Fiber-reinforced Composites Research Articles

Fatigue life prediction of continuous glass-fiber reinforced elium thermoplastic composites via energy based thermographic approach

The long-term performance of composite materials produced within the scope of lightweighting, should be examined with fatigue tests. Nonetheless, these tests take a long time and require a lot of energy. For overcoming these limitations, the thermographic method was used during the fatigue test and recorded temperature changes. Before starting the fatigue tests, the mechanical properties of glass fiber-reinforced Elium-based composites were clarified via tensile and three-point bending tests for two different fiber orientations (0/90 and 0/90/45). Then, the fatigue tests were carried out to identify the long-term performance of these materials. During the test, temperature values were recorded with an infrared camera. These values were converted to energy dissipated per cycle and temperature increase. These data established high cycle fatigue strength limits for both fiber orientations. In addition, using the fatigue test data, the potential cycles at lower stress values were calculated using a mathematical model and were validated with verification tests. With this method, the fatigue cycle has been predicted for high cycle fatigue tests and it carried out the validation test successfully with 93% similarity of fatigue cycle. Finally, the cycle numbers of all low-stress high-cycle fatigue tests were determined.

Synthesis and characterization of pectin biopolymer from orange peel wastes and its effect on pineapple fiber-reinforced vinyl ester composite

Synthesis and characterization of pectin biopolymer from orange peel wastes and its effect on pineapple fiber-reinforced vinyl ester composite

Hybrid Fiber-Reinforced Biocomposites for Marine Applications: A Review

Highly efficient fiber-reinforced composites find extensive application in diverse industries. Yet, conventional fiber-reinforced composites have significant environmental impacts during both manufacturing and disposal. Environmentally friendly fiber-reinforced composites have garnered significant attention within the framework of sustainable development. Utilizing natural fibers in place of synthetic fibers and progressively decreasing the use of synthetic fibers are the main approaches to achieving a balance between economic progress and environmental quality. Attention is increasingly being drawn to natural fiber-reinforced biocomposites that exhibit outstanding environmental performance, exceptional physical and mechanical capabilities, and biological features. The lightweight and high-strength characteristics of these biocomposites enable them to significantly decrease the weight of structures, making them increasingly popular in many industries. The objective of this review is to evaluate the effectiveness of hybrid fiber-reinforced biocomposites in marine applications, specifically examining their mechanical characteristics, resistance to seawater, and ability to absorb moisture, all while advocating for sustainable material methodologies. To achieve this objective, the paper delineates the distinction between synthetic and natural fibers, examines the benefits of hybrid fiber-reinforced biocomposite materials, and addresses the obstacles and effective approaches in their production and application in seawater. Considering the review analysis, it can be inferred that the use of fiber-reinforced biocomposites in maritime applications shows significant potential and has abundant untapped growth prospects in the future years.

Tensorial harmonic bases of arbitrary order with applications in elasticity, elastoviscoplasticity and texture-based modeling

In continuum mechanics, one regularly encounters higher-order tensors that require tensorial bases for theoretical or numerical calculations. By using results from [Formula: see text] representation theory, we present a method to derive tensorial harmonic bases which unifies existing approaches in one framework. Applying this convention to symmetric second-order tensors results in a second-order harmonic basis which, for example, simplifies the depiction and numerical handling of stiffness tensors for most common material symmetries and reduces the computational effort involved in implementations of incompressible elastoviscoplastic material laws. The same convention can be applied to texture analysis to yield tensorial texture coefficients for both polycrystals and fiber-reinforced composites. Rotations of higher-order tensors are particularly efficient in harmonic bases as both material and index symmetries can be exploited. While special attention is given here to the examples of small-strain material laws and texture analysis, the framework is entirely general and can be used to simplify calculations in other physical contexts involving tensors of arbitrary order and symmetry. A Python implementation of the harmonic basis convention defined in this work is available as a Supplementary Material.

