Feed Flow Rate Research Articles

Evaluation of Selected Operating Process Variables for a Bioflocculant Supported Column Flotation System

The poultry industry generates significant volumes of slaughterhouse wastewater, laden with numerous pollutants, thus requiring pretreatment prior to discharge. However, new technologies must be used to re-engineer the existing wastewater treatment equipment and incorporate new designs to improve the treatment processes or system performance. In this study, three variables, i.e., diffuser design, bioflocculant form, and flow rate, were evaluated to determine their effect on the performance of a bioflocculant-supported column flotation (BioCF) system. It was found that bioflocculants influenced diffuser performance with limited impact when the feed flow rate was varied, i.e., 3D-printed air diffusers and cell-free flocculants imparted high BioCF performance when compared to moulded diffusers and cell-bound flocculants. Notably, the combination of 3D-printed air diffusers and cell-free flocculants resulted in relatively high pollutant removal (81.23% COD, 94.44% TSS, 97.77% protein, and 90.38% turbidity reduction). The study lays a foundation for exploring 3D-printed air diffusers, a relatively new technology in conjunction with microbial flocculants usage that are regarded as eco-friendly for application in industry to enhance the performance of column flotation systems.

Flux decline in crossflow ultrafiltration-based diafiltration process for lignin recovery from a deep eutectic solvent comprised of lactic acid and choline chloride

This study investigates a continuous ultrafiltration (UF)-based diafiltration (DF) method to separate and purify lignin from a deep eutectic solvent (DES) containing lactic acid and choline chloride after biomass delignification. A crossflow setup with a polyether sulfone UF membrane with a molecular weight cut off of 5000 Da was used to evaluate flux decline and fouling in this process. Under different pressure, feed flowrate, lignin, and DES concentrations, lignin rejection is around 0.90. Higher lignin and DES concentrations increase filtration resistance, and thus decrease flux at constant pressure. On the basis of a previously setup model based on dead-end filtration, a modeling approach was further developed to predict the system size required to implement UF-DF on a large scale. The results shows that at a constant pressure, the membrane system's area increases as the cake layer thickness over the membrane's surface increases.

Gasification of Egusi Melon (Citrullus lanatus) Shell over a Novel Ni/dolomite/MgO/[formula omitted]Al2O3 Catalyst for the Production of H2-rich gas

Hydrogen-rich gas was produced from Citrullus-lanatus in a fixed-bed reactor using a novel Ni/dolomite/MgO/γ−Al2O3 with air-steam mixture as the gasifying agent. The feed and steam-air flow rates were 3 and 0.8 kg/h with fixed steam-air volume-concentration of 40% v/v. The results displayed a high cracking activity of the hydrocarbons/tar in the biomass by the catalyst with a resultant upgrade in the gas quality/H2 yield. The highest H2 yield was 66.1 g/kg biomass, a minimal tar concentration of 2 g/Nm3 with steam-to-biomass ratio of 2 at 1100 °C. The highest H2 yield (57 vol%) was achieved at 0.28 equivalence ratio.

NFeS Embedded into Cryogels for High-Efficiency Removal of Cr(VI): From Mechanism to for Treatment of Industrial Wastewater.

Most studies have focused on complex strategies for materials preparation instead of industrial wastewater treatment due to emergency treatment requirements for metal pollution. This study evaluated sodium polyacrylate (PSA) as a carbon skeleton and FeS as a functional material to synthesize PSA-nFeS material. The characteristics and interactions of PSA-nFeS composites treated with hexavalent chromium were analyzed by means of various techniques, such as scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDS), X-ray photoelectron spectroscopy (XPS), Fourier transform infrared spectrometry (FTIR), and atomic absorption spectroscopy (AAS). Adsorption-coupled reduction was observed to be the predominant mechanism of Cr(VI) removal. The feasibility of PSA-nFeS composites in reducing toxicity and removing of Cr(VI) from real effluents was investigated through column studies and material properties evaluation. The continuous column studies were conducted using tannery effluents to optimize feed flow rates, initial feed Cr(VI) concentration, and column bed height. The results revealed that PSA-nFeS composites are ideal for filling materials in portable filtration devices due to their lightweight and compact size.

