Influence Of Surface Finishing Research Articles

Influence of surface finishing by grinding on the cavitation erosion resistance of 316L and NiAl-bronze

Improving the mechanical properties of bulk and near-surface materials and alternating the dynamics of cavitating bubbles are two main methods to reduce cavitation erosion damage. Grinding and polishing, as two common surface finishing stages, can alter the cavitation erosion damage on metallic materials by affecting both the bubble dynamics and the mechanical properties of the surface. In this paper, the ultrasonic cavitation erosion resistance of 316L and NiAl-bronze alloys, each with two initial surface conditions of grinding and polishing is investigated, focussing on the material reaction. The mechanisms of material removal are discussed based on surface and subsurface observations to explain the effect of surface finishing on the cavitation erosion damage. After 8.5 h cavitation erosion testing time, a lower erosion mass loss was obtained for both alloys in the ground state as compared to the polished state suggesting that grinding can improve the cavitation erosion resistance of alloys. On the other hand, the polishing process improved the erosion resistance of NiAl-bronze at the early stages of cavitation. This is discussed in light of the two distinct surface characteristics of roughness and hardness, which, in turn, tend to increase and decrease cavitation erosion damage. Planar crystallographic boundaries and intermetallic-matrix interfaces were found to be the most susceptible sites to early erosion damage on the polished 316L and bronze, respectively.

Influence of surface finishing and printing layer orientation on surface roughness and flexural strength of stereolithography-manufactured dental zirconia

ObjectiveTo evaluate the effect of surface finishing and printing layer orientation on the surface roughness and flexural strength of three-dimensionally (3D) printed 3 mol% yttria-stabilized zirconia manufactured by stereolithography (SLA). MethodsNinety bar-shaped zirconia specimens (1 mm x 1 mm x 12 mm) were 3D-printed via SLA. After debinding and sintering, they were randomly divided according to the printing layer orientation: parallel (PR) or perpendicular (PD) to the tensile surface for bending test. Each group was submitted to a surface finishing protocol (n=15/group): unpolished (subgroup 0), with polished tensile surface (subgroup 1), and with polished lateral and tensile surfaces (subgroup 3). Roughness of tensile surface was determined using a contact sensor and surface morphology was analyzed under Scanning Electron Microscopy (SEM). Flexural strength, apparent elastic modulus, and Weibull parameters were assessed using a 3-point bending test. Fractured specimens were examined to identify failure origins. Finite element analysis was used to evaluate tensile stress peaks and failure risk. ResultsPR orientation exhibited higher strength, higher apparent elastic modulus, higher maximum principal stress peaks, and lower failure risk. For both layer orientations, groups with polished lateral and tensile sides (PR3 and PD3) were the strongest. SEM revealed that polishing led to changes in defect type, location, and size. SignificanceSLA zirconia shows different mechanical properties according to surface roughness and defects. Orienting the printed layers parallel to the tensile side improves its mechanical performance. Polishing can significantly improve its flexural strength. It is necessary to reduce the final product's surface roughness and large pores for its best performance.

Influence of surface finishing and heat treatments on the corrosion resistance of LPBF-produced Ti-6Al-4V alloy for biomedical applications

Additive manufacturing (AM) technologies are gaining increasing attraction for biomedical applications due to the granted customizability and optimal surface topography for osteointegration. Ti-6Al-4V is one of the most promising materials due to its biocompatibility. However, excessive ions release can occur, leading to a relevant immunologic response in the surrounding tissues. Despite the corrosion behavior of the conventionally-manufactured material being well known, it should be assessed for AM-processed components, as the effect of the unique superficial and microstructural features granted by the process is still quite unknown. The aim of this paper is the electrochemical evaluation of the passive current density of the laser powder bed fusion (LPBF)-processed Ti-6Al-4V alloy via potentiostatic tests, carried out at typical in-service potentials for biomedical implants. This parameter is correlated with the ion release rate of the alloy, a fundamental phenomenon to address to prevent possible inflammations caused by the implant. Different manufacturing conditions (surface finishing, heat treatment) and exposure time (0, 60 and 6000 h) were considered. The importance of performing these measurements over a long period (> 8 months) was demonstrated. In fact, despite the initial current densities being significantly affected by the surface and microstructural differences, the ion release rates converged for long-time exposures. The results also underlined the good corrosion resistance of the material. Poor corrosion performances, alongside with significant current densities development, were observed in the as-built condition. A pickling treatment demonstrated to mitigate such effect without compromising the unique surface finishing granted by the manufacturing technology.