Autonomous intelligent additive manufacturing of continuous fiber-reinforced composites: data-enhanced knowledgebase and multi-sensor fusion

ABSTRACT Additive manufacturing (AM) are an emerging technique to generate complex structures of composite. However, the instability of the AM process leads to adverse manufacturing effects, including dimensional inaccuracies and poor mechanical performance in CFRP composites. Online monitoring and adaptive control based on autonomous cognition are suggested to ensure the accuracy of as-fabricated parts and enhance their quality upon manufacturing. In this study, a method of online monitoring and self-adaptive control based on multi-sensor fusion is proposed to predict and adjust the process parameters during AM of CFRP. The force sensor, visual camera, and thermal camera are employed to obtain the multiple signals upon manufacturing and then realize the autonomous perception, cognition, and decision features. Herein, the quantitative correlations between local defects and multi-sensing features are established to guide the decision-making of closed-loop adjustment. Besides, an empirical surrogate model between the misalignment of fiber bundles and input parameters is built to predict the proper parameters. Moreover, the temperature difference and contact force are selected as the controlled features, which are acquired using a thermal camera and a force sensor. The proposed system offers a novel framework for bolstering both the stability of the AM process and the quality of fabricated components.

Char, gas, and action: Transfer of the flame-retardant modes of action in epoxy resins and their fiber-reinforced composites

Flame retardants are often developed for epoxy resins and then transferred into their fiber-reinforced composites with uncertain results. Understanding this transfer in detail represents a critical scientific challenge. This study systematically compares epoxy resins with their glass-fiber reinforced composites, focusing on bisphenol A diglycidyl ether with the hardener dicyandiamide, the flame retardants melamine polyphosphate, ammonium polyphosphate, and silane ammonium polyphosphate, along with inorganic silicate. The research investigates changes in pyrolysis (thermogravimetry), flammability (UL 94, limiting oxygen index), and fire behavior (cone calorimeter) while also examining the flame-retardant modes of action and overall fire performance. The findings reveal that alterations in the amount of fuel, thermal properties, melt flow, and protective layer significantly impact ignition, flammability, and fire load, with a critical reduction in carbonaceous char within the composites preventing intumescence. This study quantifies the effects and provides a fundamental scientific understanding of the complex transfer process of flame retardants from resins to composites, offering essential insights that are of major importance for developing more effective flame-retardant materials.

Theoretical model to predict the fracture strength of fiber-reinforced ceramic matrix composites at elevated temperatures

The mechanical properties of ceramics and their composites in extreme environments, especially the fracture strength under high-temperature conditions, are key factors in assessing the safety and reliability of equipment. In this study, a temperature-dependent theoretical model is proposed with the aim of predicting the fracture strength for fiber-reinforced ceramic matrix composites at elevated temperature environments. This model encompasses not just the collective effects of various factors, including the Young's modulus of both fibers and matrix, the fiber volume fraction, and the melting point of the matrix, but also integrates the evolution of the Young's modulus of the fiber and matrix with temperature. Through the validation of multiple sets of experimental results, it is shown that the proposed model is able to predict the fracture strength of composites at elevated temperatures more accurately without conducting any high-temperature destructive tests. This model can help engineers and scientists to evaluate the mechanical properties of fiber-reinforced ceramic matrix composites at high temperatures more conveniently, thus guiding the optimal design and practical application of the materials, and thus improving the reliability and safety of the materials.

Development of the Views of Yu.N. Rabotnov on Strength Criteria of Composites

Besides the well-known fundamental works of Yu.N. Rabotnov in the field of hereditary elasticity and creep theory, one of the aspects of his scientific activity was the mechanics of composite materials and, in particular, a new class of strength criteria for structurally anisotropic composites proposed by him. The main feature of Yuri Rabotnov’s approach was not an attempt to construct a uniform smooth limiting surface in the stress-space, but taking into account real fracture mechanisms, which, as a rule, are directional in nature. Now such approaches become crucial in calculation algorithms modeling the fracture process with taking into account the degradation of elastic and strength properties, but in the period of the first Yu.N. Rabotnov’s papers they were pioneering and caused certain discussions. Development and application of some of Rabotnov’s proposed types of strength criteria for fiber-reinforced composites in tension, compression and complex stress state are discussed in this anniversary paper.

