A powder metallurgy approach was applied for the synthesis of an [Formula: see text] Ti-2Al-3Fe alloy. Blends of the elemental Ti, Al and Fe powders were compacted and subsequently sintered. High-frequency induction heating (HFIH) instead of conventional high-vacuum furnace heating was used for the sintering, due to its high efficiency. The effect of temperature on the level of densification, residual porosity and mechanical properties was studied. Electron dispersive spectrum analysis was used to study the dissolution and homogenization of the alloying elements. The results showed that a short induction sintering (IS) cycle in the range of 10–15 min is sufficient to achieve significant powder consolidation, evident by the increase of the density and mechanical properties. The residual porosity diminishes with the increase of the sintering temperature. Full dissolution of the alloying powders is completed after sintering at temperatures above those of [Formula: see text]- to [Formula: see text]-phase transformation.