The influence of surface finishing on laser heat treatments of a tool steel

Laser heat treatments (LHT) has received growing attention in the last years because of highly localized precision and manufacturing efficiency related to laser processing of moulds steel. Due of its strong resistance and ability to maintain hardness and strength at high temperatures, AISI P20 steel is one of the most widely used tool steel in the plastics injection mould industry.This work presents an experimental investigation on LHT using P20 mod. steel produced with different surface finishes. After mechanical surface finishing, the diode laser beam with 15 mm width was applied to the P20 specimens at 1060 ⁰C using a feed rate of 8.8 mm·s-1in an air and argon ambient. The influence of different LHT atmosphere conditions and specimen initial surface finishing on characteristics such as final roughness, microhardness and microstructure were comprehensively analyzed. The use of a controlled atmosphere during processing showed an increment in depth and hardness values of samples. Through 3D profilometer, it was possible to determine the samples roughness. Results showed that lower average roughness leads to higher hardness values close to the surface, while higher average roughness lead to a deeper heat-treated zone. Macroscopical analysis revealed the depth and width afftected by LHT. The microhardness results showed an increment from 300 HV to around 750 HV on laser heat-treated zone using a controlled environment. Optical microscopy analysed the microstructural changes into martensite between LHT and non LHT zones for all samples.

Fracture and viscoelastic behavior of novel self-adhesive materials for simplified restoration concepts

ObjectiveThe aim of the study was to offer a comparative perspective on the mechanical and viscoelastic behavior of currently developed materials for simplified restoration concepts. These materials have not yet been clearly assigned whether they are complex hybrids of already known material categories or new material classes. MethodsA dual-cured, bulk-fill, bioactive resin-based composite (alkasite), a resin-modified glass ionomer cements (RM-GIC) with novel polymerizable acid polymers, and a glass ionomer cement (GIC) with improved adaptation to an acidic environment were compared with regard to their macro-mechanical parameters (3-point bending test, 3-PBT), fracture mechanism, quasi-static and viscoelastic behaviour (instrumented indentation test, IIT), morphology and structural appearance of the filler system (SEM analysis). The influence of surface finishing was quantified on the outcome of the 3-PBT, while the influence of aging and frequency was monitored on the outcome of the IIT. One and multiple-way analysis of variance (ANOVA) with Tukey honestly significant difference (HSD) post-hoc tests (α = 0.05) and Weibull analysis were applied. ResultsSurface finishing strongly influenced the outcome of the 3-PBT for RM-GIC and GIC but not of the alkasite. The highest material reliability (Weibull parameter m) was found with the alkasite, irrespective of the curing mode. Ground specimens showed decrease reliability, except for the alkasite in the light-cured mode. The predominant failure mode originated from sub-surface defects (52.5%), followed by corner (25%), edge (18.1%), and crack arrest (4.4%). The effect of the parameter material on the quasi-static outcome of the IIT was highest on elastic/plastic parameters (p < 0.001; e.g. elastic indentation work, ηP2 = 0.875), was moderate on the Martens Hardness (ηP2 = 0.420), and was low on the Vickers hardness (ηP2 = 0.218). The viscoelastic parameters, in particular the loss factor (tan δ) allow a clear documentation of the ongoing acid-base setting reaction during aging of one month, which was more pronounced in the GIC than in the RM-GIC. The decrease in tan δ with aging for GIC and RM-GIC reflects the maturation process and increased brittleness, while the increase in tan δ with aging reflects the polymer plasticization in the polymer-based alkasite. ConclusionsThe mechanical and viscoelastic behavior depending on surface refinement, aging and frequency clearly allow to classify the currently developed materials for simplified restoration concepts into known material categories such as RBCs (alkasite), RM-GIC or GIC.

Influence of Surface Finishing on Corrosion Behaviour of 3D Printed TiAlV Alloy

Additive manufacturing is currently one of the promising methods for the fabrication of products of complex shapes. It is also used in medical applications, thanks to technological progress, which also enables the printing of metallic materials. However, the final products often have to undergo a final surface treatment. In this work, the influence of surface finishing on the corrosion behavior of the medical alloy Ti-6Al-4V prepared by the selective laser melting technique is studied. The samples were subjected to mechanical, chemical and electrochemical treatments. Corrosion behavior was investigated using DC and AC electrochemical techniques such as potentiodynamic and potentiostatic curves and electrochemical impedance spectroscopy. Furthermore, the influence of surface treatments on the possibility of localized corrosion attack was evaluated. The results showed that the surface treatments have a positive effect on the corrosion resistance and reduce the risk of crevice corrosion.

