Microstructure Of Heat Affected Zone Research Articles

Effect of Pre-Weld Heat Treatment on the Microstructure and Properties of Coarse-Grained Heat-Affected Zone of a Wind Power Steel after Simulated Welding

The effect of pre-weld heat treatment on the microstructure and low-temperature impact toughness of the coarse-grained heat-affected zone (CGHAZ) after simulated welding was systematically investigated through the utilization of scanning electron microscopy (SEM) and electron back-scattering diffraction (EBSD). The Charpy impact test validated the presence of an optimal pre-weld heat treatment condition, resulting in the highest impact toughness observed in the CGHAZ. Three temperatures for pre-weld heat treatment (690, 720 and 750 °C) were used to obtain three different matrices (Steel 1, Steel 2, Steel 3) for simulated welding. The optimal pre-weld heat treatment is 720 °C for 15 min followed by water quench. Microstructure characterization showed that there is an evident microstructure comprising bainite (B) in Steel 1 and Steel 2 after pre-weld heat treatment, while the addition of martensite (M) with the pre-weld heat treatment temperature exceeds Ac1 by almost 60 °C (Steel 3). These differences in microstructures obtained from pre-weld heat treatment influence the refinement of high-temperature austenite during subsequent simulated welding reheating processes, resulting in distinct microstructural characteristics in the CGHAZ. After the optimal pre-weld heat treatment, Steel 2 subjected to single-pass welding thermal simulation demonstrates a refined microstructure characterized by a high density of high-angle grain boundaries (HAGBs) within the CGHAZ, particularly evident in block boundaries. These boundaries effectively prevent the propagation of brittle cracks, thereby enhancing the impact toughness.

Effect of V and Mn addition on the HAZ softening and tensile properties of friction stir welded martensitic steel

This study explores the suppression of heat-affected zone (HAZ) softening in friction stir welding (FSW) joints formed above the A3 temperature of martensitic steels by leveraging short-time secondary hardening induced by vanadium (V) addition. The HAZ microstructure was examined using scanning electron microscopy (SEM), transmission electron microscopy (TEM), and atom probe tomography (APT). Mechanical properties were evaluated through Vickers hardness (HV) measurements and tensile tests. Analysis of hardness distribution indicates effective HAZ softening suppression with V addition, attributed to the precipitation of fine and high-density V carbides within the HAZ. The inhibition of HAZ softening was correlated not only with V content but also with the A1 temperature of the steels, regulated by the manganese (Mn) content. However, at 1 mass% V content, intergranular brittle fracture occurred within the HAZ due to continuously distributed fine carbides and Mn segregation along the prior austenite boundary.

Postweld Heat Treatment of 15Cr-6Ni-2Mo-1Cu Supermartensitic Stainless Steel Welds

Supermartensitic stainless steels with 15Cr- 6Ni-2Mo-1Cu with 135 ksi minimum yield strength (15Cr-135 SMSS) offer high strength and good toughness through a complex hierarchical microstructure of nanoscale precipitates, tempered martensite, and reverted austenite. Upon welding and postweld heat treatment, substantial changes to heat-affected zone microstructure and hardness may occur. Here, we reveal spatially heterogeneous microstructure and microhardness in the HAZ of 15Cr-135 SMSS; correlate these changes to measured phase transformation temperatures; and demonstrate that HAZ hardness changes depend strongly on postweld heat treatment temperatures. Furthermore, we demonstrate that PWHT may lead to undesired reductions in base metal yield strength and formulate a design guide for PWHT that quantifies the trade-offs in desired reductions of HAZ hardness with undesired changes to base metal yield strength. These findings have important practical implications for welding procedure design and qualification.

