Fiber-reinforced Composites Research Articles

Effect of Fiber Characteristics on the Structure and Properties of Quartz Fiber Felt Reinforced Silica-Polybenzoxazine Aerogel Composites.

Fiber-reinforced aerogel composites are widely used for thermal protection. The properties of the fibers play a critical role in determining the structure and properties of the final aerogel composite. However, the effects of the fiber's characteristics on the structure and properties of the aerogel composite have rarely been studied. Herein, we prepared quartz fiber felt-reinforced silica-polybenzoxazine aerogel composite (QF/PBSAs) with different fiber diameters using a simple copolymerization process with the ambient pressure drying method. The reasons for the effects of fiber diameter on the structure and properties of the aerogel composites were investigated. The results showed that the pore structure of the aerogel composites was affected by the fiber diameter, which led to significant changes in the mechanical behavior and thermal insulation performance. At room temperature, pore structure and density were found to be the main factors influencing the thermal conductivity of the composites. At elevated temperatures, the radiative thermal conductivity (λr) plays a dominant role, and reducing the fiber diameter suppressed λr, thus decreasing the thermal conductivity. When the QF/PBSAs were exposed to a 1200 °C butane flame, the PBS aerogel was pyrolyzed, and the pyrolysis gas carried away a large amount of heat and formed a thermal barrier in the interfacial layer, at which time λr and the pyrolysis of the PBS aerogel jointly determined the backside temperature of the composites. The results of this study can provide valuable guidance for the application of polybenzoxazine aerogel composites in the field of thermal protection.

Smart Carbon Fiber-Reinforced Polymer Composites for Damage Sensing and On-Line Structural Health Monitoring Applications.

High electrical conductivity, along with high piezoresistive sensitivity and stretchability, are crucial for designing and developing nanocomposite strain sensors for damage sensing and on-line structural health monitoring of smart carbon fiber-reinforced polymer (CFRP) composites. In this study, the influence of the geometric features and loadings of carbon-based nanomaterials, including reduced graphene oxide (rGO) or carbon nanofibers (CNFs), on the tunable strain-sensing capabilities of epoxy-based nanocomposites was investigated. This work revealed distinct strain-sensing behavior and sensitivities (gauge factor, GF) depending on both factors. The highest GF values were attained with 0.13 wt.% of rGO at various strains. The stability and reproducibility of the most promising self-sensing nanocomposites were also evaluated through ten stretching/relaxing cycles, and a distinct behavior was observed. While the deformation of the conductive network formed by rGO proved to be predominantly elastic and reversible, nanocomposite sensors containing 0.714 wt.% of CNFs showed that new conductive pathways were established between neighboring CNFs. Based on the best results, formulations were selected for the manufacturing of pre-impregnated materials and related smart CFRP composites. Digital image correlation was synchronized with electrical resistance variation to study the strain-sensing capabilities of modified CFRP composites (at 90° orientation). Promising results were achieved through the incorporation of CNFs since they are able to form new conductive pathways and penetrate between micrometer-sized fibers.

Evaluation of Fracture Resistance of Reattached Tooth Fragments Restored Using Fiber-reinforced Composites: A Systematic Review.

This systematic review examined the current literature to evaluate the fracture resistance of the tooth fragments reattached using fiber-reinforced composites (FRC). An electronic search was performed on Scopus, PubMed, and Web of Science databases according to specific inclusion and exclusion criteria to identify relevant articles to be included until January 2023. Articles with full text available in the English language for randomized control studies, observational studies, retrospective studies, and in vitro studies conducted on permanent human teeth were selected. The risk of bias was assessed in all studies using the OHAT tool. Out of 16 search results, seven in vitro studies with a total of 415 samples were included in the review. Three studies reported that reinforcement using rigid FRC posts improves fracture resistance of reattached anterior teeth, three studies reported that reinforcement using flexible fiber bundles enhances the fracture strength of reattached posterior teeth and one study reported that the use of flexible polyethylene fibers improves fracture resistance in molars with reattached cusps. Within the limitations of the studies included in the review, there is low-quality evidence that reinforcement of reattached fragments using FRC posts or fibers improves fracture resistance. The reattached fractured fragments may be susceptible to re-fracture. The use of FRC to reinforce the resin composite used for reattachment may enhance the bond strength and increase resistance to fracture. How to cite this article: Albar NHM. Evaluation of Fracture Resistance of Reattached Tooth Fragments Restored Using Fiber-reinforced Composites: A Systematic Review. J Contemp Dent Pract 2024;25(6):605-615.