Analysis of the Influence of Surface Finishing on the Performances of Dies for HPDC

The Al-alloy die casting die is a sector where the operating environment imposes a very severe aggression to hot working tools. Steel grades for such application, techniques for their surface modification and specifically conceived lubricants are continuously improved so as to limit Al soldering. Within this scenario the interaction between lubricant and die surface and the effect of finishing levels of such surface is poorly studied. This paper deals with a study of the influence of dies surface roughness on the working behavior of a die casting lubricant and on surface damages of a tool steel grade. Tool steel samples were prepared for the research and two different levels of surface roughness (as polished and as finely sand blasted) were investigated. Apart from the base characterization of steels and surface, two specific test rigs were used to study the lubricant-tool steel surface-Al alloy interactions. One of test rig was devoted to study the coupling principles of tool die surface-lubricant, while the other test rig was used to perform a cyclic immersion test in molten Al-alloy. The derived data were compared to the experimental investigation of cracks and craters as provided by cycling with a correlation with the surface finishing level of samples.

Fatigue performances of selective laser melted Ti-6Al-4V alloy: Influence of surface finishing, hot isostatic pressing and heat treatments

In this study, a detailed evaluation on the effects of different surface finishing processes, hot isostatic pressing (HIP) and heat treatments on the fatigue performance of SLMed Ti-6Al-4V is conducted. It is found that surface finishing processes of turning, grinding, grinding followed by sandblasting and polishing can effectively reduce the surface roughness of as-SLMed surfaces (Rz = 68.66 μm) and significantly improve the fatigue performances. The HIP, HT-920 and HT-850-550 treatments can significantly improve the ductilities of SLMed Ti-6Al-4V due to the coarsening of α laths and formation of β grains. The ultimate tensile strengths (UTSs) and yield strengths (YSs) of HIPed and HT-920 specimens reduce more than 140 MPa, while those of the HT-850-550 specimens show no obvious reduction. The SLMed Ti-6Al-4V specimen has a fatigue limit lower than 300 MPa, while the HT-920 and HT-850-550 treatments enhance the threshold of crack growth and increase the fatigue limit to 350–400 MPa. The reduction or elimination of pores and the modification of microstructure in HIPed specimens both significantly extend the period of fatigue crack initiation, leading to an increased fatigue limit of 450–500 MPa.

Effect of surface finishing on the oxidation behaviour of a ferritic stainless steel

The corrosion behaviour and the oxidation mechanism of a ferritic stainless steel, K41X (AISI 441), were evaluated at 800°C in water vapour hydrogen enriched atmosphere. Mirror polished samples were compared to as-rolled K41X material. Two different oxidation behaviours were observed depending on the surface finishing: a protective double (Cr,Mn)3O4/Cr2O3 scale formed on the polished samples whereas external Fe3O4 and (Cr,Fe)2O3 oxides grew on the raw steel. Moreover, isotopic marker experiments combined with SIMS analyses revealed different growth mechanisms. The influence of surface finishing on the corrosion products and growth mechanisms was apprehended by means of X-ray photoelectron spectroscopy (XPS) and residual stress analyses using XRD at the sample surfaces before ageing.

Influence of surface finishing on fracture load and failure mode of glass ceramic crowns

Statement of problemCeramic restorations often require adjustments using diamond rotary instruments, which damage the glazed surface. The effect of these adjustments on the fracture behavior of these restorations is unclear. PurposeThe purpose of this in vitro study was to evaluate the influence of induced surface defects on the fracture load and mode of failure of lithium disilicate–based (LDS) glass ceramic restorations. Material and methodsPremolar crowns were obtained from LDS computer-aided design and computer-aided manufacturing blocks (n=60) and glazed. The crowns were bonded to dentin analog dies and divided into 5 groups (n=12), as follows: glaze; abrasion (diamond rotary instrument 2135); abrasion and reglaze; abrasion and polishing (diamond rotary instrument 2135F, 2135 FF, and polishing devices); and polishing. The topography of the crowns was examined by scanning electron microscopy, and roughness was measured. A compressive load (0.5 mm/min) was applied by a piston to the center of the lingual cusp until fracture. The fracture load was recorded and data were statistically analyzed by ANOVA and the Tukey HSD test (α=.05). Fractured crowns were examined to determine the fracture origin. ResultsPolishing and/or reglazing resulted in lower roughness than for the abraded group (P<.05), which did not affect the fracture loads (P=.696). Catastrophic fracture with origin at the intaglio surface was the mode of failure for all the crowns. ConclusionsThe experiment design successfully submitted the crowns to a clinical stress state, resulting in a clinically relevant failure. Reglazing or polishing were effective in reducing surface defects. Surface treatments had no effect on the immediate catastrophic failure of LDS crowns.