Effects of post-weld heat treatments in microstructure, mechanical properties, and corrosion resistance of simulated heat-affected zone of supermartensitic steel UNS S41426

Effects of post-weld heat treatments in microstructure, mechanical properties, and corrosion resistance of simulated heat-affected zone of supermartensitic steel UNS S41426

Development of a novel fabricating thin-walled TA2 titanium tube via high-frequency induction welding

Due to the problems of low welding efficiency, large heat-affected zone, and poor welding quality in the process of welding thin-walled titanium tubes by argon arc welding, there are few studies on the use of high-frequency induction welding (HFIW) of thin-walled titanium alloy tubes. The evolution law of weld microstructure and mechanical properties of the thin-walled titanium tube needs to be further studied because of rapid welding speed and the small heat-affected zone of HFIW. Therefore, a novel manufacturing method via high-frequency induction welding is proposed in this paper to solve the existing problems. With an industrial-grade titanium TA2 tube (wall's thickness is 0.5 ​mm) as the research object, a comparative study is conducted in this research to examine the morphology, microstructure, microhardness, and tensile characteristics of welded joints at different welding power. The findings demonstrated a significant efficacy of HFIW in resolving these challenges. The mechanical properties and microstructue of heat-affected zone (HAZ) were characterized. The lowest hardness is measured at 202 HV, while the base material was recorded as 184 HV, when the welding speed of HFIW is set at 50 ​m/min. Meanwhile, the heat-affected zone has the highest hardness at 224 HV, a tensile strength of 446.8 ​MPa and a post-fracture elongation of 16%. The results showed that HFIW can not only greatly improve the welding efficiency, significantly improve the microstructure of weld joint and HAZ, and improve the mechanical properties of thin-walled titanium pipe, but also provide a highly feasible welding method for welding ultra-thin-walled pipes.

Application of Machine Learning (ML)-based multi-classifications to identify corrosion fatigue cracking phenomena in Naval steel weldments

Corrosion fatigue (CF) crack detection in welded ship hull structures is quite crucial as well as challenging for ensuring their structural integrity. This is conventionally done by offline ship hull survey and inspection methods, which have large time and cost implications. Data-driven approaches of ship hull crack detection are promising in this regard. Corrosion fatigue crack growth rate (CFCGR) behaviour of shipbuilding steel was studied for its base metal (BM), fatigue-prone heat affected zones (HAZs) of Submerged Arc Welding (SAW), and shielded metal arc welding (SMAW) joints of Naval-grade steel. The results indicated the highest CFCGR for BM, intermediate for SAW, and smallest for SMAW welds. This was attributed to 44% lath martensite observed in the SMAW HAZ microstructure as compared to 33% in SAW HAZ. A novel ML-based method has been proposed for CF crack location identification by a multi-classification approach using CFCGR data for structural health monitoring (SHM) applications. Prediction of crack location (either BM, SMAW HAZ, or SAW HAZ) was investigated using K-nearest neighbour (KNN), linear support vector machine classifier (LSVC), Naïve Bayes (NB), decision tree (DT), random forest (RF), and artificial neural network (ANN) models. DT and RF models were found to perform very well even without scaling and hyper-parameter tuning operations and exhibited 98–99% classification accuracy. Scaling and tuning operations resulted in significant improvements in accuracy of KNN models from 43% to 84% (minmax scaling) and 98% (standard scaling). Significant improvement in the accuracy from 37% to 98% ANN model was achieved by standard scaling. The proposed method shall be useful in data-driven real-time crack location identification in ship hull structures.

Inclusions and microstructures in coarse-grained heat-affected zone of Al–Ti–Ca deoxidized shipbuilding steels with different Al contents after high-heat input welding