Fatigue Characteristics Analysis of Carbon Fiber Laminates with Multiple Initial Cracks

In the entire wind turbine system, the blade acts as the central load-bearing element, with its stability and reliability being essential for the safe and effective operation of the wind power unit. Carbon fiber, known for its high strength-to-weight ratio, high modulus, and lightweight characteristics, is extensively utilized in blade manufacturing due to its superior attributes. Despite these advantages, carbon fiber composites are frequently subjected to cyclic loading, which often results in fatigue issues. The presence of internal manufacturing defects further intensifies these fatigue challenges. Considering this, the current study focuses on carbon fiber composites with multiple pre-existing cracks, conducting both static and fatigue experiments by varying the crack length, the angle between cracks, and the distance among them to understand their influence on the fatigue life under various conditions. Furthermore, this study leverages the advantages of Paris theory combined with the Extended Finite Element Method (XFEM) to simulate cracks of arbitrary shapes, introducing a fatigue simulation method for carbon fiber composite laminates with multiple cracks to analyze their fatigue characteristics. Concurrently, the Particle Swarm Optimization (PSO) algorithm is employed to determine the optimal weight configuration, and the Backpropagation neural network (BP) is used to train and adjust the weights and thresholds to minimize network errors. Building on this foundation, a surrogate model for predicting the fatigue life of carbon fiber composite laminates with multiple cracks under conditions of physical parameter uncertainty has been constructed, achieving modeling and assessment of fatigue reliability. This research offers theoretical insights and methodological guidance for the utilization of carbon fiber-reinforced composites in wind turbine blade applications.

Hierarchical Interfacial Construction by Grafting Cellulose Nanocrystals onto Carbon Fiber for Improving the Mechanical Performance of Epoxy Composites.

Carbon fiber-reinforced composites have been widely used in the aerospace industry because of their superior comprehensive performance, including high strength, low density, fatigue resistance, long service life, etc. The interface between the fiber reinforcement and the matrix is one of the key factors that determines the performance of the composites. The construction of covalent bonding connections between the components has proven to be an effective strategy for improving the interfacial bonding strength but always reduces the toughness. In this work, dual silane coupling agents are applied to covalently connect cellulose nanocrystals (CNCs) onto carbon fibers, constructing hierarchical interfacial connections between the fibers and the epoxy matrix and significantly improving the interfacial bonding strength. As a result, the tensile strength of the epoxy composites increased from 519 MPa to nearly 900 MPa, which provides a potential approach for significantly improving the mechanical performance of composites.

A multiscale modeling for progressive failure behavior of unidirectional fiber-reinforced composites based on phase-field method

The effective macroscopic properties of composites are determined by the intricate interactions among the individual components within their microstructure. Preserving these microscopic details during the failure simulation of macrostructures presents significant challenges. This work proposes a multiscale modeling framework to numerically predict the macroscopic fracture properties of unidirectional fiber-reinforced composites based on micromechanical analysis. In this study, 2D representative volume elements (RVEs) combined with the phase-field method are utilized to simulate fiber-reinforced composites under transverse loadings. A series of representative loading conditions are employed to investigate cracking patterns and to construct failure strength envelopes of the composites subjected to different multiaxial proportional loadings. By extracting the softening curve from the uniaxial tensile simulation of the RVE and fitting it with a tenth-order polynomial, the homogenized cohesive law, combined with the phase-field method, is applied to the damage analysis of macroscopic heterogeneous materials. The homogenized model of unidirectional fiber reinforced composites is numerically validated through simulations of a 2D flat plate. The simulation results demonstrate the excellent potential of the proposed multiscale modeling framework to accurately and efficiently predict the progressive failure and fracture behavior of fiber-reinforced composites in engineering applications.

