DOI: 10.2514/1.T3609 Anexperimentalinvestigationexploringtheuseofawire-screen-mesh/hollow-glass-microspherecombinationasa thermal insulation media was conducted with three primary variables. These included the number of wire-mesh layers, the size of microsphere filler material, and temperature range. The test facility used included vertically stacked samples that were thermally and mechanically controlled (e.g., via gas bellows that controlled its vertical movement). From the temperature profile in the upper and lower samples, the value of the effective thermal conductivity was determined with use of the Fourier law of heat conduction. The number of screen mesh layers investigated were two, four, six, and eight, with each separated by a metallic liner. The filler materials included air andS15,S35,andS60HShollow-glassmicrospherestestedattemperaturesof27,57,93,and127Cwithaninterface pressure of 138 kPa (20 psi). The experimental results indicated that the number of layers was the primary factor in determining the effective thermalconductivity value andthusthe structure’sinsulation effectiveness. Increasing the number of wire-mesh layers resulted in acorresponding increase in effective thermal conductivity, whereas changes in temperature had negligible effect. The effective thermal conductivity values for the proposed structure ranged from 0.22 to 0:65 W=m-K, the lowest was for the two-layer case with air as filler material. Wire-screen-mesh insulation with air in the interstices leads to improved insulation, but the use of hollow-glass microspheres does not improve the insulation capabilities.