Dynamic Mechanical Tests Research Articles

Development of high-performance biocomposites through lignin modification and fiber reinforcement

This study aimed to develop and characterize novel biocomposites incorporating tall oil fatty acid (TOFA)-modified lignin (TeL), citric acid-esterified polyvinyl alcohol (CeP), and unbleached fibers (UNB) to enhance thermal and mechanical properties while utilizing renewable resources. The research addressed the growing demand for sustainable high-performance materials in various industrial applications. Kraft lignin was modified through esterification with TOFA, while polyvinyl alcohol (PVA) was crosslinked using citric acid. These modified components were combined with UNB to create biocomposites with varying compositions. The materials were characterized using Fourier-transform infrared spectroscopy (FTIR), dynamic mechanical analysis (DMA), thermogravimetric analysis (TGA), and tensile strength testing. FTIR analysis confirmed successful esterification of lignin and PVA, evidenced by a strong ester carbonyl peak at 1730 cm⁻1. DMA results revealed significant improvements in viscoelastic properties, with the highest glass transition temperature (Tg) of 179.47 °C observed in the sample containing maximum TeL and CeP content. TGA demonstrated enhanced thermal stability, with samples containing higher TeL and CeP content exhibiting increased char formation and residual masses up to 47% at 500 °C. Mechanical testing showed a strong correlation between composition and performance, with the optimal formulation (TeL12-CeP4-UNB4) achieving a tensile strength of 8.7 MPa and a tensile modulus of 59.3 MPa. Potential applications of these high-performance biocomposites include sustainable alternatives for packaging, automotive components, building materials or insulation, electronic devices and other industries where enhanced thermal and mechanical properties are required. These materials present a viable option for replacing conventional petroleum-based polymers, contributing to the advancement of eco-friendly industrial solutions.

Exploring the dynamic mechanical response and mesoscopic characteristics of typical frozen rock in Yulong Copper Mine

Dynamic mechanical characteristic testing at low temperatures was conducted for the typical porphyry and sandstone specimens of Yulong Copper Mine in Tibet, China. The stress and strain characteristics of the specimens at different temperatures were analyzed. A dynamic constitutive model was developed by considering the initial damage. Furthermore, microscopic damage characteristics during the water-saturated rock freezing process were investigated using the PFC3D software, revealing the mechanisms of frost heave damage to rocks. The results indicated that the water-ice phase transition either enhanced or deteriorated the specimen strength at low temperatures. Specifically, freezing at −10°C and −20°C enhanced the strength of sandstone. However, freezing at −10°C enhanced the porphyry specimens, and freezing at −20°C caused significant frost swelling injury. The new constitutive equation effectively fitted the dynamic stress and strain curves for both specimens, highlighting their differences. The maximum contact force and particle contact in the frozen rock PFC3D model were affected by rock and water particle deformations. The frost swelling deformation of water particles had a more pronounced impact on specimen damage and was related to the temperature. A specific freezing temperature existed at which the increase in saturated rock strength corresponded to the maximum specimen strength at that temperature.

Determining the Relationship Between Corneal Stiffening and Tissue Dehydration After Corneal Cross-Linking.