The inclusions, microstructure evolution and impact toughness of the coarse-grained heat-affected zone (CGHAZ) of Al–Ti–Ca deoxidized shipbuilding steel plates with different Al contents after high-heat input welding of 400 kJ cm−1 are investigated. The characteristics of inclusions and their influence on the refinement of microstructure and impact toughness in CGHAZ was elucidated. Increasing the Al content from 0.016 wt% to 0.022 wt% and 0.043 wt% results in an increase in the average size of prior austenite grain and the brittle phase fractions, while decreasing the content of intragranular acicular ferrites (IAFs). The results of the thermodynamic calculations, high-temperature laser scanning confocal microscopy and differential scanning calorimetry all show that increasing the Al content can diminish the austenitic stable region, elevate the transition temperature from austenite to ferrite and suppress the nucleation of IAF. In the present steels, the IAF formation is successfully induced by the specific inclusions, namely Al2O3–CaO–Ti2O3–MnS(-CaS), in which the calcium aluminate inclusions are embedded with Ti-oxides and CaS–MnS precipitates. The effective inclusions have the number density of 93 mm−2 in 16Al steel and 27 mm−2 in 22Al steel, but they are rarely found in 43Al steel. On average, an effective inclusion can induce 3.4 IAFs in 16Al steel and 2.8 IAFs in 22Al steel. Thus, as the Al content increases from 0.016 wt% to 0.22 wt% and 0.043 wt%, the impact toughness of CGHAZ at −40 °C decreases from 134 J to 78 J and 24 J with the welding heat input of 400 kJ cm−1.

Influence of HAZ microstructure on RCF under twin-disc test of a flash-butt welded rail

A new twin-disc test was performed using discs containing all microstructures of the heat-affected zone (HAZ) of flash-butt welded rails. It was observed that the lower hardness regions (spheroidized cementite in a ferritic matrix) at the HAZ boundary underwent a local deformation, generating valleys and reproducing a common defect type observed in rail welds: double squat-like defect. Longer crack lengths or crack clusters were observed in the HAZ boundary and central weld regions. The cross-section metallography showed that these cracks are directly related to the microstructure of spheroidized cementite at the HAZ edges or pro-eutectoid ferrite at the central region. The decrease in surface roughness before the cracks, the presence of oxide on the bottom crack surface, and superior spheroidized cementite microstructure in the upper crack region suggest that these larger/cluster cracks are predominated by extrusion of the softer material above the harder material (pearlitic/base metal).

Heat affected zone evolution in fine grained aluminum alloys during laser welding: Phase-field simulation and analytical investigation

One of the biggest challenges in the welding of strengthened alloys by grain refinement is the grain growth phenomenon in the heat-affected zone (HAZ), which would result in the degradation of mechanical properties. The goal of this study is to comprehend the HAZ evolution in the fine-grained aluminum alloy during laser welding as a low heat input process. Spot laser welding of fined grain 1050 aluminum alloy revealed that grain growth and HAZ formation occurred in samples with 4 µm grain size, but no grain growth occurred outside of the fusion line (FL) in larger grain samples. The microstructure of HAZ was simulated using the numerical phase-field technique. The numerical model's findings demonstrated that a critical grain size (Dcr) for the base metal can be established, above which grain growth would not occur outside FL. To predict grain size distribution outside FL, an analytical model was also used. According to both models, as grain size increases, the HAZ width decreases, and above a critical grain size, no HAZ will form outside of FL. In spot welding, Dcr was independent of power density but for continuous welding processes, Dcr has a direct relationship with heat input per unit length of weld. Moreover, HAZ grain growth mainly occurred in heating step for both types of processes.

Changes in microstructure and properties of weld heat-affected zone of high-strength low-alloy steel

Changes in microstructure and properties of weld heat-affected zone of high-strength low-alloy steel

Effect of Mo microalloying on impact toughness of X80 pipeline steel in SCGHAZ

The microstructure and impact toughness of subcritically reheated coarse-grained heat-affected zone (SCGHAZ) of X80 pipeline steels with different Mo content (0Mo and 0.11 wt%Mo) were investigated. Gleeble 3500 thermal simulation experiment was used to simulate the heat-affected zone (HAZ) of X80 pipeline circumferential weld, and the two samples were characterized by a series of material testing techniques such as SEM, TEM, EBSD and XRD. The research showed that: Appropriate addition of Mo element can improve the hardenability of the matrix, increase the content of bainitic ferrite (BF) in the microstructure, refine the BF lath, cause plastic deformation, and reduce local stress concentration. The increase of BF content greatly increases the proportion of high angle grain boundary (HAGB) in order to effectively inhibit crack propagation. On the other hand, Mo element influences precipitation with solid solution, reduces the early energy barrier for nucleation, delays the disappearance of dislocation lines at high temperature, forms high-density dislocation grid, so that it can increase the nucleation site for NbC precipitation, prevent the coarsing of NbC, increases the threshold of external stress required for the generation of micropores induced by precipitation, and hinder crack initiation. The impact toughness of SCGHAZ was significantly improved by adjusting the microstructure and second phase morphology of HAZ by using Mo element microalloying.