Table-top numbering-up 3D-printed miniaturized hydrocyclone for high-efficiency and high-throughput separation of oil-in-water emulsions

Oily wastewater from home and industrial effluents, as well as marine oil spills, poses significant environmental problems, such as water and soil contamination and ecosystem devastation. We here developed a parallelized miniaturized hydrocyclone (mHC) system consisting of multiple mHCs and a flow distributor for high-efficiency and high-throughput separation of oil-in-water emulsions. From a manufacturing perspective, our system can be easily and rapidly created using 3D printing technology. It was also specifically designed to provide simple and durable connections between tubes and components, eliminating the need for a time-consuming bonding process. Direct visualization of primary and secondary vortex flows generated within the mHC device was achieved, allowing the variation of the vortex flows as a function of the feed flow rates to be analyzed. Furthermore, we demonstrated that a single mHC was capable of separating six types of oil-in-water emulsions with different oil phases and a separation efficiency greater than 90 %, with olive oil-based emulsions achieving a remarkable separation efficiency of 98.3 % at the optimal feed rate of 200 mL/min. By numbering-up a single mHC and incorporating a 3D-printed flow distributor to ensure a uniform flow distribution into each individual mHC, we can construct a parallelized mHC system. The separation system can process an estimated 3,168 L (837 US gallons) of mineral oil-based emulsion per day with a separation efficiency of approximately 97 %. The results of this study can be further enhanced by modifying the flow distributor, increasing the number of single mHCs, and introducing high-performance pumps.

Operational strategy of reconfigurable membrane process for bio-based amino acid production

Reconfigurable manufacturing systems can rapidly and economically transform production facilities, allowing for the simultaneous realization of diverse customized product manufacturing and high productivity. In this study, the concept of reconfigurable manufacturing systems was introduced to the counter-current diafiltration membrane process for bio-based amino acid production. A superstructure model adaptable to any counter-current diafiltration cascade configuration was developed. This superstructure model optimizes the objective cost function, minimizing fluctuation costs associated with yield and utility. Case studies such as the production of L-lysine, L-arginine, and L-tryptophan were considered. Sensitivity analysis indicated that when membrane capacity becomes limited due to increased overall feed flow rates and decreased permeate flux, the role of the counter-current diafiltration step grows in importance. Circumstances caused by diverse product manufacturing, natural disturbance in bioprocesses, and shifts in productivity and cost priorities based on market dynamics indicate the promising economic potential of reconfigurable membrane systems. Since scalability, diagnosability, customization, modularity, and integrability are high, the reconfigurable membrane system has proven its capability to flexibly adapt to continuously changing conditions. All superstructure modeling and simulations in this study were executed using in-house graphical user interface software.

Theoretical and experimental investigation of cylindrical air gap membrane distillation system and effect of the membrane support net on its performance.

In present study a cylindrical module is studied based on air gap membrane distillation configuration and studied for desalination purpose. A complete theoretical model was developed with consideration of design and operating parameters that enabled a Cylindrical Air Gap Membrane Distillation (CAGMD) module specific performance analysis. Theoretical model was verified with the literature as well as with the experimental results carried out on a lab scale CAGMD module. The effect of support nets which supports the membrane on the air gap side is also discussed on the performance. Support nets made up of four different thermal conductivities material- copper, aluminum, brass and polypropylene (PP) are considered for this study. The effect of feed temperature and flow rate, air gap width, cold flow rate, effect of thermal conductivities of support nets and height of the module was studied on the performance of CAGMD module. Permeate flux, Specific Thermal Energy Consumption (STEC) and the Gained output ratio (GOR) was selected as the performance indicators and the results for all the resulted parameters obtained from experimental and theoretical model falls in good agreement with only 6% deviation, that suggests that the proposed model is best suitable for predicting the behavior of any cylindrical AGMD module with great effectiveness. It is suggested that for better performance of the system feed flow rate, temperature and cold flow rate should be maintained at higher level. Maximum permeate flux achieved from the CAGMD module is 9.22kg/m2h.