To quantify corneal cross-linking (CXL)-induced stiffening via mechanical testing to estimate the impact of changes in hydration levels (H) and evaluate depth-dependent tissue hydration after CXL. Eighty-three porcine corneal buttons were divided into three groups: Standard protocol CXL (S-CXL), accelerated CXL (A-CXL), and untreated (nonirradiated riboflavin-only) controls. Samples were hydrated or dehydrated to modulate H and dynamic mechanical analyzer compression tests were performed to measure Young's modulus (E). To extract the solid tissue network modulus, the cornea was modeled as a biphasic material after measuring E at different H. Corneal hydration was correlated with depth-dependent tissue thickness characterized by confocal reflection microscopy (CRM). Young's modulus increased fourfold after S-CXL (0.72 ± 0.1 MPa) and threefold after A-CXL E (0.53 ± 0.12 MPa) versus controls (0.17 ± 0.045 MPa). However, H decreased from 4.07 ± 0.35 in controls to 2.06 ± 0.2 after S-CXL and 2.79 ± 0.12 after A-CXL. After H modulation and biphasic mechanical modeling, Young's modulus for corneal solid tissue network showed only a 1.8-fold increase after S-CXL (2.25 MPa) and 1.5-fold increase after A-CXL (1.85 MPa) versus controls (1.22 MPa). With CRM, the overall thickness of the corneal tissue was found to linearly correlate to hydration H as expected. No appreciable depth dependence of hydration-induced thickness changes throughout the corneal buttons were observed. Corneal tissue hydration changes significantly impact measured corneal stiffness after CXL using mechanical testing. Not considering H leads to major overestimation of the stiffening effect of the CXL procedure. Depth-dependence of corneal thickness because of changing hydration is strongly dependent on the integrity of the tissue.

Dynamic mechanical characteristics of coal in front of the mining face under different mining layouts

To study the dynamic mechanical characteristics of coal in the area affected by mining in front of the mining face under different mining methods, an improved split Hopkinson pressure bar (SHPB) was used to apply different static loads to different positions. Then, dynamic mechanical tests were conducted on coal at different positions on the mining face, analyzing the dynamic response under strong dynamic load disturbances, under three different mining layouts. Within the range of static water pressure to the peak support pressure, the dynamic strength of coal gradually increases with increasing distance from the mining face. The dynamic strength is the smallest at the peak support pressure stress, and under strong external disturbances, instability and failure are increasingly likely to occur at the peak stress. Under the same loading rate conditions, the dynamic strength of the peak stress in coal is as follows: Protective coal-seam mining (PCM) > Top-coal caving mining (TCM) > Nonpillar mining (NM).

Nonlinear mechanical behaviour and visco-hyperelastic constitutive description of isotropic-genesis, polydomain liquid crystal elastomers at high strain rates

The mechanical behaviour of isotropic-genesis, polydomain liquid crystal elastomers (I-PLCEs) at various strain rates is systematically investigated via experiments, theoretical analysis, and numerical modelling. Experiments encompassing SEM (scanning electron microscope), DSC (differential scanning calorimetry), TGA (thermogravimetric analyser), quasi-static and dynamic (SHPB – split Hopkinson pressure bar) mechanical tests, as well as drop-weight impact tests, are undertaken to identify the nonlinear, large-strain, rate-dependent relationship between compressive stress and deformation of the I-PLCEs studied. Subsequently, a three-dimensional compressible visco-hyperelastic constitutive model for the material is established based on the summation of Cauchy stress components. The as-used model yields good agreement with experimental data, particularly an excellent description of the mechanical responses at high strain rates of 103∼104 s−1. The fully-calibrated constitutive model is implemented in the commercial finite element code ABAQUS via a virtual user-defined material (VUMAT) subroutine. The inhomogeneous deformation processes of the I-PLCEs, corresponding to impact by a hemispherically-tipped drop weight, which induces complex stress states, are also well described. Finally, when evaluated by two dimensionless physical parameters, the I-PLCEs demonstrate a more pronounced strain rate sensitivity in terms of dynamic strength and impact toughness compared to other commonly used materials, highlighting their superior performance in dynamic loading scenarios. The present study is helpful for the design and development of impact-resistant LCE-based materials and structures.

Advancing the performance characteristics of rubber asphalt mixtures through the integration of Basic Oxygen Furnace (BOF) slag: A focus on static and dynamic mechanical enhancements.

