. The expression levels of PcLec1–4 were upregulated in the intestine of P. clarkii upon white spot syndrome virus (WSSV) challenge at multiple time points. Further analysis indicated that GATA transcription factor regulated PcLec1–4 expression. RNA interference and recombinant PcLec1–4 protein injection experiments suggested that PcLec1–4 promoted the expression of calreticulin (PcCRT) and negatively regulated the expression of antimicrobial peptides, thereby promoting WSSV replication. This study contributes to the understanding of the function of CTLs produced by GD during WSSV invasion in crustaceans.

Critical Condition of the Depth Limit of Oil Accumulation of Carbonate Reservoirs and Its Exploration Significance in the Lower Ordovician of the Tazhong Area in the Tarim Basin

Critical Condition of the Depth Limit of Oil Accumulation of Carbonate Reservoirs and Its Exploration Significance in the Lower Ordovician of the Tazhong Area in the Tarim Basin

A cylinder block dynamic characteristics-based data augmentation method for wear state identification under data imbalance condition

The deterioration of the wear state in the key friction pairs will degenerate the performance of the axial piston pump. The wear rates differ under different wear states in practical applications. Therefore, the amount of monitoring data is significantly different under different wear states, which causes data imbalance problem. In addition, the distribution characteristics of the external signals are often drowned by environmental noise. To address these issues, a novel cylinder block dynamic characteristics-based data augmentation method is presented for wear state identification. Firstly, a cylinder block’s dynamic characteristics state perception method is proposed to obtain the time domain data. Then, to reduce the computing costs, the raw data is fused into multi-channel time–frequency domain data by the short-time Fourier transform (STFT) based method. Finally, the minority time–frequency data is augmented by the designed deep convolutional generative adversarial network (DCGAN). To verify the wear state identification performance of the proposed method, a convolutional neural network (CNN) is designed. Wear states injection experiments are adopted to verify the feasibility of the proposed method. The advantage of the developed method is that it obtains prominent data distribution characteristics from internal signals to enhance the performance of the data augmentation process.

Afferent and efferent connections of the secondary general visceral sensory nucleus in goldfish.

The secondary general visceral sensory nucleus (SVN) receives ascending fibers from the commissural nucleus of Cajal (NCC), or the primary general visceral sensoru in the medulla oblongata of teleosts. However, the full set of fiber connections of the SVN have been studied only in the Nile tilapia. We have investigated the connections of the SVN in goldfish by tracer injection experiments to the nucleus. We paid special attention to the possible presence of spinal afferents, since the spinal cord projects to the lateral parabrachial nucleus, or the presumed homologue of SVN, in mammals. We found that the SVN indeed receives spinal projections. Spinal terminals were restricted to a region ventrolaterally adjacent to the terminal zone of NCC fibers, suggesting that the SVN can be subdivided into two subnuclei: the commissural nucleus-recipient (SVNc) and spinal-recipient (SVNsp) subnuclei. Tracer injections to the SVNc and SVNsp as well as reciprocal injections to the diencephalon revealed that both subnuclei project directly to diencephalic structures, such as the posterior thalamic nucleus and nucleus of lateral recess, although diencephalic projections of the SVNsp were rather sparse. The SVNsp appears to send fibers to more wide-spread targets in the preoptic area than the SVNc does. The SVNc projects to the telencephalon, while the SVNsp sends scarce or possibly no fibers to the telencephalon. Another notable difference was that the SVNsp gives rise to massive projections to the dorsal diencephalon (ventromedial thalamic, central posterior thalamic, and periventricular posterior tubercular nuclei). These differential connections of the subnuclei may reflect discrete functional significances of the general visceral sensory information mediated by the medulla oblongata and spinal cord.

Experimental study on the gas desorption law in coal affected by dynamic water injection

Water from hydraulic technology affects the desorption of gas from coal seams. Gas desorption behavior is critical information for gas control in coal mines. In this study, a designed coal seam water injection simulation experimental device was utilized to conduct dynamic water injection experiments on coal samples at different adsorption equilibrium pressures, analyzing the gas desorption law under dynamic water injection, as well as the role of water replacement, water imbibition and water blockage in gas desorption. The results showed that water altered the gas desorption rate in coal, causing fluctuating attenuation of the desorption rate of a water-injected coal sample (WCS). Under the same adsorption equilibrium pressure, the relationship between the desorption rate of the WCS and the non-water-injected coal samples (NCS) underwent a transition in desorption time. In contrast to the NCS desorption curves, the WCS desorption curves lacked a rapid growth phase and exhibited only a slow growth phase and a stopping phase. Water imbibition and water replacement promoted the desorption of gas in the non-wet area during the water injection process, while it inhibited the desorption of gas in the wet area. Under the effects of water imbibition, water blockage, and water replacement, the discharge rate of WCS is greater than the desorption rate of NCS, indicating that water injection increases the total amount of gas desorption. The study results have significant implications for gas extraction and the prevention and control of coal and gas outbursts.

Permeability enhancement by CO2 injection and chelating agent stimulation for creating geothermal reservoirs in granite

Existing research indicates that to create geothermal reservoirs using CO2 injection, additional stimulation methods are necessary. N, N-bis(carboxymethyl)-L-glutamic acid (GLDA) injection has been predicted to increase the permeability of CO2 injection-induced cloud-fracture networks (CFNs) and could serve as an additional stimulation method. Nevertheless, the influence of differential stress, flow geometry, and scale on the characteristics of permeability enhancement by GLDA injection is yet to be clarified. Accordingly, this study experimentally elucidated the permeability enhancement characteristics of injecting a chelating agent in fractured granite under differential stress conditions as an additional method for creating geothermal reservoirs using CO2 injection. GLDA injection experiments were conducted on fractured-granite samples under conventional- and true-triaxial stress states under varying differential stress and pH conditions. Regardless of the differential stress and pH conditions, rock deformation and acoustic emission (AE) were negligible during the chelating agent flow-through experiments on the fractured samples, whereas similar permeability enhancement factors were achieved within the same duration. Thus, stress did not affect the permeability enhancement by chelating agent injections. The permeability enhancement factors were inferred to be high near the injection borehole because of the high viscosity of the solution. Therefore, reservoir stimulation should be conducted using low-concentration chelating agent solutions at constant injection pressures. The study provides insights into the stimulation strategies for creating geothermal reservoirs using CO2 injection.

Active‐Source Seismic Imaging of Fault Re‐Activation and Leakage: An Injection Experiment at the Mt Terri Rock Laboratory, Switzerland

AbstractWe conducted a time‐lapse seismic experiment utilizing automated active seismic source and sensor arrays to monitor a reactivated fault within the Opalinus clay formation at the Mont Terri Rock Laboratory (Switzerland), an analog caprock for geologic carbon storage. A series of six brine injections were conducted into the so‐called Main Fault to reactivate it. Seismic instrumentation in five monitoring boreholes on either side of the fault was used to continuously probe changes in P‐wave travel‐times associated with fault displacement and leakage. We performed time‐lapse travel‐time tomography on five hundred sequential data sets; this revealed a zone of decreased P‐wave velocity, up to 16 m/s, during each injection cycle, followed by a velocity increase during shut‐in. These results demonstrate varying elastic property perturbations, both spatially and temporally, along the fault plane during reactivation. We then interpreted these velocity changes in terms of fault dilation induced by pressurized fluids along the fault.