Hot Work Tool Steel Research Articles

Durability of Forging Tools Used in the Hot Closed Die Forging Process—A Review

The article presents the classification of the wear mechanisms of forging tools. The durability of dies can be enhanced through a variety of methods, including the selection of appropriate hot working tool steel, the application of effective heat treatment, the utilization of advanced surface engineering techniques, and the incorporation of lubricating and cooling agents. Two popular methods of tool regeneration, such as re-profiling and laser regeneration, are presented. The issue of numerical wear prediction based on the Archard model, the correlation of this model with experimental results, low-cycle fatigue (HTLCF), and an alternative method based on artificial neural networks are discussed. The paper aims to present currently known wear mechanisms and the methods of increasing and predicting tool durability.

The Effect of Cryogenic Treatment on a High Co Bearing DIN 1.2888 Steel Used as Die in Hot Forging Process

Abstract Hot work steels used as dies in metal forming processes must endure harsh conditions, typically achieved through a martensitic structure. However, retained austenite can persist after martensitic transformation, negatively impacting mechanical properties. Cryogenic treatment (CT) refines martensite, reduces retained austenite, and increases fine carbide density, thus enhancing performance. DIN 1.2888, a hot work tool steel with high cobalt content (~10%) and low carbon content (~0.2%), is less studied concerning the effects of CT. The objective of this study was to investigate how cryogenic treatment affects the mechanical and microstructural properties of DIN 1.2888 steel. Samples underwent conventional heat treatment (HT) and CT at -100, -140, and -180°C for 6 hours, followed by double tempering. Various analytical methods, including X-ray diffraction (XRD), scanning electron microscopy with energy-dispersive X-ray spectroscopy (SEM-EDS), and Vickers Microhardness tests, were used to examine the samples. Wear mechanisms were evaluated through pin-on-disc tests under different loads, and impact toughness was measured both at room temperature and the working temperature of dies (350°C). Results indicated that lowering the cryogenic treatment temperature resulted in a slight increase in hardness values from 507HV for the heat-treated sample to 529HV for the sample treated at -180°C. Additionally, the impact toughness improved significantly, with values rising from 12.35J for the heat-treated sample to 23.44J at 350°C for the cryogenically treated sample at -180°C. Wear rates also decreased by approximately 50%, particularly at higher cryogenic treatment temperatures. The improvement in wear resistance was attributed to finer carbide precipitation and a more homogeneous distribution of carbides. These findings suggest that deep cryogenic treatment has a positive effect on DIN 1.2888 steel by decreasing retained austenite and increasing fine carbide density, leading to enhanced mechanical properties and extending the lifespan of the steel in die applications.

Tool life improvement for stamping dies in the coining process

ABSTRACT High temperature and high-speed pressing in minting operations lead to the failure of coin-stamping dies. As a result, new coining tools were required more frequently leading to lower operational productivity and higher production costs. This research has examined the effects of materials and surface coating selections on the tool life of the stamping dies in the coining process. The aim of this research was to explore the possibility of extending the tool life of stamping dies. The three kinds of materials under study were alloy tool steel, cold working tool steel, and hot working tool steel. Additionally, Titanium Nitride (TiN) and Chromium Nitride (CrN) surface coating materials using the Physical Vapour Deposition (PVD) process were investigated. The experiment results revealed that the hot working steel yielded the highest tool life of up to 1,300,000 coins, followed by cold working steel at 900,000 coins, and alloy tool steel at 600,000 coins. The CrN PVD coating provided up to more than 400,000 coins compared to TiN PVD coating on hot working tool steel.

On the Origin of Enhanced Tempering Resistance of the Laser Additively Manufactured Hot Work Tool Steel in the As-Built Condition