An Adaptive Fuzzy Logic Control Method for Froth Velocity in the Flotation Process

In the flotation process, too high or too low froth velocity can lead to a reduction in the recovery of useful minerals. However, it is difficult to achieve stable control of froth velocity due to complex process characteristics and fluctuating working conditions. Uncertain feed conditions (feed flow rate, feed grade, and feed concentration) can cause large changes in the desired froth velocity and other uncertain conditions, which affect the accurate evaluation of the velocity state for feedback control. In this paper, an adaptive fuzzy logic control method for froth velocity (AFLC-FV) in the flotation process is proposed. In the method, an adaptive fuzzy quantization function with a dead zone is designed and used instead of the constant fuzzy quantization factor in the fuzzification procedure. Thus, the dynamic real domain of the velocity error can be mapped to a fixed standard fuzzy domain. Meanwhile, the width of the dead zone is adaptively adjusted according to froth mobility to improve steady-state performance. In addition, the velocity trend is extracted and used as an input variable to the controller together with the velocity error. The application results show that, compared with manual control, the AFLC-FV significantly enhances the control accuracy and stability under different ranges of velocity set-points, and effectively improves the mineral recovery by 0.18%.

Experimental Investigation of Vacuum Membrane Distillation (VMD) Performance Based on Operational Parameters for Clean Water Production

Freshwater shortage is an ongoing concern across the world, due to increasing populations and climate change. Vacuum membrane distillation (VMD) is a viable approach for producing fresh water to meet the needs of society. In the current study, an experimental investigation has been conducted on a laboratory-scale single-stage module to explore the impact of operational parameters such as feed temperature, vacuum pressure, and feed salinity on the performance of vacuum membrane distillation (VMD), including permeate flux, gained output ratio, and specific thermal energy consumption. Results show that increasing the feed temperature and feed flow rate, and reducing the salinity, increases the permeate flux. As the feed temperature rises from 60 to 70°C, the permeate flux increases from 1.90 to 4.36 kg/m²h at a permeate pressure of 12 kPa and salinity of 30 g/L. Similarly, increasing the vacuum pressure from 12 to 18 kPa reduces the permeate flux. As a result, the specific thermal energy consumption increases from 728 to 803 kWh/m³. From experimental findings, it was observed that the rejected brine from VMD retains sufficient energy that could be utilized in another desalination system.

Different Configuration Comparisons for Seawater Desalination Systems: Performance Analyses

This study simulates an RO system for seawater desalination to overcome Iran’s water crisis due to drought and increasing demand. Based on previous studies, a scientific gap has been observed in that the effect of single‐stage or two‐stage systems on performance and effective parameters has not been investigated. In addition, examining the types of arrangements for using pressure vessels will make the present study more comprehensive. SW30XHR‐440i modules are used for desalination and three different feed flow rates (800, 1200, and 1600 m3/day) and three different recovery percentages (40, 55, and 70%) are used for sensitivity analysis. The methodology of the solution includes the examination of different configurations and the solution of the transport equations in the Water Application Value Engine (WAVE) 1.82 software. The configurations without technical errors are selected as the answer for further investigation and comparison with each other. The results show that the lowest specific energy of the pump with the amount of 4.18 kWh/m3 corresponds to the 55% recovery of the two‐stage system (800 m3/day permeate flow rate). As a general result, it can be stated that as the flow rate increases, the advantage of using a 6‐element pressure vessel over an 8‐element pressure vessel becomes more significant. Also, using the two‐stage system instead of single‐stage system is less feasible for higher permeate flows.

Green synthesis approach using deep eutectic solvents to enhance the surface functional groups on porous carbon for CO2 capture

This study explores the potential of green solvents using amino acids-based deep eutectic solvents to alter surface functionality of activated carbon thus enhancing the carbon dioxide (CO2) adsorption capacity. Green solvent is prepared by mixing an amino acid (L-Arginine) with ethylene glycol to form amino acid-based deep eutectic solvents. Amino acid-based deep eutectic solvents were used to modify the surface functionalities of activated carbon derived from palm shell waste. The change in surface functional groups and surface morphology of the modified activated carbon samples were characterized by Fourier-transform infrared spectroscopy and Scanning electron microscopy-energy dispersive X-ray analysis. Then, CO2 removal performance was performed using a packed-bed CO2 adsorption reactor to evaluate CO2 breakthrough time and adsorption capacity. CO2 adsorption experiments were measured at a certain temperature (25–45°C), at a fixed feed flow rate and CO2 concentration of 200 mL/min and 15%. It was observed that modified activated carbon showed the highest breakthrough time (15.2 min) compared to raw palm shell (5.2 min) at an adsorption temperature of 25°C. CO2 breakthrough times significantly decreased with increasing adsorption temperature because of physical adsorption.