Recyclable hemp hurd fibre-reinforced PLA composites for 3D printing

In this study, 3D printing filaments were produced from hemp hurd fibre-reinforced polylactide (PLA) composites. Hemp hurd microfibres were obtained through alkaline digestion followed by a bleaching treatment and were used to produce PLA-based composites with 20–40 wt% fibre content for fused deposition modelling. Tensile testing of 3D printed composites revealed a gradual increase of Young's modulus with the addition of fibres, reaching a maximum of 7.1 GPa for the 40 wt% composite - a two-fold increase to neat PLA. However, tensile strength was only improved for the 20 wt% formulation, with an increase of 8% in comparison with neat PLA. Nevertheless, the thermo-mechanical properties of the composites were significantly enhanced with the addition of fibres. In addition, physical objects were printed from the recycled filaments to assess their recyclability and printability. It was found that the recycled filaments maintained comparable mechanical properties and printability after three recycling cycles.

Impact sensing, localization and damage assessment in Fiber-Reinforced composites with ZnO Nanowires-Based sensor array

The structural integrity and monitoring of load distributions in composites are critical for safety and economic efficiency but still challenging. Herein, zinc oxide nanowires (ZnO NWs) were embedded into a carbon fiber-reinforced composite serving as mechanical reinforcement and sensing components. The presence of ZnO NWs in the composite material increased the flexural strength, interlaminar, and interfacial shear strength by respectively 4.9 %, 8.8 %, and 19.9 % due to the strong bonding at the fiber/resin interface and the mechanical interlocking effect. Additionally, the piezoelectric nature of ZnO NWs with an asymmetric crystal structure generated piezoelectric charges under stress, thereby enhancing the sensitivity of capacitive monitoring. A self-developed algorithm was then designed to analyze the array capacitance changes collected from the prepared composite laminate to determine the impact load with high precision with an error margin of 3 mm and not exceeding 0.25 MPa. Furthermore, damage was also able to be detected by monitoring capacitance changes. Overall, the proposed high-precision and minimally aggressive approach for load localization and quantification provides a promising direction and strategic pathway for the development of smart self-monitoring composites.

Development of Fiber-Reinforced Polymer Composites for Additive Manufacturing and Multi-Material Structures in Sustainable Applications

This study investigates the mechanical properties of carbon and natural fiber-reinforced Polylactic Acid (PLA) and Polyethylene Terephthalate Glycol (PETG) composites produced via Additive Manufacturing (AM), focusing on Material Extrusion (MEX). The performance of filaments made from pre-consumer recycled PLA (rPLA) and PETG, with varying weight percentages of hemp and jute short fibers, was evaluated through tensile testing. Comparisons were made between the original filaments (PLA, carbon fiber-reinforced PLA [CF–PLA], and PETG) and their recycled versions. Multi-material compositions—neat PLA and PETG, single-graded (PLA + CF–PLA, PETG + CF–PETG), and multi-gradient (PLA + CF–PLA + PLA, PETG + CF–PETG + PETG)—were analyzed for mechanical properties. Optical microscope images of multi-material specimens were captured before and after fracture to assess failure mechanisms. The results indicate that the original CF–PETG filaments achieved a tensile strength of 50.14 MPa, which is higher than rPLA, PLA, and CF–PLA by 2%, 70%, and 6.7%, respectively. The re-manufactured PLA filaments reinforced with 7 wt% hemp fibers exhibited a tensile strength of 38.8 MPa, representing a 29% increase compared to the original PLA filaments and a 26% improvement over recycled PLA. Additionally, incorporating 7% jute fiber into PETG resulted in a tensile strength of 62.38 MPa, reflecting a 12% improvement over the original PETG filaments and a 15% increase compared to the recycled PETG filaments. Among specimens produced by AM, CF–PLA and rPLA demonstrated the highest tensile and compressive strengths. However, multi-material composites showed reduced mechanical performance compared to neat PLA and PETG, highlighting the need for improved interlayer adhesion. This study emphasizes the importance of optimizing material combinations and fiber reinforcement to enhance the mechanical properties of composites produced through AM.