To investigate the advantageous effects of incorporating industrial solid waste basic oxygen furnace (BOF) slag on the mechanical characteristics of warm-mixed rubber asphalt (WMRA) and hot-mixed rubber asphalt (HMRA) mixture, varying proportions of BOF slag were substituted for limestone coarse aggregates (0%, 25%, 50%, and 75%). Additionally, a 1.5% dosage of Sasobit warm-mixed modifier was introduced to prepare the rubber asphalt. Subsequent to preparation, both static mechanical tests (including Marshall and indirect tensile tests) and dynamic mechanical tests (including dynamic creep and elastic modulus tests) were conducted to evaluate the influence of BOF slag on the mechanical behavior of WMRA and HMRA mixtures across different substitution levels. Following testing, a two-way analysis of variance (ANOVA) was employed to dissect the impact of BOF slag content and Sasobit warm-mixed modifier on the static and dynamic mechanical properties of the rubber asphalt mixtures. The findings reveal that BOF slag exhibits commendable engineering aggregate properties, enabling substantial substitution of coarse aggregates in both HMRA and WMRA mixtures. As the proportion of BOF slag increases, it enhances the resistance of asphalt mixtures to permanent deformation and cracking under static and dynamic loading conditions, while broadening the range of elastic deformation for both WMRA and HMRA mixtures subjected to repeated loading. Moreover, a synergistic enhancement in the resistance of rubber asphalt mixtures to dynamic load-induced deformation is observed when employing both BOF slag and Sasobit warm-mixed modifier. The findings offer valuable insights for enhancing the performance of WMRA and HMRA mixtures, as well as broadening the utilization of BOF slag and waste rubber.

Integrating dynamic relaxation with inelastic deformation in metallic glasses: Theoretical insights and experimental validation

Metallic glasses (MGs), a metastable material far from equilibrium, exhibit intricate dynamic relaxation behaviors. The challenge lies in developing a model that accurately describes the dynamics and deformation mechanisms of MG. This paper introduces a model integrating dynamic relaxation with deformation behavior. Validation through dynamic mechanical analysis, stress relaxation, creep, and strain recovery tests confirm the existence of four deformation modes: elasticity, anelasticity from β relaxation, anelasticity from α relaxation at low temperatures, and viscoplasticity from α relaxation at high temperatures. The model captures all of these deformation modes. The dynamical mechanical spectrum and stress relaxation spectrum unveil dynamic features during glass to liquid transition, and a simple and effective experimental method was developed for identifying ultra-low-frequency dynamic relaxation. This work provides new perspectives on the study of relaxation dynamics in glassy states and establishes important connections between dynamic relaxation behavior and deformation mechanisms. These findings lay a theoretical and experimental foundation for the broad application of MGs.

Mechanical and optical properties assessment of an innovative PDMS/beeswax composite for a wide range of applications

Polydimethylsiloxane (PDMS) is an elastomer that has received primary attention from researchers due to its excellent physical, chemical, and thermal properties, together with biocompatibility and high flexibility properties. Another material that has been receiving attention is beeswax because it is a natural raw material, extremely ductile, and biodegradable, with peculiar hydrophobic properties. These materials are applied in hydrophobic coatings, clear films for foods, and films with controllable transparency. However, there is no study with a wide range of mechanical, optical, and wettability tests, and with various proportions of beeswax reported to date. Thus, we report an experimental study of these properties of pure PDMS with the addition of beeswax and manufactured in a multifunctional vacuum chamber. In this study, we report in a tensile test a 37% increase in deformation of a sample containing 1% beeswax (BW1%) when compared to pure PDMS (BW0%). The Shore A hardness test revealed a 27% increase in the BW8% sample compared to BW0%. In the optical test, the samples were subjected to a temperature of 80 °C and the BW1% sample increased 30% in transmittance when compared to room temperature making it as transparent as BW0% in the visible region. The thermogravimetric analysis showed thermal stability of the BW8% composite up to a temperature of 200 °C. The dynamic mechanical analysis test revealed a 100% increase in the storage modulus of the BW8% composite. Finally, in the wettability test, the composite BW8% presented a contact angle with water of 145°. As a result of this wide range of tests, it is possible to increase the hydrophobic properties of PDMS with beeswax and the composite has great potential for application in smart devices, food and medicines packaging films, and films with controllable transparency, water-repellent surfaces, and anti-corrosive coatings.