Hybrid vacuum membrane distillation-multi effect distillation (VMD-MED) system for reducing specific energy consumption in desalination

This study focuses on the integration of vacuum membrane distillation into the multi-effect distillation (VMD-MED) system, incorporating heat recovery mechanisms to augment fresh water productivity and minimize the specific thermal energy consumption of the desalination process when compared to stand-alone vacuum membrane desalination systems. The hybrid system was devised by integrating the experimental output of VMD (permeate flux and hot brine) as heat source to MED. Two hybrid systems were investigated in this study: VMD/MED, wherein the heated brine from VMD served as a heat source for MED, facilitating the recovery of sensible heat from VMD; and VMD-HR/MED, where the latent heat of VMD vapor during condensation was utilized to pre-heat the feed water for MED. Based on the performance parameters, it was concluded that the VMD-HR/MED hybrid system outperformed both the stand-alone VMD and VMD/MED hybrid system in terms of efficiency. The latent heat recovery from the condenser of VMD in VMD-HR/MED hybrid system reduces the specific thermal energy consumption (STEC) to 38.42 kWh/m3, however, it enhanced the gain-output-ratio (GOR) and productivity of the system. Additionally, a rise in GOR and a simultaneous decrease in STEC were observed with increasing feed flow rates and vacuum pressure.

Y-tube assisted coprecipitation synthesis of iron-based Prussian blue analogues cathode materials for sodium-ion batteries.

Prussian blue analogues possess numerous advantages as cathode materials for sodium-ion batteries, including high energy density, low cost, sustainability, and straightforward synthesis processes, making them highly promising for practical applications. However, during the synthesis, crystal defects such as vacancies and the incorporation of crystal water can lead to issues such as diminished capacity and suboptimal cycling stability. In the current study, a Y-tube assisted coprecipitation method was used to synthesize iron-based Prussian blue analogues, and the optimized feed flow rate during synthesis contributed to the successful preparation of the material with a formula of Na1.56Fe[Fe(CN)6]0.90□0.10·2.42H2O, representing a low-defect cathode material. This approach cleverly utilizes the Y-tube component to enhance the micro-mixing of materials in the co-precipitation reaction, featuring simplicity, low cost, user-friendly, and the ability to be used in continuous production. Electrochemical performance tests show that the sample retains 69.8% of its capacity after 200 cycles at a current density of 0.5C (1C = 140 mA g-1) and delivers a capacity of 71.9 mA h g-1 at a high rate of 10C. The findings of this research provide important insights for the development of high-performance Prussian blue analogues cathode materials for sodium-ion batteries.

Performance assessment of a modified air-gap and water-gap membrane distillation systems

This work experimentally evaluates and compares the performance of four membrane distillation (MD) units with and without an internal gap rotating impeller blade. The novelty of the current study lies in the installed impeller within the condensation cavity and the impeller design parameters. The investigated MD units include a novel modified water-gap MD (M-WGMD) system featuring an internal impeller blade; a novel modified air-gap MD (M-AGMD) system with an internally rotating impeller blade; a regular water-gap MD (WGMD) process; and a conventional air-gap MD (AGMD) system. The evaluated system performance index includes gained output ratio (GOR) and vapor flux. The performance of the four MD systems is assessed and compared against each other under the same test conditions for various system design and operating variables, including impeller blade material, impeller blade angle, saline feed temperature, coolant temperature, and saline feed flowrate. Findings indicate that M-WGMD and WGMD systems (modified and conventional) produce higher flux than M-AGMD and AGMD units. Meanwhile, air-gap MD units (AGMD and M-AGMD) exhibits better energy efficient (higher GOR) than WGMD and M-WGMD systems. Furthermore, modified MD systems recorded superior performance compared to conventional MD systems and the blade angle effect is more influential than the blade material. At 80 °C feed temperature and 3200 mg/L feed salinity, the M-WGMD reaches a maximum flux of 128.39 kg/m2h and a GOR of 0.7702. On the other hand, the WGMD attained a flux of 67.32 kg/m2h and a GOR of 0.6199. The M-AGMD recorded a flux of 30.20 kg/m2h and a GOR of 0.8696. For the AGMD system, the GOR and the flux values are 0.7357 and 15.58 kg/m2h, respectively.