Abstract In laser additive manufacturing (AM) of hot work tool steels, direct tempering (DT) of the tool from as-built (AB) condition without prior conventional austenitization and quenching results in enhanced tempering resistance. To date, intercellular retained austenite (RA) decomposition, leading to a shift in secondary hardening peak temperature, and finer martensite substructure are reported to be responsible for such a behavior. In this work, authors aimed at studying the strengthening contributions by performing isothermal tempering tests for long times (up to 40 hours) at elevated temperatures (up to 650 °C) on DT and quenched and tempered (QT) specimens. The thermal softening kinetics and the microstructural evolution were evaluated with the support of computational thermodynamics. The results suggest that the main contributor to enhanced temper resistance in DT condition is the larger fraction of thermally stable and extremely fine (~ 20 nm) secondary (tempering) V(C,N) compared with QT. This could be explained by the reduction of available V and C in austenitized and quenched martensite for a later secondary V(C,N) precipitation during tempering, because of equilibrium precipitation of relatively large (up to 500 nm) vanadium-rich carbonitrides during the austenitization process. A complementary effect of the substructure refinement (i.e., martensite block width) in rapidly solidified highly supersaturated martensite was also quantified in terms of Hall–Petch strengthening mechanism. The significant effect of secondary V(C,N) was successfully validated by assessing a laser AM processed vanadium-free hot work tool steel in QT and DT condition, where no significant differences in strength and temper resistance between the two conditions were evident. Graphical Abstract

Wear mechanisms and failure analysis of a tool used in refill friction stir spot welding of AA6061-T6

Investigating tool wear in refill friction stir spot welding (RFSSW) is essential for understanding its limitations and improving its efficiency. Increasing the tool's service life is important to push the technology's readiness level and transfer the technology from the laboratory to industrial applications. In this study, the quasi-static lap shear performance of AA6061-T6 similar welded spots was investigated and tool wear was continuously monitored until tool failure at 3450 welding cycles. Furthermore, the fundamentals of the wear mechanisms in RFSSW were further elucidated. The investigation shows that it is possible to achieve steady quasi-static lap shear performance of the spot welds over advancing tool wear by adjusting the heat input to compensate for losses in frictional heat generation efficiency (related to tool profile changes by abrasion). A subsequent tool failure case analysis showed the main causes for the continuous wear degradation of the shoulder. Tool wear was driven by plastic deformation of the hot-work tool steel and subsequent break-out of tool steel ridges, introducing big hard particles into the contact region between the moving and rotating tools. In addition, the formation and detachment of Fe-Al intermetallic compounds counteract with the rotating tools and increase tool wear.

In-situ preheating: Novel insights into thermal history and microstructure of directed energy deposition-arc of hot-work tool steels

Directed Energy Deposition-Arc (DED-Arc/M) represents a promising approach to the production of complex and medium-sized parts, eliminating the need for specific tooling and the minimization of resource use. However, the inherent thermal conditions of DED-Arc/M, characterized by high cooling rates and successive reheating cycles, result in microstructures distinctly different from those observed in traditional cast materials. Nevertheless, the influence of thermal history on DED-Arc/M processed hot-work tool steels remains an insufficiently addressed topic in previous studies. Therefore, this work systematically investigates the effects of heat input and accumulation through assessing the thermal history and resulting microstructural changes during DED-Arc/M processing of the hot-work tool steel AISI H13 (X40CrMoV5-1). Accordingly, layer-wise heat input results in heat accumulation, leading to high interpass temperatures, significantly impacting the solidification and, thus, the microsegregation as well as the overall chemical homogeneity. By employing an innovative statistical approach that incorporates quantitative EDS data, the distribution of chemical elements was investigated. Furthermore, a novel computational procedure through the utilization of empirical and thermodynamic calculations was used to identify microstructural effects on the thermodynamic stability of retained austenite. This research offers vital insights into the microstructural dynamics of tool steels processed through DED-Arc/M, underlining the pivotal role of precise thermal management in tailoring material microstructures and, consequently, influencing the properties for unlocking the full potential of additive manufacturing for industrial applications.

High and very high cycle fatigue behavior of an additive manufactured hot-work tool steel

In the present study, the fatigue response of an additive manufactured H13 type hot-work tool steel is investigated across the High Cycle Fatigue (HCF) and Very High Cycle (VHCF) regimes. The primary focus encompasses the interpretation of fatigue strength models, the defect type analysis along with a detailed examination of crack initiation and growth mechanisms. Despite the tremendous development in AM technology, experimental data regarding advanced mechanical properties, and particularly fatigue behavior, are still limited. Here, microstructural analysis of a modified AMed H13 hot-work tool steel, a combination of HCF and VHCF testing methodologies implemented for the characterization of the fatigue behavior, as well as a thorough fractographic analysis of the fractured surfaces were performed. Results are compared with historical data of a conventionally ingot cast and forged grade to assess the influence of the AM process on the fatigue response of H13 hot-work tool steels. It proves to be comparable to the conventionally manufactured grade, showcasing the potential utilization of AM in the production of components used in high-demanding applications, and in hot work tooling applications. However, the type of critical defects identified in the AM grade was found to be process-induced, emphasizing the need to optimize process parameters to reduce both the number and size of defects and also to ensure component reliability and high performance in various industrial applications.