A novel rigidizable inflatable lunar habitation system: design concept and material characterization

Constructing lunar bases is crucial as lunar missions progress towards utilization and exploitation. The challenging lunar environment, with its unique characteristics and limited resources, requires special materials, structures, and construction methods. Inflatable structures offer great potential for lunar construction due to their advantages in transportation, stowage, construction, and reliability. This paper proposes a rigidizable inflatable lunar habitat that maintains its shape even after air leakage, enhancing safety, durability, and fixability. The membrane material adapts to different requirements during transportation, construction, and service, achieved through solid-state actuation of shape memory polymer (SMP) for stiffness variation, allowing multiple moves and ground tests. This work comprises three parts: 1) system: design concept and construction processes, 2) material: design and characterization of restraint and rigidization materials, and 3) structure: numerical validation of structure properties. Finite element analysis, based on material models obtained through dynamic mechanical analysis (DMA) and tensile tests, demonstrates the effectiveness of including an SMP rigidization layer in preventing collapse and enhancing dynamic properties. This paper not only proposes a new system, but also provides material design methods and requirements, along with structural validation techniques. Findings validate the feasibility of rigidizable inflatable lunar habitats, applicable in extreme environments, also in temporary buildings, space structures, and soft robotics.

Preparation, mechanical analysis and investigation of swelling behavior of boron nitride reinforced hydrogel polymer composite films

AbstractThis study presents the preparation, hydrogel kinetics, and mechanical analysis of Boron Nitride (BN) reinforced PVA/PVP/PEO‐BN hydrogel composite films using Polyvinyl alcohol (PVA), Polyvinyl pyrrolidone (PVP), and Polyethylene oxide (PEO) commercial polymers. Dynamic mechanical analysis tests reveal that PVA90PEO5PVP5‐BN composite films exhibit plastic‐viscoelastic behavior under a maximum force of 18 N. The Young's Modulus values for PVA90PEO5PVP5, PVA90PEO5PVP5‐BN%10, and PVA90PEO5PVP5‐BN%20 are 0.22, 0.32, and 0.44 MPa, respectively. The highest % Strain value is observed in PVA90PEO5PVP5‐BN%20, reaching 279.80%. In the hydrogel kinetics study, Schott's and Fickian models are utilized. The regression from the Fickian model is quite low, with exponential diffusion index, n, values lower than 0.5, indicating a classical Fickian water diffusion mechanism. Schott's model provides graphs with significantly higher regression compared to the Fickian model. The results indicate compatibility with the other model and confirm the presence of water‐based diffusion. Equilibrium swelling values (Se, g H2O/g gel) are 6.71, 7.03, and 7.91 for PVA90PEO5PVP5, PVA90PEO5PVP5, PVA90PEO5PVP5‐BN%10, and PVA90PEO5PVP5‐BN%20, respectively. Differential Scanning Calorimetry (DSC) analysis results show that the glass transition temperatures, Tg, are 52.37, 60.20, and 63.05°C for PVA90PEO5PVP5, PVA90PEO5PVP5‐BN%10, and PVA90PEO5PVP5‐BN%20, respectively.

Investigation of Dynamic Viscoelastic Asymmetric Response of PA6 Film Based on Fractional Rheological Model.