Chloride threshold value to initiate reinforcement corrosion in simulated concrete pore solutions: The influence of surface finishing and pH

The influence of steel surface finishing and pH of simulated concrete pore solutions (SCPS) on the chloride threshold value (CTV) was evaluated. Steel samples were analysed, with four different finishes: as received (T), diamond-polished (D), polished (P500) and pre-oxidized (DH). The studies were performed in SCPS with pH values of 11.6 and 13.5, and of different chloride concentrations. The electrochemical behaviour of the samples was assessed using open circuit potential, potentiodynamic polarization curves and scanning vibrating electrode techniques. The surface of the steel samples was observed by optical microscopy and SEM/EDS. The results showed that the samples were ranked D>DH>P500>T for the CTV after which pitting corrosion occurs. The highest chloride threshold value was found in D samples.

Influence of Surface Finishing on High-Temperature Oxidation of AISI Type 444 Ferritic Stainless Steel Used in SOFC Stacks

This research is focused on the study of the samples, approximatively 15 × 30 mm2 sized, that were mechanically cut from two sheets (0.4 and 0.2 mm thick, respectively) of AISI 444 Type ferritic stainless steel (FSS) (DIN 1.4521, Eu designation X2CrMoTi18-2); this material was in the ‘as-rolled’ state. Part of these specimens were treated superficially on one side using abrasive SiC papers with different average grit sizes (i.e., 46.2, 30.2, 18.3 μm) and diamond suspension (up to 1 μm) in order to obtain various surface roughness. Both the ‘as-rolled’ and superficially treated samples were then aged in a muffle furnace in static air according to a thermal cycle corresponding to the curing phase of an experimental glass used as sealing in the solid oxide fuel cell stacks. After aging, the chemical compositions and morphological peculiarities of the scale formed depending on the thickness of the samples and their surface state were studied by scanning electron microscopy, energy-dispersive spectroscopy, micro-Raman spectroscopy, bright field light optical microscopy. The obtained results show that all scales formed consist of an inner Cr2O3 subscale and an outer (Mn,Cr)3O4 spinel layer; the relationship between FSS grain size and scale microstructural features is consistent on the samples with mirror-like surface only; the scale thicknesses on SiC grinded samples are comparable; the scales covering the ‘as-rolled’ surfaces are morphologically similar to those grown on the surfaces finished with the 30.2 and 18.3 μm SiC papers, and their thicknesses show an intermediate situation between the abraded and the mirror-like specimens. The last described characteristics depend mainly on the surface and microstructural peculiarities resulting from the rolling process.

VLIV POVRCHOVÉ ÚPRAVY NA RYCHLOST ŠÍŘENÍ ULTRAZVUKU VE DŘEVĚ

Non-destructive diagnostic methods are very useful for monumental buildings. This paper deals with one of these technique, namely with ultrasound testing and influence of surface finishing on ultrasound velocity measured by means of device the Arborsonic Decay Detector. Surface finishing (Primalex – thick synthetic film of the surface finishing, Luxol – Extra – thin synthetic film of the surface finishing and Impranal Profi SL – thick acryl film the surface finishing) were selected and tested in this research. The transmittion time was measured and velocity was converted from it. This was compared before and after application of surface finishing.

High- and very high-cycle plain fatigue resistance of shot peened high-strength aluminum alloys: The role of surface morphology

The present paper is aimed at investigating the effect of shot peening on the high and very-high cycle plain fatigue resistance of the Al-7075-T651 alloy. Pulsating bending fatigue tests (R=0.05) were carried out on smooth samples exploring fatigue lives comprised between 105 and 108cycles. Three peening treatments were considered to explore different initial residual stress profiles and surface microstructural conditions. An extensive analysis of the residual stress field was carried out by measuring with the X-ray diffraction (XRD) technique the residual stress profile before and at the end of the fatigue tests. Fatigue crack initiation sites were investigated through scanning electron microscopy (SEM) fractography. The surface morphology modifications induced by shot peening were evaluated using an optical profilometer. The influence of surface finishing on the fatigue resistance was quantified by eliminating the surface roughness in some peened specimens through a tribofinishing treatment. The capability of shot peening to hinder the initiation and to retard the subsequent propagation of surface cracks is discussed on the basis of a model combining a multiaxial fatigue criterion and a fracture mechanics approach.