An in situ prepared fiber-based piezoresistive film for ultrasonic wave detection on nonplanar carbon fiber-reinforced composites

Owing to the flexibility and high-frequency responsiveness, nanocomposite piezoresistive sensors are suitable for Lamb wave detection on composite materials. Various types of nanocomposite films have been developed for this purpose. However, the inelasticity trait of commonly used electrodes for the nanocomposite films impedes their application on the nonplanar surface of composites. Herein, an in situ prepared piezoresistive film based on graphene and polymethyl methacrylate nanocomposite has been proposed for ultrasonic wave detection on nonplanar carbon fiber-reinforced composites. Electrospinning method is employed to fabricate piezoresistive fiber film onto carbon fiber-reinforced polymer (CFRP) composites, and the sensitivity along the thickness direction is utilized via employing the CFRP layer as one electrode. The fabricated sensitive films exhibit the capability to detect up to 150 kHz ultrasonic signals on curved surfaces. With the help of Hilbert energy spectrum, the precise damage localization on CFRP is achieved by the sensitive film array with a relative error of only 1%. This innovation provides a new in situ preparation method for ultrasonic sensitive film on nonplanar-shaped CFRP components for nondestructive evaluation task.

Modification of fiber-reinforced composites using polymer blends as matrices

Modification of fiber-reinforced composites using polymer blends as matrices

Quasi-static punch shear behavior of glass/epoxy composite: Experimental and numerical study in artificial seawater environment

Enhancing the understanding of how fiber-reinforced polymer composites respond to high-speed impacts is crucial, particularly in comparison to Quasi-Static Punch Shear Test (QS-PST). While researchers have extensively investigated QS-PST in FRP composites through experimental and numerical approaches, there's a notable gap in studies addressing the aging effects through both experimental and numerical methods. In this study, the QS-PST was conducted on S2 glass fiber reinforced epoxy composite materials aged in an artificial seawater environment. Composite plates were fabricated using Vacuum-assisted resin transfer molding (VARTM). Test samples were subjected to aging for durations of 4, 8, and 12 months. Experimental QS-PST were performed on the samples, followed by Finite Element Analysis (FEA) using LS-DYNA and the MAT 162 material model. The mechanical properties of the composite material were incorporated into the FEA and aging effects were simulated with a maximum error of 8.08% by using the proposed material model. The results indicated that the aging process led to a reduction in the punch shear strength of the composite by up to 26.84%. These findings provide valuable insights into the degradation mechanisms of composite materials in marine environments, aiding in the development of strategies for enhanced durability and performance in such conditions.

Study on Process Parameters of Liquid–Solid Infiltration Extrusion of Continuous Carbon Fiber-Reinforced Aluminum Matrix Composites

Study on Process Parameters of Liquid–Solid Infiltration Extrusion of Continuous Carbon Fiber-Reinforced Aluminum Matrix Composites

Experimental investigation on the mechanical properties of multi-walled carbon nanotubes modified glass fiber-reinforced polymer composites

Experimental investigation on the mechanical properties of multi-walled carbon nanotubes modified glass fiber-reinforced polymer composites

Development of the forming limit diagram for fiber-reinforced thermoplastic composites and its temperature effect

The aim of this study is to investigate the formability properties of thermoplastic composite sheets and to develop a forming limit diagram (FLD) for them under ambient and elevated temperatures. Polypropylene thermoplastic composite sheets reinforced with unidirectional continuous glass fibers in a four-layer 0–90 layup were used in this research. Experimental findings demonstrate that the failure of samples at room temperature is more similar to brittle failure and occurs suddenly, whereas at elevated temperatures, the failure resembles ductile failure and occurs gradually. Employing the Nakajima method, a forming limit diagram for the composite material was successfully established at both ambient and elevated temperatures. The resultant forming limit diagrams illustrate an augmented strain tolerance of the material at elevated temperatures. Notably, despite the increased depth of stretch observed at elevated temperatures in comparison to ambient conditions, a concomitant reduction in the force requisite to induce deformation is evident.