Development of new effective activated carbon supported alkaline adsorbent used for removal phenolic compounds

Phenolic (phenol) compounds are the major contaminates in wastewater, which can have a considerable negative influence on the environment and health of human. Adsorption is an efficient process that is widely applied in order to eliminate phenol in wastewater. In recent, Adsorption process has acquired a lot of attentiveness owing to its relative moderate operating conditions. However, adsorption process needs considerable ameliorations in terms of adsorbent modification, process type, productivity, and conversion rate. This work studies the development of a fast and effective adsorption process in a fixed bed adsorption column (FBAC) in order to reach safe and continuous elimination of phenolic compounds. Several adsorption parameters (reaction temperature, adsorbent bed height, feed flow rate and kind of adsorbent) were studied to achieve the highest removal of phenolic compounds. The adsorption process was conducted in the presence of two type of adsorbents (activated carbon (AC), and KOH/AC), 73% and 94% of phenol elimination were attained, respectively, at 10 cm bed height, 1 ml/s feed flow rate, and 75 °C reaction temperature. The adsorbents activity was investigated after six consecutive adsorption cycles at the best process conditions, and the adsorbents show high stability in terms of phenolic compounds adsorption. After that, the spent adsorbents were regenerated by utilizing various solvents (methanol, ethanol and iso-octane), and the results show that iso- octane achieved highest regeneration efficiency. The adsorption process was implemented in the adsorption column that the performance is possibly to be adjusted at an industrial scale since it can be scaled up predictably.

Treatment of Antihypertensive and Cardiovascular Drugs in Supercritical Water: An Experimental and Modeled Approach

Pharmaceutical pollutants are considered emerging contaminants, representing a significant concern to the ecosystem. Thus, this study reports on the degradation of antihypertensive and cardiovascular drugs (atenolol, captopril, propranolol hydrochloride, diosmin, hesperidin, losartan potassium, hydrochlorothiazide, and trimetazidine) present in simulated wastewater through applying the technology of oxidation using supercritical water (SCW). The operational parameters of the treatment process, particularly the feed flow rate, temperature, and concentration of H2O2, were assessed. A central composite design of experiments associated with differential evolution was employed in the optimization. Both liquid and gaseous phase products were submitted to physical–chemical characterization. As a result, the optimized conditions for the treatment were discovered to be a feed flow rate of 13.3 mL/min, a temperature of 600 °C, and a H2O2 oxidation coefficient of 0.65, corresponding to the oxygen stoichiometric coefficient in the carbon oxidation chemical reaction. Under optimal conditions, the total organic carbon (TOC) decreased from 332 to 25 mg/L (92.1%), and the pharmaceutical molecules underwent near-complete degradation. The physical–chemical parameters also met with the main environmental regulations for wastewater disposal. The compounds determined in the gaseous phase were CO2 (97.9%), H2 (1.3%), CH4 (0.3%), and CO (0.5%.). Additionally, a modeling thermodynamic equilibrium of the system was performed, based on the experimental data. The results revealed that SCW technology has a great potential to oxidize/degrade organic matter and can be applied to treat pharmaceutical pollutants.

Influence of Spray Drying Inlet Temperature on the Physical Properties and Antioxidant Activity of Black Garlic Extract Powder

Black garlic is a fermented product from garlic (Allium sativum L.) that is processed by heating fresh garlic at a certain temperature and humidity for several days. Black garlic has higher antioxidant activity and is rich in organosulfur compounds. Therefore, black garlic has an unpleasant taste and odor. Spray drying of black garlic extract is important for wider application, preservation and prolongation of its shelf-life. Black garlic powders were produced using SD-18A mini spray dryer. The purpose of this research was to evaluate the effect of inlet temperatures on the physical properties and antioxidant activity of aqueous black garlic powder. The inlet temperatures ranged from 165 to 225 °C, whereas other conditions were kept constant such as maltodextrin concentration (8 %) and feed flow rate (4.5 mL/min). The black garlic powders were examined for powder yield, moisture content, hygroscopicity, bulk density, wettability, antioxidant activity and total phenolic and flavonoid content. The optimal conditions for the drying process were achieved with an inlet temperature of 225 °C. An increase in the inlet temperature of the spray dryer has increased the powder yield, hygroscopicity, antioxidant activity and total phenolic and flavonoid content of the black garlic powder, but reduced the water content, bulk density and wettability of the spray-dried product. HIGHLIGHTS The best properties of black garlic powder were obtained at an inlet temperature of 225 °C The bioactive compounds of black garlic were stable at high temperatures The higher inlet temperatures increased antioxidant activity in black garlic powders GRAPHICAL ABSTRACT