An experimental study on the influence of surface finishing on the weathering of a building low-porous limestone in coastal environments

Limestones used as building material are especially prone to weathering in coastal environments due to interactions between sea mist and the carbonate stone. Subtle variations of the commercial surface finishing may lead to differences in decay patterns and aesthetic properties due to salt crystallization. To explore this potentially contrasting behavior, tablets of rough and polished low-porous limestone were aged in a sea-salt spray corrosion chamber to simulate their exposure in a coastal environment. Different crystallization morphologies and relative proportions of soluble (halite) and less soluble (gypsum) salts were observed in the aged rough and polished surface samples. These morphologies are ascribed to the microtextural characteristics and the surface pore systems of the diverse (rough and polished) substrates that in turn influence fluid (saline solution) transport toward their interior, as well as the different salt solubilities interacting with the substrates. Polished surfaces exhibit little evidence of damage after the ageing test in contrast to the rough samples but do have conspicuous gypsum on the surface together with halite. The scarcity of gypsum on the rough surfaces, in addition to a more severe change in the porosity system, suggests that salts penetrate deeper when the stone surface is not polished. Potential decay induced by salt crystallization pressure is therefore minimized when the stone surface is polished. However, polished surfaces show more significant changes in luminosity and chroma after the ageing test, and so are less attractive from an aesthetic point of view. Surface finishing is thus an important feature that needs to be characterized for a better understanding of the weathering behavior of building stones used in coastal environments.

Influence of Surface Finishing on the Oxidation Behaviour of VPS MCrAlY Coatings

CoNiCrAlY coatings were produced by means of the vacuum plasma spraying (VPS) process onto CMSX-4 single crystal nickel superalloy disk substrates. As-sprayed samples were annealed at high temperatures in low vacuum. Three kinds of finishing processes were carried out, producing three types of samples: as-sprayed, mechanically smoothed by grinding, ground and PVD coated by using aluminum targets in an oxygen atmosphere. Samples were tested under isothermal conditions, in air, at 1000 °C, and up to 5000 h. Morphological, microstructural and compositional analyses were performed on the coated samples in order to assess the high temperature oxidation behavior provided by the three different surface finishing processes. Several differences were observed: grinding operations decrease the oxidation resistance, whereas the PVD process can increase the performances over longer time with respect of the as-sprayed samples.

Influence of Surface Finishing on Corrosion Behaviour of Mg-Al Hydrotalcite Doped Hybrid Sol-Gel Coatings on Al Alloy in Saline Environment

The behaviour of hybrid sol-gel coatings doped with hydrotalcite-like compound applied on AA2024-T3 alloy was investigated in the present work. The hybrid sol-gel coatings were prepared by copolymerization of 3-Glycydoxypropyltrimethoxysilane (GPTMS) and tetra-n-propoxyzirconium (TPOZ). Three different surface finishing on the aluminium alloy AA-2024-T3, grounded, chemical etching and degreased were studied. A sol-gel film with hydrotalcite 5% w/w was deposited by dip coating procedure. The presence of hydrotalcite particles was confirmed by means of X-ray diffraction technique. The different surface morphologies were characterised using mechanical profilometry. The corrosion resistance properties were studied by means of electrochemical impedance spectroscopy and salt fog spray cabinet. The results show higher barrier properties in grounded aluminium substrates.

Influence of surface finishing on flexural strength of veneered zirconia

Influence of surface finishing on flexural strength of veneered zirconia

Metal release and formation of surface precipitate at stainless steel grade 316 and Hanks solution interface – Inflammatory response and surface finishing effects

The influence of surface finishing (polishing and passivation) on the release of Cr, Fe, Ni from the stainless steel 316 implant materials to Hanks solution with or without H 2O 2 (simulating a body inflammatory response) was investigated. The surfaces were characterized by means of SEM EDXS, XPS and Kelvin Probe measurements before and after exposure to the synthetic body fluids. The total metal ions release rates are more than 10 times higher in the presence of H 2O 2, independently of the surface finishing. In the absence of H 2O 2, formation of a surface layer consisting mainly of Ca 3(PO 4) 2 was observed, most likely it was responsible for the observed decrease of the release rates.

Influence of Surface Finishing and Binder Phase on Friction and Wear of WC Based Hardmetals

At present, cobalt is the most commonly used binder material in tungsten carbide based hardmetals. Current research on sliding wear performance of these cemented carbides, however, reveals promising results for nickel binder as well. Test samples of WC-Co and WC-Ni hardmetals have been machined and surface finished by wire-EDM and grinding. From comparative dry sliding pin-on-plate experiments on wire-EDM’ed, ground and polished grades, correlations are derived between wear volume loss and friction on the one hand and contact pressure, sliding distance, binder phase and microstructure on the other hand. The lowest wear levels are encountered with polished cemented carbides. The EDM induced surface modification turns out to deteriorate wear resistance, especially during the running-in stage of sliding. These findings are in agreement with Xray diffraction measurements of the residual stress level in the WC phase.