New 3D petal-like structures with lightweight, high strength, high energy absorption, and auxetic characteristics

A novel type of petal-like structure that exhibits superior mechanical properties, was proposed and fabricated by integrating advantages of metamaterial, multi-stage deformation, and high strength of fiber-reinforced composites. Compression testing and finite element analysis were first conducted on three petal-like structures formed with different angles and made from fiber-reinforced composites. The findings indicated that these composite-based multi-cell structures can also exhibit a satisfactory stress plateau stage through judicious structural design. After ensuring the structures' performance under quasi-static compression load, the impact resistance of the new structures was further examined. It was found that the structure's auxetic characteristics diminished under low-speed impact load. However, under a 20 J impact load, the structures exhibited energy absorption characteristics (SEA) that surpassed those of both conventional and other new auxetic structures by 8–40 times. These promising results demonstrate that the newly designed petal-like structures have high potential applications in various fields such as construction and automotive industries.

Performance-tunable thermal barrier coating for carbon fiber-reinforced plastic composites via flame spraying

Thermal barrier coatings (TBCs) are essential for improving the heat resistance of materials operating in high-temperature environments. This paper proposes a new method for manufacturing double-layered TBC with graded porosity for carbon fiber-reinforced plastic (CFRP) composites. The TBC was created by a flame spraying process, consisting of relatively dense and porous layers: (1) a dense layer was produced by spraying yttria-stabilized zirconia (YSZ) particles directly onto neat carbon fabric substrate and (2) a porous layer was prepared by co-spraying YSZ particles with sacrificial polyetheretherketone (PEEK) particles. The porosity of the porous layer was controlled by varying a PEEK injection distance (D) and a PEEK feed rate (R). The correlation between porosity and thermal conductivity of the TBC layer was investigated to assess its thermal barrier performance. The TBC fabricated with the D = 5 cm and the R = 1.0 g/min offered the optimal porosity and conductivity. The 640μm-thick TBC with 34% porosity and 0.27 W/m·K thermal conductivity protected the CFRP substrate remarkably under the subjected torch at 500°C, as the TBC layer reduced the surface temperature of CFRP to 230°C. Thermomechanical analysis, following thermal shock tests, revealed that the double-layered TBC/CFRP composite retained 87% and 75% of its pristine flexural strength and modulus, respectively, while the neat CFRP composite was completely burnt out. This study explored the application of flame spray technology to develop highly effective double-layered TBCs with tunable porosity to maximize their thermal barrier performances. All results from the current study provide new insights into the design and development of TBC and CFRP composites, which will benefit a wide range of lightweight high-temperature applications.

Mechanical and flammability properties of ultrasonically processed silane-treated areca-banana fiber-reinforced epoxy composites for lightweight applications

Mechanical and flammability properties of ultrasonically processed silane-treated areca-banana fiber-reinforced epoxy composites for lightweight applications

Investigation of Sugarcane Bagasse Ash (SBA)-Based Engineered Geopolymer Mortar Reinforced with Coconut Fibre for Engineered Geopolymer Composites

In recent years, there have been growing demand for fibre-reinforced cementitious composites using materials wastes to reduce cost and cement usage in concrete production. Therefore, this study aims to prepare sugarcane bagasse ash (SBA)-based geopolymer reinforced with coconut fibre as a material suitability evaluation for engineered geopolymer composites. The sugarcane baggase ash was characterised for its physical and chemical properties using scanning electron microscopy (SEM), Energy dispersive X-ray spectroscopy (EDS), X-ray powder diffraction (XRD). The coconut fibres was added at 0%, 1%, 2%, and 3%, while the plain cement mortar was used as the control mix. Both destructive (compressive and tensile strength) and non- destructive test (water absorption, and ultrasonic pulse velocity test) were conducted on the resulting geopolymer mortar. The result of the SBA characterisation showed that the SBA met the ASTM C618 requirement for a pozzolanic material. The addition of 1% fibre to the geopolymer composite resulted in enhanced durability property than the plain cement mortar. The ultrasonic pulse velocity test demonstrated that bagasse ash-based geopolymer composites can be classified as a excellent cementitious material. The study also found the engineered cementitious composite showed better compressive and tensile strength than the plain concrete mortar, while the addition of fibre provided a denser microstructure for additional strength. The optimum fibre content was found at 1% for improved water absorption performance, UPV, and compressive strength. The study concludes that SBA composite reinforced with coconut fibre can provide better alternatives to achieve sustainability in engineered geopolymer concrete applications.