Melt Pool Changes Characterization in Laser-Processed H11 Hot Work Tool Steel Using Point-by-Point Scanning Mode towards LPBF Process Optimization.

Additive manufacturing techniques employing laser-based metal melting have garnered significant attention within the scientific community. Despite a decade of comprehensive research on the fundamentals of these techniques, there still remain unexplored facets related to heat flux impact on metallic alloys' properties. Particularly, the effects of point-by-point laser operation on melt pool formation in metallic materials still remain unclear. Thus, this study focuses on the implications of laser metal melting, particularly investigating a point-by-point laser mode operation's influence on melt pool formation and its geometry in the phase-transformation-sensitive material H11 hot work tool steel. To examine the melt pool, singular laser tracks with various laser parameters were scanned across H11 sheet metal, which allowed for the elimination of layer-by-layer heat cycles' influence on the melt pool's microstructure. Samples were examined by means of metallography, revealing significant differences in the melt pool's depth, influenced mostly by exposure time rather than volumetric energy density. Heat-affected zone effects were found to have a limited range and thus potentially marginal effects in layer-by-layer manufacturing conditions. At the same time, retained austenite concentrations near fusion lines have been found within melt pools, suggesting potential micro-segregation of the alloying additions. The results present guidelines towards laser melting processes optimization.

Effect of the Laser Cladding Parameters on Microstructure and Elevated Temperature Wear of FeCrNiTiZr Coatings.

In order to prepare coating with good friction and wear resistance at elevated temperature on the surface of hot-working tool steel, by using a CO2 laser, FeCrNiTiZr high-entropy alloy coating with different laser scanning speeds (360, 480 and 600 mm/min, respectively) was successfully fabricated by using laser cladding technology on the surface of H13 steel in this paper. Phase constitutions, microhardness, microstructure, and wear characteristics of FeCrNiTiZr coatings under different laser scanning speeds were analyzed. It was determined that 480 mm/min was the optimal laser scanning speed. The results showed that the coating at the scanning speed of 480 mm/min consists of a BCC phase with significant lattice distortion and high dislocation density; the crystal structure is cellular crystal and dendrite crystal. The coating demonstrates the highest microhardness (842 HV0.2), which is 4.2 times that of the substrate (200 HV0.2). Its average friction coefficients at room temperature and 823 K are approximately one-seventh and one-third of the substrate's, respectively, and its wear volume is reduced by about 98% and 81% under these conditions. Compared to the substrate, the coating underwent slight abrasive wear, adhesive wear, and oxidative wear at both room temperature and 823 K. In contrast, the substrate underwent severe abrasive wear, adhesive wear, oxidative wear, and even fatigue wear.

Role of oxidation in thermal fatigue damage mechanisms and life of X38CrMoV5 (AISI H11) hot work tool steel

Hot work tools steels, which are submitted to severe solicitations in service, are often damaged by thermal fatigue and corrosion. Interrupted Thermal Fatigue experiments were performed on X38CrMoV5 tool steel between 100 and 650 °C, in air and reduced oxygen partial pressure atmospheres after primary or secondary vacuum. A thermal and thermo-mechanical analysis by finite element method was carried out to estimate the strains and stresses undergone by the axisymmetric disc-shaped specimen during thermal cycling. The morphology, structure and phase composition of the oxide layer were analysed using scanning electron microscopy, energy dispersive spectroscopy and X-ray diffraction. It was shown that the thickness, homogeneity, structure, and compacity of the oxide multilayer formed on the specimen changed depending on test atmosphere. In air, crack initiation and propagation were strongly assisted by oxidation, leading to reduced fatigue life compared to inert atmospheres. Steel softening was highlighted in sub-surface, whatever the test atmosphere.