Experimental studies of a continuous catalytic distillation column from startup to steady state for the production of methyl acetate

Abstract Esterification of acetic acid with methanol to produce methyl acetate and water has been studied in a continuous packed bed catalytic reactive distillation. The key challenge is the startup method of the experiments fora continuous reactive distillation as well as reactive zone height selection. In the present study, the effect of various operating conditions on the methyl acetate composition (mole fraction) is studied. Indion 180 ion-exchange resin solid catalyst is used in the reactive zone. The catalyst is immobilized by using a novel equivalent Katapak-S in the reactive section. Experiments were performed under different operating conditions to find the high purity methyl acetate product in the distillation. The experiments were performed for various conditions like total feed flow rate, reboiler temperature, reflux ratio, methanol to acetic acid mole ratio and catalyst loading with the time. The experiments were carried out till the system reaches to the steady state under different conditions. The maximum methyl acetate concentration is obtained at 80 °C reboiler temperature, 2.01 reflux ratio, 16.3 g/min flow rate, 60 g catalyst loading and 1 mol ratio of methanol to acetic acid. The highest purity of methyl acetate obtained under optimal condition is 95 % by mole.

Desalination Fuel Cell Stacks: Scaling up the Co-Production of Electricity and Clean Water

The world faces a rising demand for potable water and electricity, while a lack of clean water and use of polluting electricity sources are major hazards1. Nowadays reverse osmosis (RO) is widely used for sea and brackish water desalination2, where RO consumes ~3-4 kWh/m3 for seawater desalination3. A new class of water treatment technologies is emerging that is distinguished from the classical methods by utilizing chemical energy to power both water treatment and electricity generation simultaneously from a single electrochemical cell. When using the hydrogen/oxygen redox couple, such a cell is termed a desalination fuel cell (DFC) which was introduced by our group in 20204.A DFC utilizes a fuel cell anode and cathode to catalyze the chemical-to-electrical energy conversion, as well as a cation and anion exchange membrane to desalinate the feedwater flowing through the cell. A device with a single feed channel (figure a) was able to produce up to 10 kWh/m3 while desalinating water with sea-water level salinity4. In order to for this nascent technology to become practical, scale-up strategies need to be proposed and demonstrated.In this work we show results from the first scaled DFC, where we utilize scaling rules associated with electrodialysis by increasing the number of membrane pairs to allow either two or three feed channels (Figure b). We find the three feed channel device was associated with high voltage loss in the ohmic region and lower limiting current (figure c), but the salt concentration behaved linearly as a function of the current density as expected (figure d). The main voltage losses are clearly emanated from the cathode and the anode sides as the membranes potential loss was proven to be insignificant5. We showed that implementing higher acid concentration in the catholyte and higher base concentration in the anolyte channels can significantly improve performance of the stack. Figure (e) shows results using three different anolyte and catholyte solutions, with highest open circuit voltage (OCV) and improved polarization performance for 0.5M HClO4 and 0.5M NaOH in the catholyte and the anolyte, respectively. We also investigated the feed flow rate impact on DFC polarization performance and salt removal. Overall, we show successful implementation of a scaled-up DFC.

The Optimization of Operating Conditions in the Cross-Flow Microfiltration of Grape Marc Extract by Response Surface Methodology.

The recovery of valuable compounds like phenolic compounds and sugars from grape marc extracts implies different steps, including clarification. In this study, a response surface methodology (RSM) was used as a statistical tool to study the effects of operating conditions such as transmembrane pressure (TMP), temperature and feed flow rate on the performance of a microfiltration (MF) monotubular ceramic membrane with a pore size of 0.14 μm in the clarification of grape marc extract from the Carménère variety, as well to optimize the process conditions by implementing the Box-Behnken statistical design. The desirability function approach was applied to analyze the regression model equations in order to maximize the permeate flux and concentration of malvidin-3-O-glucoside, glucose and fructose in the clarified extract. The optimal operating conditions were found to be 1 bar, 29.01 °C and 5.64 L/min. Under these conditions, the permeate flux and concentration of malvidin-3-O-glucoside, glucose and fructose resulted in 65.78 L/m2h, 43.73 mg/L, 305.89 mg/L, and 274.85 mg/L, respectively.