Exploring the influence of specimen types on the intralaminar fracture behavior of fiber-reinforced polymer matrix composites

The accurate determination of fracture toughness of fiber-reinforced composites is critical for the assessment of structural integrity. Although there have been many studies on the intralaminar fracture behavior of composites, satisfactory results have not yet been obtained regarding the influence of specimen types. In this paper, commonly used fracture specimens (DCT, CT, ESET, pin-loaded SENT and clamped SENT specimen) are applied to study their applicability in the fracture behaviors of composites with different orientations. And the impact of data processing methods for the area method, GC-compliance and GC-stress intensity factors on fracture performance was analyzed. The results showed that the above three data processing methods have obtained relatively consistent fracture properties. Different specimens obtained significantly various results, showing a gradually decreasing trend from clamped SENT, ESET, pin-loaded SENT, CT to DCT. Furthermore, considering that the clamped SENT specimen is closest to the Mode-I fracture toughness obtained from the DCB specimen, and there is no compression damage in the experiments under different orientations, this specimen type is the most recommended specimen. Finally, the failure mechanisms of carbon fiber-reinforced composite under different specimen types and orientations were revealed. As the orientation angle increases (β from 0° to 90°), the failure mode gradually transitions from matrix cracking and interface debonding to matrix shear and fiber fracture. The above achievements will contribute to a deeper understanding of the intralaminar fracture process and failure mechanism of fiber-reinforced composites.

Upcycling Post-Consumer Paint Pail Plastic Waste.

The need for ending plastic waste and creating a circular economy has prompted significant interest in developing a new family of composite materials through recycling and recovery of waste resources (including bio-sourced materials). In this work, a family of natural fiber-reinforced plastic composites has been developed from paint pail waste recycled polypropylene (rPP) and waste wool fibers of different diameter and aspect ratio. Composites were fabricated by melt processing using polypropylene-graft-maleic anhydride as a compatibilizer. The internal morphology, interfacial and thermal characteristics, viscoelastic behavior, water sorption/wettability, and mechanical properties of composites were studied using electron microscopy, high-resolution synchrotron Fourier transform infrared microspectroscopy, thermal analysis, rheology, immersion test, contact angle measurement, tensile test and flexural test. The composite matrix exhibited an internal morphology of coalescent micro-droplets due to the presence of polyethylene and dry paint in the rPP phase. In general, the rheological and mechanical properties of the composites comprising higher-aspect-ratio (lower diameter) fibers exhibited relatively superior performance. About an 18% increase in tensile strength and a 39% increase in flexural strength were measured for composites with an optimal fiber loading of 10 wt.%. Interfacial debonding and fiber pull-out were observed as the main failure mechanism of the composites. The developed composites have potential for applications in automotive, decking, and building industries.

Damage and fracture studies of continuous flax fiber-reinforced composites 3D printed by in-nozzle impregnation additive manufacturing

Additive manufacturing (AM) of continuous yarn-reinforced biobased composites presents multi-functional properties and low environmental impact of this technology. Few studies focused on the mechanical damage mechanisms of continuous biobased composites obtained by AM processes, while it is a topic of high interest for the mastery of mechanical behaviors and optimization of the materials for high requirement applications. This study aims to assess the damage and fracture modes of continuous flax yarn-reinforced PLA manufactured by AM, with different yarn orientations. The additively manufactured biobased composites were characterized by tensile test, 3D microscopy and micro-tomography to link the process-structure-properties relationships regarding the damage and fracture modes. The results showed that the 0° manufactured composite had a significant enhancement of tensile properties compared to other configurations. The damage mechanism presented fiber rupture with polymer transverse cracks at 0°, while the 45° and 90°-oriented composites showed premature fiber/matrix interface debonding. This study aims to find the relationship between damage mechanisms, deposition strategy, and anisotropy of the additively manufactured long vegetal fibers-reinforced biobased composite materials. The results bring a new understanding of the anisotropy and defects in printed composite materials regarding their mechanical behaviors during damage.