Effect of post-weld heat treatment on heat affected zone microstructure of additively manufactured Inconel 718

Laser powder bed fusion for metals is a method of producing end use components for industrial use. Powder bed fusion machines are relatively small, and are usually used to create only the critical part of the larger assembly. Therefore, L-PBF manufactured parts must be attached to each other for example by welding. The industrial world needs to be able to join the printed superalloy components to the traditionally manufactured components to reach better corrosion, wear and/or heat resistance in selected parts in an assembly. The problem is that there is limited amount of information about the suitable welding parameter values for these applications. This study examines how the standard heat treatment cycles affect to the quality of the weld, and if the post-heat treatment is reducing undesired phases in the heat affected zone. Test has shown that post heat treatment highlights cuboidal shaped niobium rich carbides throughout the material to the heat affected zone grain boundaries.

Study on Microelectrochemical Inhomogeneity of an SA508-309L/308L Overlay Welded Joint.

The corrosion behavior of the dissimilar metal welded joint (DMWJ) is highly dependent on its heterogeneous microstructures. However, directly measuring the electrochemical properties of microstructures in different heat-affected zones (HAZs) is a formidable challenge, because traditional bulk electrochemistry can only offer an average signal. Herein, the microelectrochemical properties of an SA508-309L/308L DMWJ were measured in 3.5 wt % NaCl solution using lithography and capillary techniques. Specifically, high-throughput microelectrochemical tests, including open circuit potential (OCP), electrochemical impedance spectroscopy (EIS), and potentiodynamic polarization (PDP), were conducted on 168 spots (Φ 12 μm). Results revealed five typical EIS responses and seven varieties of PDP curves (different magnitudes of the current density). The maps of thermodynamic and kinetic metrics, such as polarization resistance derived from EIS, corrosion potentials, and corrosion currents extracted from potentiodynamic polarization curves, demonstrated good consistency. The uniform corrosion tendency of the SA508 HAZ subregions during the immersion tests is basically consistent with its Ecorr_avg order of subcritical HAZ (C5, -371 mV) < intercritical HAZ (C4, -546 mV) < fine-grained HAZ2 (C3, -579 mV) < fine-grained HAZ1 (C2, -593 mV). The random presence of inclusions leads to highly heterogeneous microelectrochemical properties of the DMWJ, thereby causing localized corrosion to occur preferentially. Moreover, the macroscopic corrosion behavior is affected by the corrosion products, which display a protective effect that modifies the local electrochemical activity of the SA508 HAZ. The combination of microelectrochemical properties allows for a more comprehensive understanding of the macroscopic corrosion behavior of metals and the galvanic effect between the heterogeneous microstructures.

Gleeble Simulation of HAZ in S690QL Steel: Microstructural and Mechanical Properties

When investigating the heterogeneous properties of welded joints, mechanical testing of certain Heat Affected Zone (HAZ) regions, using standard approach test specimens, is very difficult or sometimes even impossible. Inability to precisely position and extract mechanical test specimens, even ones of the subsize dimensions, from the narrow HAZ regions is a limiting factor in the mechanical testing implementation. Detailed investigation of the HAZ is made possible by the use of thermo-mechanical simulations on the Gleeble welding simulator. In scope of this paper several characteristic HAZ microstructures of S690QL grade High Strength Steel (HSS) are being simulated. Multi-pass welding simulations are done on special 10x10 mm square section bar specimens in order to reproduce thermal gradients and characteristic microstructures at any location in a weld. Such simulated HAZ microstructures are of a sufficiently large volume, with homogeneous and repeatable properties, that standard specimen methods for mechanical testing can be readily implemented. Metallographic optical examinations, as well as hardness measurements were done initially. Mechanical properties are focused on determining stress-strain curves for each characteristic weld region. The paper investigates whether the mechanical properties of Gleeble simulated hard-soft combined HAZ regions are better in comparison to exclusively hard or soft HAZ regions. The obtained results can subsequently be used for the material model development.

