Distilled Water Solution Research Articles

Methanolic Extract of Ricinus Communis ameliorated cardiovascular dysfunction in dichlorvos-exposed rats.

Cardiovascular diseases are the leading causes of death globally resulting in 17-19 million death every year. The search for an effective medicine to manage cardiovascular disorder without any side effect has led to the use of traditional based medicine. 75% of the world's population has been reported to depend on traditional medicine as their basic form of health care and this has resulted to the use of herbal medicine in the treatment and management of metabolic diseases. The study evaluated the effect of methanolic extract of Ricinus communis on DDVP-induced cardiotoxicity in male Wistar rats. Thirty-two (32) male Wistar rats were randomly divided into four groups of eight (8) rats each. Group A served as control rats, received 10mL/Kg of dimethyl sulfoxide (DMSO) and distilled water solution (vehicle) for six weeks. Group B served as DDVP-induced rats and were exposed to DDVP (15 minutes daily) for 3 weeks without any treatment. Group C rats received DDVP as in group B and then administered 300mg/kg of R. communis extract for 42days. While Group D rats were administered 300mg/kg of R. communis extract daily, for 6 weeks in addition to normal feed and water. Exposure to DDVP caused significant cardiac dysfunction evidence by alteration in cardiovascular variables and electrocardiac function, compromised lipid profile and reduced antioxidant enzymes. However, treatment with methanolic extract of Ricinus communis improved antioxidant defense system, attenuate hemodynamic impairment and left ventricular dysfunction, as well as inhibit lipid peroxidation and prevent hyperlipidemia in rats. In addition, histopathology observation showed that Ricinus communis extract was able to regenerate the myocardial injury caused by exposure to dichlorvos. In conclusion, Ricinus communis exhibited cardioprotective properties and may be a potential remedy for cardiovascular diseases with low risk of toxicity.

Effectiveness of common household methods for removal of deltamethrin from vegetables

The importance of fresh fruits and vegetables in a healthy diet is well-established but concerns about pesticide residues have raised questions about their safety. This study investigated the effectiveness of common household methods for decontaminating the deltamethrin residue from tomato, okra, bitter gourd, cowpea, and green chili. The residue was estimated using gas-chromatography. The technique was validated through recovery, limit of detection (LoD), limit of quantitation (LoQ). Various processing techniques, including washing with tap water, salt water, vinegar, baking soda solutions, blanching and sonication were evaluated. The study found that these household methods significantly reduced deltamethrin residues in the tested vegetables. Boiling water washing (blanching), and sonication with distilled water and vinegar solution washing led to reductions of approximately 70-80% in deltamethrin residues. Additionally, warm water washing and blanching were effective, with reduction percentages ranging from 46 to 79%. The results varied depending on the type of vegetable and the method employed. However, overall these techniques showed promise in reducing the deltamethrin residues. Therefore, it is important to adopt multiple decontamination strategies such as thorough washing and cooking, to mitigate the potential risks associated with pesticide residues in vegetables.

Влияние воздействий поверхностно-активных веществ на прочность образцов мерзлых вскрышных горных пород угольных месторождений криолитозоны

The harsh climatic conditions of the cryolithic zone with its long winter period and presence of permafrost soils significantly slow down all technological processes in surface mining. The resistance of frozen rocks at coal mines to digging with mining equipment can be reduced by their preliminary softening with the use of surfactants. The paper discusses the softening effect of aqueous surfactant solutions on samples of frozen overburden rocks. The authors demonstrate that treatment of rocks with solutions of optimal composition and concentration decreases their strength, which makes it possible to enhance the efficiency of In-Pit Crushing and Conveying Systems based on the rotary mechanical shovel in combination with a conveyor as well as the use of continuous miners. Experimental data are presented on the strength properties of artificially made samples of overburden rocks from the Kangalassky coal deposit saturated with surfactant solutions of different concentrations. The authors point out that the highest decrease in the samples strength is achieved when using aqueous solution of aluminum chloride. The results of experiments carried out to establish the effects of distilled water (H2O) and NaCl solutions of different concentrations on the strength properties of fine-grained sandstones from the Elga coal deposit are presented, which confirm that at the temperature of -10°С the maximum reduction of up to 55% is achieved in the strength of the samples, and when the temperature decreases from -10°С to -20°С a slight increase is observed in the sample strength. The authors suggest that the use of surfactants will reduce the strength of the frozen overburden soils, thus making it possible to apply a blast-free mining technology.