Self-healing performance of engineered geopolymer composites subjected to sodium sulphate

Engineered geopolymer composites (EGCs) have self-healing potential due to their multiple fine-cracking features. However, water immersion, as a self-healing condition for fibre-reinforced cement-based composites, may limit the self-healing ability of EGCs due to water would not directly participate in the precipitation reaction. By contrast, sodium sulphate is proved as an effective activator to promote the geopolymerisation process, while the self-healing performance of EGCs exposed to sodium sulphate has not been comprehensively demonstrated in the literature. Therefore, this paper investigates the self-healing performance of the EGCs subjected to sodium sulphate (Na2SO4) under wet-dry cycles. The results show that the EGCs preloaded at 3 days attain a higher increment of C-(A)-S-H gels at the cracks than those preloaded at 28 days, indicating the EGCs cracked at the early age have better self-healing performance under sulphate exposure. Besides, ettringite and calcium carbonate are detected as the self-healing products in the EGCs preloaded at 3 days, while the ettringite cannot be found in the EGCs preloaded at 28 days. The EGCs exposed to 5 % Na2SO4 solution and wet-dry cycles can achieve self-healing by forming more CaCO3. Increasing the Na2SO4 concentration to 10 % can accomplish self-healing by facilitating the C-(A)-S-H and CaCO3 formation, enhancing the tensile stiffness recovery and crack width reduction ratios for the EGCs with tensile strains of 2 % and 4 % at 3 days. Decreasing the preloading level also improves the tensile stiffness recovery and crack width reduction ratios regardless of the Na2SO4 concentration and preloading age, since the self-healing products are easier to fill the small cracks. Through a combination of Na2SO4 solution and wet-dry cycles, this study develops a new strategy for the accomplishment of self-healing of EGCs.

Effects of minimally invasive endodontic access cavity in molar teeth on polymerization, porosity and fracture resistance

Minimally invasive access cavities have been proposed in the last decade to reduce tooth tissue loss during endodontic treatment and mitigate compromised fracture resistance of endodontically treated teeth. Fracture resistance of molars with different types of access cavity design may be affected by restorative materials and aging. Insufficient literature data exist on the effect of cavity design and type of restorative materials on restorative aspects such as material adaptation or photo-polymerization in restricted access cavities. This study analyses quality of polymerization, material adaptation and fracture resistance of molars with different types of access cavities restored with glass-ionomer, high-viscosity fiber-reinforced bulk-fill and nanofilled resin composite. Plastic molar teeth with truss (TREC) and traditional endodontic access cavity (TEC) were restored with nanofilled composite (Filtek Supreme), glass-ionomer Fuji IX and Filtek or fiber-reinforced everX Posterior and Filtek. Porosity was determined using microcomputer tomography and the degree of conversion of resin-based materals using micro-Raman spectroscopy. Human molars prepared and restored in the same way were used for fracture resistance testing at baseline and after thermocycling. The results demonstrate that high-viscosity fiber-reinforced composite was difficult to adapt in TREC cavity leading to greater porosity than Filtek or Fuji. TREC design did not affect composite polymerization and led to higher fracture resistance of restored molars compared to TEC but also more unrestorable fractures.