Polyamide 6 (PA6) film as a typical viscoelastic material, satisfies the time-temperature superposition (TTS), and demonstrates obvious dynamic strain amplitude and frequency correlation under dynamic load. The investigation of the dynamic mechanical behavior of PA6 film is essential to ensure the safety of these materials in practical applications. In addition, dynamic mechanical property testing under conventional experimental conditions generally focuses on the short-term mechanical performance of materials. Therefore, the dynamic viscoelasticity of PA6 film was tested using a dynamic thermo-mechanical analyzer (DMA) in this study, and the complex modulus master curve was constructed based on time-temperature superposition (TTS) to realize the accelerated characterization of long-term mechanical properties. Furthermore, according to experimentally obtained asymmetric characteristics of the Cole-Cole diagram and the loss modulus master curve of the PA6 film, the parameter distribution of the fractional Zener model and the modified fractional Zener model were compared, and the asymmetric dynamic viscoelastic response of PA6 film under different conditions was systematically investigated using these models. The results indicate that the modified fractional Zener model can truly describe the dynamic asymmetric characteristics of PA6 film, verify the feasibility and advantages of the modified fractional rheological model, and provide some theoretical guidance for exploring the tensile rheological mechanism of PA6 film.

Mechanical and Dynamic Mechanical Characterization of Epoxy Composites Reinforced with Casuarina Leaf Bio Fibre

This study investigates the influence of casuarina leaf biofibre on the mechanical and morphological characteristics of epoxy resin composites. Composites were prepared using the hand-layup method, incorporating varying volume fractions of the biofibre (4%, 8%, 12%, 16%, 20% and 24% v/v). Mechanical and dynamic mechanical tests were carried out to assess the impact of the biofibre on the composite material. Mechanical testing revealed significant enhancements in tensile strength of 29.2 MPa, particularly at a biofibre volume fraction of 12% and the composite with the highest impact and flexural strengths measured at 2621 J/m2 and 41.1 MPa, respectively for the 16%v/v fibre loading. Dynamic mechanical analysis (DMA) results demonstrated improved viscoelastic properties attributed to the presence of the biofibre. Scanning electron microscopy (SEM) examination of tensile tested samples provided insights into interfacial bonding and filler dispersion within the composite matrix. Overall, the findings highlight the potential of casuarina leaf biofibre to enhance specific mechanical properties and viscoelastic behaviour of epoxy casuarina composites. Optimizing the biofibre volume fraction offers possibility to tailor composite properties for specific application requirements. This research advances the development of bio-based composite materials, contributing valuable insights for the creation of sustainable and high-performance engineering materials.

Research on the Mechanical Response and Constitutive Model of 18Ni300 Manufactured by SLM with Different Build Directions.

Metals manufactured by selective laser melting (SLM) with different directions exhibit different mechanical properties. This study conducted dynamic and static mechanical tests using a universal testing machine and split-Hopkinson bar (SHPB). The mechanical properties of 18Ni300 with 0° and 90° build directions manufactured by SLM were compared, and the micro-structure properties of the two build directions were analysed by metallographic tests. The Johnson-Cook (J-C) constitutive model was fitted according to the experimental results, and the obtained constitutive parameters were verified by numerical simulations. The results revealed that the constitutive model could predict the mechanical properties of 18Ni300 in a dynamic state. The build direction had little influence on the mechanical properties in a static state, but there was a significant difference in the dynamic state. The difference in the dynamic compressive yield strength of the 18Ni300 material manufactured by SLM with two build directions was 9.8%. The SLM process can be improved to produce 18Ni300 with uniform mechanical properties by studying the reasons for this difference.

Synergic effects of silica aerogel (SA) particles on tensile behavior of cryo-conditioned epoxy: The role of particle morphology and mixing sequence