Microstructural characterization of simulated and actual constituent regions of P91 steel weldment

In the present study simulated and the actual microstructures of the coarse grain, fine grain and intercritical heat-affected zones of P91 steel weldment are characterized using electron backscattered diffraction (EBSD) technique. Both the simulated and actual heat-affected zone (HAZ) microstructures showed profound substructural recovery after post-weld heat treatment/tempering. The subgrain size distributions between the simulated and the actual HAZs are comparable. The actual HAZ microstructures exhibited greater low angle grain boundaries and local strain distributions compared to the simulated HAZ microstructures due to the complex microstructural geometry of the actual weldment. The similarity in the variations of grain size, precipitate size and hardness of the simulated and actual HAZs validates the simulation of HAZ microstructures through furnace heat treatment.

Effects of heat input on microstructure evolution, mechanical and corrosion properties of TC4 alloy by keyhole TIG welding

In this study, Keyhole tungsten inert gas (TIG) process, a new variation of traditional TIG process, was performed to weld TC4 titanium alloy with a thickness of 6 mm. The effect of heat input on microstructure and their correlation with mechanical properties and corrosion behavior was studied. The results showed that the microstructure of fusion zone and heat-affected zone changed obviously due to the change of heat input. The microstructure in the joints was transformed from equiaxed primary α and α+β lamellae to complete primary β grains, and then α′ phases were precipitated in the primary β grain. With the increase of heat input, the content and length of the acicular α′ phase grains were increased, resulting in a decrease in the number of high angel grain boundaries (HAGBs). Due to the phase strengthening effect of α′ phases, the microhardness of the joints increased, and the tensile strength increased, reaching a maximum value of 1030.1 MPa when the heat input was 1118 J/mm. The impact toughness of the joints increased firstly and then decreased. The corrosion behavior of the joints was worse than that of the base metal (BM). The best corrosion resistance was obtained when the heat input was 1046 J/mm. It concluded that the excellent comprehensive properties can be obtained when the heat input was in the range of 1046–1118 J/mm.

Characterization of pulsed-tungsten inert gas (PTIG) welding on AA5754-H111 alloy: mechanical properties and microstructural analysis

Abstract Aluminium and its alloys were widely used in engineering because they are lightweight, strong, and resistant to corrosion. However, using standard arc welding techniques can be difficult when dealing with such materials. Pulsed-Tungsten Inert Gas (PTIG) welding is being researched as a potential solution to this problem. This study is the first to investigate the use of the straightforward and intuitive PTIG technique on the ubiquitous AA5754 wrought aluminium alloy. Welded samples were supplied for examination of mechanical parameters such as surface hardness and strength under impact and tensile loading. The results of a statistical analysis of the mechanical characterization of a PTIG-welded permanent joint fabricated from AA5754 aluminium alloy were presented and discussed. The heat-affected zone (HAZ) on the AA5754 retracting side of the weld had a hardness of 50–70 Hv0.5, while the HAZ on the AA5756 side had a hardness of 90–100 Hv0.5, as measured by testing on the perfect weld specimen. Samples taken from different parts of the weldment all showed that the HAZ is the softest and weakest. The shattered surface of the welded sample consisted of flat facets and quasi-cleavage patterns, as revealed by scanning electron microscopy. Analysis of the HAZ microstructure revealed widespread dissolution of Mg2Si precipitates in the AA5754-H111.