A New Cu-Alloyed Precipitation-Hardening Hot-Work Tool Steel

Abstract Hot-work tools for hot forming processes, such as die forging, are subject to complex loads that can often lead to premature tool failure. The present study attempts to reduce the main cause of failure of high-speed hot working tools, i. e., wear due to surface breakdown, with the aid of damage-tolerant microstructures. For this purpose, a hot-work tool steel is specifically alloyed with copper in order to form copper precipitations during the subsequent heat treatment, which increase the strength of the material and contribute to the reduction of dislocation movements. The aim is to close the property gap between the standardized direct-hardening and secondary-hardening hot-work tool steels.

High-Temperature Mechanical and Tribological Performance of W-DLC Coating with Cr interlayer on X40CrMoV5-1 Hot Work Tool Steel

High-Temperature Mechanical and Tribological Performance of W-DLC Coating with Cr interlayer on X40CrMoV5-1 Hot Work Tool Steel

Nanoindentation Creep Behavior of Additively Manufactured H13 Steel by Utilizing Selective Laser Melting Technology.

Nowadays, H13 hot work steel is a commonly used hot work die material in the industry; however, its creep behavior for additively manufactured H13 steel parts has not been widely investigated. This research paper examines the impact of volumetric energy density (VED), a critical parameter in additive manufacturing (AM), and the effect of post heat-treatment nitrification on the creep behavior of H13 hot work tool steel, which is constructed through selective laser melting (SLM), which is a powder bed fusion process according to ISO/ASTM 52900:2021. The study utilizes nanoindentation tests to investigate the creep response and the associated parameters such as the steady-state creep strain rate. Measurements and observations taken during the holding phase offer a valuable understanding of the behavior of the studied material. The findings of this study highlight a substantial influence of both VED and nitrification on several factors including hardness, modulus of elasticity, indentation depth, and creep displacement. Interestingly, the creep strain rate appears to be largely unaltered by these parameters. The study concludes with the observation that the creep stress exponent (n) shows a decreasing trend with an increase in VED and the application of nitrification treatment.

Investigation of the Influence of NiBSi/NiCrBSi Coatings Applied by Flame Spraying with Simultaneous Fusing on the Substrate Material

The aim of this research is to investigate the influence of nickel alloy type from the same group, the parameters of flame spraying, as well as the preparation of the substrate and the heat treatments of the substrate on the microstructure of the coating/substrate system. Due to the possibility of applying nickel alloys in corrective maintenance of tools used on elevated working temperatures, hot work tool steel X38CrMoV5-1 was selected as a substrate material. The investigation of the microstructure of the coating/substrate system was carried out according to the factorial design of experiment, where the input factors were varied on two levels. The factors that were varied are: Ni based self-fluxing alloys - NiCrBSi and NiBSi; distance of the burner from the workpiece - small (6 mm) and large (20 mm); preparation of the substrate - roughened and non roughened and the heat treatments of the substrate - soft annealed and tempered condition. Ni-based self-fluxing alloys were applied on samples (12,5 × 25 × 25 mm) by flame spraying with simultaneous fusing process. Analysis of the microstructures of the coating/substrate system was carried out on the Leica DM 2500M light microscope. After the conducted analysis the paper concluded that by spraying the selected coatings onto the X38CrMoV5-1 tool steel base, poor quality coatings are obtained, due to the appearance of cracks (NiCrBSi) or separation of the coating from the substrate (NiBSi). This is attributed to the formation of martensitic structure of the substrate after spraying and the presence of residual stresses.

The Effect of Cryogenic Treatment on W360 and E38K Hot Work Tool Steels

The present study examines the impact of cryogenic treatment (CT) on W360 and E38K hot work tool steels used in forging dies, subjected to conventional heat (HT) and CTs followed by double tempering treatment. Results reveal that CT facilitates the transformation of retained austenite from 4.9% and 2.5% for W360 and E38K steels, respectively, into martensite to an undetectable limit. Also, when compared to HT, CT at −180 °C results in about 3 times higher amount of the carbide precipitation for both steel types. In contrast, a slight increment in the hardness values with decreasing treatment temperature is observed. Notch impact test results indicate higher impact energy with lower CT temperatures, particularly notable in W360 steel. Although both steel types exhibit almost similar impact energy values at room temperature, E38K steel has ≈100% higher energy at 350 °C. DCT‐treated samples show improved wear resistance at lower cryogenic temperatures. Cryotreated W360 steel displays nearly 25% less wear rate than cryotreated E38K steel. The study underscores the suitability of W360 and E38K steels for hot work applications, with CT enhancing their mechanical and microstructural performance, particularly in W360 steel due to its higher carbide density.