Research progress on laser processing of carbon fiber-reinforced composites

Research progress on laser processing of carbon fiber-reinforced composites

Additive manufacturing of continuous fiber-reinforced polymer composites: current trend and future directions

Additive manufacturing of continuous fiber-reinforced polymer composites: current trend and future directions

An analysis of diffusion mechanism and mechanical properties of jute, JUCO, and banana fiber composites in three different mediums

Natural fiber-reinforced polymer composites (NFRPC) are the most desirable for their low-cost, eco-friendly, and high-durability properties. Scientists are facing numerous challenges with this type of composite in a wet or high-humid environment. High water absorption and reduced mechanical properties are the main concerns for this type of composite. A new kind of fiber mat called JUCO, which is a mixture of jute and cotton, is introduced here. Banana fiber and jute yarn were used to fabricate unidirectional mats, which were made using a custom-designed handloom. The composite fabrication was done by hand layup with the cold press method. The tensile and flexural strengths decreased after immersion in three mediums (pH 3, pH 7, and pH 8) for 150 days due to the water aging effect. Minimum strength was found when the samples were immersed in pH 3 mediums. Tensile and flexural test results were also evaluated by the finite elemental method (FEM) to validate the experimental results. The main objectives of this study are to investigate the mechanical properties and degradation due to the aging of newly developed JUCO fiber-based composites.

Tensile Properties of Open Hole and Unhole Sugar Palm ‘Ijuk’ (SPI) Fibre Composite Treated with Sodium Hydroxide (NaOH)

This study evaluates the effects of sodium hydroxide (NaOH) treatment on tensile properties of sugar palm 'ijuk' (SPI) fibre-reinforced polymer (FRP) composites, with and without an open hole that acts as a stress concentrator. The NaOH treatment is aimed to improve the interfacial adhesion between SPI fibres and polymer matrix. Composite specimens were prepared using the hand lay-up method, incorporating SPI fibres in various orientations, and featuring a 6 mm diameter hole. Tensile tests were conducted to evaluate the mechanical performance of SPI FRP composite, including ultimate tensile strength, Young's modulus, and elongation at break. The research also compared the properties of SPI to those of synthetic glass fibre in fibre-reinforced polymer composites. The results showed that NaOH treatment significantly improves the fibre-matrix adhesion with 26% increase in tensile strength, leading to enhanced tensile properties in both samples, regardless of hole presence. The 0° orientation provides the highest strength and stiffness when the load is applied in the direction of the fibres. While for the 90° orientation, strength reduces by 14%. The impact of the hole on stress concentration and the subsequent mechanical behaviour of the open-hole specimens is substantial. The findings of this study offer insightful perspectives on the potential use ofNaOH-treated SPI fibre in structural and other applications, demonstrating its ability to withstand tensile stresses, even with geometric discontinuities like holes.

The effect of nanocellulose and silica filler on the mechanical properties of natural fiber polymer matrix composites

Natural fiber-reinforced polymer matrix composites recently got great attention in biomedical applications due to their inherent characteristics such as biocompatibility, lightweight, and biodegradability. However, natural fiber composites suffer from poor mechanical properties and weak interfacial adhesion. It is well documented that the addition of nanofiller has improved the mechanical properties of different synthetic fibers such as glass and carbon composites. The main objective of this paper is to study nanofillers' effect on the mechanical properties of unidirectional false banana fibers reinforced polymer composites. The filler materials, crystalline nanocellulose fibrils, and crystalline nanosilica particles were extracted from sugarcane bagasse and its byproducts. The composite samples were fabricated by adding the nanofillers in unidirectional natural fibers arranged in four fiber orientations (0°, 0o/90o ±45o, and quasi-isotropic), and their tensile, flexural, compression strength, thermal stability, and void content were measured following ASTM standards. The results revealed that adding nanofillers increased the tensile, flexural, and compressive strengths by 16 % (98.83 Mpa), 11 % (161.60 Mpa), and 23 % (114.62 Mpa), respectively. Similarly, at 0° orientation, the addition of nanoparticles enhances the tensile, bending, and compressive modulus by 30 % (15.43 Gpa), 12 % (13.52 Gpa), and 60 % (42.6 Gpa), respectively. On the other hand, the void content was reduced with the addition of nanofillers. The results also revealed that composites with crystalline nanosilica particle fillers had superior thermal stability compared to crystalline nanocellulose fibril fillers. The overall results of this research give the confidence that nano particle-filled natural fiber composites can be used for bio-based engineering applications, such as prosthetic sockets.