Nd: YAG laser beam welding of UNS N07718 superalloy and UNS S32304 duplex stainless steel: Phase transformations and mechanical properties of dissimilar joints

This article implies the phase transformations and mechanical behavior of dissimilar laser welded UNS N07718 superalloy/UNS S32304 duplex stainless steel. Laser power, welding speed, and focal point were the variables of the laser beam welding (LBW) approach. Optical microscopy and electron backscattered diffraction (EBSD) analysis were utilized. They demonstrated that the weld metal (WM) mainly had an austenitic microstructure with a face-centered cubic structure in the form of columnar and equiaxed dendrites. Also, the occurrence of directional solidification in WM was verified by EBSD. The heat-affected zone (HAZ) microstructure of Inconel 718 superalloy included austenite grains with normal grain growth, annealing twins, and precipitates. There was a ferritic-austenitic microstructure in the HAZ of 2304 duplex stainless. In this area, the volume fraction of the ferrite phase was excessively higher than that of the austenite phase and the austenite was characterized as Widmanstätten plates and grain boundary austenite. Furthermore, abnormal ferrite grain growth was identified in this. Welding defects e.g., molten spatter, solidification crack, and lack of penetration were observed, as well. Based on the uniaxial tensile test, it was realized that the highest failure load (9.7 ± 0.4 kN) was achieved in the laser power of 1900 W, welding speed of 3 mm/s, and focal point of 0 mm. Therefore, these variables were known as the optimum variables of the LBW process. All laser weldments failed from the WM and fractography via scanning electron microscopy (SEM) showed a mixture of dimple and cleavage features in the fracture surfaces of the laser welds.

Heat-Affected Zone Characterization of X2CrNiN22-2 Lean Duplex Stainless Steel by Metallographic and Electrochemical Techniques

This research aimed to investigate the heat-affected zone of lean duplex stainless steel grade X2CrNiN22-2. Different heat-affected zone microstructures and grain morphologies were developed by Gleeble simulations. The governing microstructures were evaluated by metallographic techniques and electrochemical corrosion measurements. It was found that the 1200-800 °C cooling time significantly affects the microstructure, austenite content, and corrosion properties. The average austenite content in the case of 1 s cooling time is 30.7 ± 1%, which increased with the longer cooling times up to 38.6 ± 0.9%. The rapid cooling times resulted in a more ferritic microstructure, which promoted nitride precipitation in the ferrite grains. The nitride precipitations acted as nucleation sites for pitting initiation in 3.5 wt.% NaCl solution. The lowest pitting potential was measured in the case of the most rapidly cooled sample: 573 ± 31 mV, while the balanced, annealed microstructure had much better pitting corrosion resistance, showing a pitting potential of 1308 ± 62 mV vs. the Ag/AgCl (KCl sat.) reference electrode. The results of this research can be used in designing welding parameters for the welding of the X2CrNiN22-2 lean duplex stainless steel.Graphical

Influence of Butter Layer Thickness on Microstructure and Mechanical Properties of Underwater Wet 16Mn/304L Dissimilar Welded Joint.

Butter layers of different thicknesses were successfully deposited on ferritic steel by using the tungsten arc welding (TIG) process. The effects of butter layer thickness on the microstructural characteristics, elemental distribution, and mechanical properties of underwater wet 16Mn/304L dissimilar welded joints were investigated. The results showed that the butter layer significantly changed the microstructure and elemental distribution of 16Mn/304L joints. As the thickness of butter increased, the heat-affected zone (HAZ) at the ferritic steel side changed from the original 16Mn steel to the ERNiCrMo-3 butter layer. The martensite content in HAZ also exhibited a downward trend. When the thickness of the butter layer exceeded 6 mm, the microstructure of HAZ at the ferritic steel side was composed of ferrite and pearlite, instead of quenched martensite. The microhardness of underwater dissimilar steel welded joints significantly reduced due to the absence of martensite. The addition of the butter layer increased the ultimate tensile strength from 515 MPa to 565 MPa. The results of this work could provide a robust basis for future applications of dissimilar steel structures.