Investigation of Energy Consumption and Surface Roughness in Hot Work Tool Steel (DIN 1.2367) and Cold Work Tool steel (DIN 1.2550)

Investigation of Energy Consumption and Surface Roughness in Hot Work Tool Steel (DIN 1.2367) and Cold Work Tool steel (DIN 1.2550)

Thermophysical properties and microstructure of 32CrMoV12-28 hot-work tool steel

Thermophysical properties and microstructure of 32CrMoV12-28 hot-work tool steel

Metallographic and Extraction Replica Methods for Characterization of Tungsten Heavy Alloy: H13 Clads

Tungsten heavy alloys are used in demanding high pressure die casting applications due to their high temperature strength, high thermal conductivity, and low thermal expansion. High cost limits applications to small sintered die inserts and manual gas tungsten arc weld repairs. A new tungsten heavy alloy consumable, Anviloy wire, was developed for automated cladding of hot work tool steel dies. Literature regarding characterization of tungsten heavy alloy die steel clads was lacking. Understanding base metal dilution effect on clad microstructure is critical but required new sample preparation methods. An Anviloy wire-H13 clad was made using hot wire gas tungsten arc cladding and analyzed with metallography. Samples were found to have grain boundary M6C carbide phase as-welded with the help of an alkaline sodium picrate etchant. An isothermally aged arc crucible melted sample of the same composition was characterized using metallography, scanning electron microscopy, and transmission electron diffraction. The clad representative arc crucible melted sample was subjected to isothermal aging at 725°C for 100 hours. Isothermal aging resulted in precipitation of a high volume fraction of intermetallic platelets. Using a new carbon extraction replica sample preparation method involving two chemical polishing steps, transmission electron diffraction of precipitates indicated they were mu phase intermetallic.

The effects of austenitization temperature on the microstructural characteristics and mechanical properties of Cr–Mo–V hot work tool steels with different nitrogen contents

Two kinds of Cr–Mo–V hot work tool steels with different nitrogen contents, i.e. High-N steel and Low-N steel, were heat treated to investigate phase transformation phenomena in the present study. Microstructure characterization revealed the existence of numerous particles within both steels, which could be further categorized as the following three types: large- (>150 nm), medium- (50–100 nm), and tiny-sized (<10 nm) particles. It should be noted that numerous nanometer-sized V (C, N) precipitates were randomly dispersed within the tempered martensite matrix. Fewer V (C, N) precipitates were found in the High-N steel than in the Low-N steel, which was consistent with the hardness test results. Microstructure analysis (EBSD) also revealed that the matrixes of both hot work tool steels consisted of primarily tempered martensite matrix with extremely low amounts of retained austenite, indicating that the retained austenite could be eliminated effectively by suitable tempering treatment, even in the High-N steel. On the other hand, from the impact toughness and hardness tests, it was found that a higher nitrogen content was beneficial in achieving higher impact toughness, especially at higher austenitizing temperatures, which could be ascribed to the smaller austenite grains in the High-N steel.

Comparison of Softening Behavior and Abrasive Wear Resistance between Conventionally and Additively Manufactured Tool Steels

Directed energy deposition (DED) is a powerful method for hard‐facing the existing tool components. Herein, three tool steel grades including a newly developed maraging steel (NMS), a cold work tool steel (V4E), and a high boron steel (HBS) are cladded on a hot work tool steel substrate. After tempering, the cladded tool steels are exposed to high temperatures at 600, 700, and 800 °C for 3 h to evaluate their softening resistance. The results show that all three tool steel grades have a significant hardness drop when the softening temperature reaches 700 °C. The investigated NMS has the lowest initial hardness in the tempered state but the best softening resistance. In contrast, HBS has the highest initial hardness but the worst softening resistance among the three steel grades. V4E tool steel has a moderate softening resistance compared to the other two steel grades. The factors contributing to the softening resistance have been discussed. Corresponding conventional tool steels are also adapted as references for comparison. Except for the NMS, the additive manufacturing tool steel samples have a better softening resistance than the conventional counterparts owing to more alloying elements trapped in the matrix. The abrasive wear resistance of the tempered and softened tool steels manufactured by DED and conventional methods is also evaluated and the wear mechanism is discussed. Besides the hardness, the free spacing λ between coarse hard particles is one of the major factors influencing the abrasive wear resistance.