A Novel Plasma-Enhanced Solvolysis as Alternative for Recycling Composites

In this work, a plasma-assisted solvolysis method is proposed as an alternative method for the oxidative degradation of carbon fiber-reinforced composites (CFRCs). Nitrogen plasma ignition within bubbles in a concentrated nitric acid solution is employed, combining the synergistic effects of traditional nitric acid solvolysis and plasma chemistry. A comprehensive process flowchart, including steps such as composite pretreatment, matrix dissolution, fiber recovery and cleaning, solvent regeneration and reuse, and waste treatment, is also discussed, highlighting their importance in process effectiveness. Moreover, a study on the effect of the composite’s mass on the plasma-enhanced solvolysis process is conducted, and the results are exploited for the calculation of critical parameters such as efficiency, recovery rates, capacity, fibers quality, energy consumption, consumption of raw materials, operational and installation costs, and environmental impact. A preliminary comparison to other recycling methods based on the literature findings is also attempted, and preliminary metrics to assess the sustainability of the recycling process are proposed.

Simulation and mechanical testing of 3D printing shin guard composite materials

ABSTRACT This study critically examines the composite material's mechanical properties and performance for 3D-printed shin guards. It contains a thermoplastic polymer matrix with short carbon fibre reinforcement. Shin guard stress and deformation under impact loading were modelled using FEA models. The composite material was 3D-printed and tested for tensile, flexural, and impact properties. The entire cycle of FEA models and careful mechanical testing allows for the development and evaluation of new composite materials and designs. The finite element analysis, such as maximum von Mises stress, is 2890.5 MPa. The carbon fibre-reinforced composite's mechanical properties, including tensile strength, flexural strength, and impact resistance, showed a considerable improvement over those of the unreinforced polymer. The solid design could be heavier and less adaptable than the pattern. Compared to unreinforced polymers, carbon fibre improves strength, stiffness, and impact resistance for the 3D-printed composite. This result thus proves that 3D-printed carbon fibre-reinforced composites could make superior sports protective equipment like shin guards. The FEA calculations and extensive mechanical testing provide a dependable framework for creating and testing these new composite materials and systems.

Three-Dimensional Printing Limitations of Polymers Reinforced with Continuous Stainless Steel Fibres and Curvature Stiffness

This study investigates the printability limitations of 3D-printed continuous 316L stainless steel fibre-reinforced polymer composites obtained using the Materials Extrusion (MEX) technique. The objective was to better understand the geometric printing limitations of composites fabricated using continuous steel fibres, based on a combination of bending stiffness testing and piezoresistive property studies. The 0.5 mm composite filaments used in this study were obtained by co-extruding polylactic acid (PLA), with a 316 L stainless steel fibre (SSF) bundle. The composite printability limitations were evaluated by the printing of a series of ’teardrop’ shaped geometries with angles in the range from 5° to 90° and radii between 2 and 20 mm. The morphology and dimensional measurements of the resulting PLA-SSF prints were evaluated using μCT scanning, optical microscopy, and calliper measurements. Sample sets were compared and statistically examined to evaluate the repeatability, turning ability, and geometrical print limitations, along with dimensional fluctuations between designed and as-printed structures. Comparisons of the curvature bending stiffness were made with the PLA-only polymer and with 3D-printed nylon-reinforced short and long carbon fibre composites. It was demonstrated that the stainless steel composites exhibited an increase in bending stiffness at smaller radii. The change in piezoresistance response of the PLA-SSF with load applied during the curvature bending stiffness testing demonstrated that the 3D-printed composites may have the potential for use as structural health monitoring sensors.