Cryogenic conditions are of crucial importance for gas storage tanks to provide increased storage density, reduced pressure requirements and minimized energy losses. Incorporation of silica aerogel (SA) particles as a nanostructured material with extremely low density and exceptional thermal insulating properties into epoxy matrices has the potential to facilitate the progress of high performance nanocomposite coatings for advanced cryogenic applications. The objective of this study is therefore to investigate the impacts of particle size, particle content, milling method and mixing sequence on toughness of the cryo-conditioned epoxy coatings. SA particles of varying size (50 μm to 300 μm) were prepared using two different techniques (planetary ball milling vs. 2-blade grinding). Nanocomposite samples were prepared using two distinct mixing sequences, i.e., adding particles (in 0, 0.5, 1 and 1.5%wt.) to epoxy followed by mixing with hardener or adding particles to epoxy/hardener (with 3 or 15 min delay). The nanocomposite samples were subjected to different cryogenic conditions (single 3-h immersion in liquid nitrogen vs. three consecutive 1-h immersions). Mechanical properties of the samples were evaluated by conducting fractography, dynamic mechanical thermal analysis (DMTA) and tensile tests. Large SA particles settled towards the bottom of nanocomposite and resulted in loss of mechanical properties at cryo-conditions. Mixing 1 wt% of optimized SA particles with epoxy/hardener system led to an enhanced tensile strength (26 %), stiffness (3 %) and toughness (71 %) by providing uniform cross-linking reactions and mitigating thermal shock effects at cryo-conditions. Toughening mechanisms included crack deflection, crack pinning, crack arrest and crack branching.

Investigation of mechanical properties of compatibilized polyvinyl chloride/polylactic acid nanocomposites

AbstractPolymer alloying is particularly important due to the possibility of choosing a wide range of materials and the ability to design a product with desired properties. In case of incompatibility between the components, the resulting alloy cannot meet the set of desired properties and shows poor performance. In this research, alloys of polyvinyl chloride and polylactic acid were prepared in an internal mixer and nanoclay and maleic anhydride‐grafted styrene‐ethylene/butylene‐styrene (SEBS‐g‐MAH) compatibilizer were used to improve the properties. In order to investigate the morphology and phase distribution of polylactic acid, scanning electron microscope images were taken. Tensile and dynamic mechanical thermal analysis tests were performed to evaluate the properties of the samples. The scanning electron microscope test images show the improvement of system uniformity by adding compatibilizer to the alloy. Adding nanoclay to the alloy increased the storage modulus and uniformity of the system. An increase in glass transition temperature and storage modulus was observed in the samples containing compatibilizer, and the uniformity of the system was also improved. The tensile test results showed that by adding nanoclay up to 3 % by weight, the tensile strength and Young′s modulus increase. Addition of compatibilizer up to 5 % by weight increased the physical and mechanical properties.

Correlation between AFM characterizations and dynamic mechanical testing to assess the ductile-to-brittle transition during ABS photodegradation

The extensive use of Acrylonitrile Butadiene Styrene (ABS) raises challenges due to its vulnerability to oxidative degradation, primarily impacting its mechanical behavior. Photodegradation appears to be the pivotal driver in this degradation process. The main aim of the present study is to provide a comprehensive approach to the underlying mechanisms governing the transition from ductile to brittle behavior in ABS after exposure to UV-induced photodegradation. This study thus focuses on the multiphase nature of ABS, wherein polybutadiene (PB) nodules are dispersed within a matrix of styrene-acrylonitrile. Dynamic mechanical tensile tests have been employed to highlight aged layer mechanical impact by blocking the dissipative response of the matrix and applying a homogenous stress field, while atomic force microscopy (AFM) has been used to characterize the local mechanical properties of ABS finely. The evolution of global mechanical properties has been correlated with changes in microstructural behavior. One of the main contributions of the present work is the correlation between the formation of brittle layers with the brittle state of aged ABS. Mechanical testing using dynamical tensile test revealed a critical aging time marking the transition from a ductile to a brittle state of the 450 µm thick samples. Chemical analysis using infrared spectroscopy revealed evolutions in the material composition, especially in the carbonyl, hydroxyl, and PB unsaturation groups. Distinct thin oxidized layers on each exposed surface were observed using optical microscopy. Finally, AFM analysis on the exposed surface shows the stiffening of PB nodules, indicating the formation of brittle thin layers due to oxidation causing an apparent fragile behavior of ABS.

