The severe environmental pollution related to the manufacturing, recycling and disposal of metal-based and synthetic fiber-based composites has a major impact on human and animal life. A wide range of studies are conducted on alternative materials in order to reduce greenhouse gas emissions. Various industries are focusing on using natural fibers from banana, jute, coir, hemp, pineapple, areca, kenaf, Sterculia foetida and Delonix regia that are the key sources of different components for developing nanocomposites. Drilling is a vital factor in the assembly process of composites. The amorphous structure of the natural fibers causes the formation of cracks at the entry and exit sides of the drilled hole. So, in the present work a nanocomposite was synthesized and optimized the machining parameters, which affect the surface finish of the hole at the entry, exit and inner surface of the drilled hole. The effect of the hybridization of glass fiber with the pineapple leaf fiber and areca fiber was studied in terms of tensile properties, delamination around the hole and surface roughness. The microstructure of the holes was studied by Scanning Electron Microscopy.