FLAx‐REinforced Aluminum (FLARE): A Bio‐Based Fiber Metal Laminate Alternative Combining Impact Resistance and Vibration Damping

Fiber metal laminates (FMLs) have mainly been used in aerospace applications with synthetic fibers. To improve their environmental credentials and address issues regarding the end‐of‐life of these materials, a shift to FMLs based on natural fibers can be a promising course of action. However, regarding them as conventional FMLs overlook some of the unique benefits of natural fibers. Therefore, this study pioneers the examination of FLAx‐REinforced aluminum (FLARE) for its combined impact resistance and vibration damping. Dynamic mechanical analysis and vibration beam tests demonstrate that the metallic layer predominantly influences the damping behavior of FLARE. The loss factor notably decreases with aluminum addition (by 80% compared to the flax composite), approximated via an inverse mixture rule. Low‐velocity impact tests highlight the role of aluminum layers in energy absorption and the composite strength as a critical factor in impact resistance. FLARE exhibits 25% less specific energy absorption compared to its glass fiber counterpart. A quasi‐static analytical model suggests the potential of FLARE for practical applications. With its balance of properties and considering its potential advantages at end‐of‐life, allowing recycling of aluminum, and its expected lower carbon footprint, FLARE renders potential beyond the aerospace sector, e.g., in other forms of transportation.

In Vitro Assessment of a New Block Design for Implant Crowns with Functional Gradient Fabricated with Resin Composite and Zirconia Insert.

This study aims to evaluate and compare the mechanical resistance, fatigue behavior and fracture behavior of different CAD/CAM materials for implant crowns. Eighty-eight implant crowns cemented-screwed with four sample groups: two monolithic G1 Zirconia (control) and G3 composite and two bi-layered G2 customized zirconia/composite and G4 prefabricated zirconia/composite. All static and dynamic mechanical tests were conducted at 37 °C under wet conditions. The fractographic evaluation of deformed and/or fractured samples was evaluated via electron microscopy. Statistical analysis was conducted using Wallis tests, which were performed depending on the variables, with a confidence interval of 95%, (p < 0.05). The Maximum Fracture Strength values displayed by the four groups of samples showed no statistically significant differences. The crown-abutment material combination influenced the failure mode of the restoration, transitioning from a fatigue fracture type located at the abutment-analog connection for monolithic materials (G1 and G3) to a brittle fracture located in the crown for bi-layered materials (G2 and G4). The use of layered crown materials with functional gradients appears to protect the crown/abutment connection area by partially absorbing the applied mechanical loads. This prevents catastrophic mechanical failures, avoiding long chairside time to solve these kinds of complications.

Reconsidering Museums’ Climate and Seasonal Adjustment for Vulnerable Artifacts

ABSTRACT The paper provides new experimental evidence for vulnerable artifacts on the dependence of failure strain on the loading rate corresponding to typical environmental loads lasting between hours and months. Animal glue-based ground was chosen for this study as an easily available, hygroscopic and brittle material as well as due to its abundance in collections and its relevance when discussing the risk of mechanical damage to objects. Gesso specimens were tested using dynamic mechanical analysis and tensile testing at different frequencies, under a variety of loading rates and temperatures. The time-temperature superposition principle was used to predict the material response to slow deformations (lasting hours to months) that are otherwise inaccessible on laboratory timescales. The results demonstrate that brittle materials such as animal glue-based grounds do not benefit from longer cycles of applied loads as failure strain is not time-dependent within the investigated timescale.

Development of physiologically relevant synthetic thrombus for use in visual analysis of in vitro mechanical thrombectomy device testing

BackgroundIschemic stroke is a leading cause of death and significant long-term disability worldwide. Mechanical thrombectomy is emerging as a standard treatment for eligible patients. As clinical implementation of stent retrieval...