Valorization of Aloe vera waste for the production of Ca and P-rich hydrochars

The production of gel from Aloe vera plants is an emerging industry, however the residual leaves are considered waste and are not utilized. The purpose of this work was to prepare hydrochars from Aloe vera leaves under different conditions, and determine the fate of macro- and micronutrients in the solid products, in view of developing a novel biofertilizer. In this framework, distilled water, citric acid and potassium hydroxide solutions were used as feedwaters and the experiments were performed at the temperatures of 180 and 220 °C and treatment times of 1 – 8 h. All obtained hydrochars had increased Ca and P contents compared to the feedstock, whereas the highest Ca and P concentration of 10.4% and 7382 mg kg−1, respectively, were achieved under alkaline conditions after 8 h of treatment. Citric acid promoted carbonization, achieving H/C = 1.11, O/C = 0.34 of the hydrochar obtained at 220 °C after 8 h of treatment. The use of KOH counterbalanced the production of acids from the degradation of the biomass, thus restricting the carbonization progress. The metals K, Fe, Cu and Mg showed high solubilization tendencies, however their concentrations on the hydrochars increased beyond the 4 h treatments due to precipitation and re-sorption phenomena. The N content in the hydrochars ranged between 0.56 – 1.12%, increasing with temperature and time due to the formation and precipitation of pyridine, pyrroline and pyrrolidine derivatives. Overall, due to the high ash content, low pH and increased Ca and P concentrations, the hydrochars may be suitable as substrates for the development of bio-fertilizers purposed for alkaline soils.

Effect of extraction solution on functional properties of extracted protein from Bombay locust (Patanga succincta Johannson, 1763)

Alternative sources of protein are gaining popularity since they require less natural resource input, but still provide a significant amount of protein as compared to traditional protein sources. Insect protein is one of the alternative protein types, and due to its nutritional benefits, research interest in Bombay locust (Patanga succincta) (BL) protein has grown. In the present work, we aimed to determine the protein content, yield, molecular weight profile, and functional properties such as protein solubility, emulsion, and foam properties of BL protein extracted using distilled water, salt (NaCl), or alkaline (NaOH) solution, at the concentrations of 0.5, 1.0, or 1.5%. The highest protein extraction yield was alkaline soluble protein (22 - 28%), which was followed by water (16%) and salt (11 - 13%) soluble proteins. The protein powder prepared by 0.5% alkaline extraction had the highest foam capacity (33.33%) and foam stability (12.50%) (p < 0.05), but the water soluble protein powder had the highest emulsion activity index (118.3 m2/g) and emulsion stability index (52.45 min) (p < 0.05). These results indicated that the type and concentration of solution could have an impact on the protein extraction yield, molecular weight profile, and functional characteristics.

Determination of Optimum Processing Condition of High Protein Laver Chip Using Air-Frying and Reaction Flavor Technologies.

This study aimed to develop a high-protein and gluten-free laver chip using air-frying and reaction flavor technologies via response surface methodology (RSM). The optimum processing condition (w/w) was determined with a batter composition of 20% dried laver, 21.3% hair tail surimi, and 58.7% rice flour. Additional ingredients included б-gluconolactone, NaHCO3, soybean oil, corn syrup, table salt, saccharin, and a mixture of distilled water and reaction flavor-inducing solution (RFIS). The laver pellet processed and dried (50 °C, 1-2 h) with air-frying (195 °C, 52.5 s) to process the laver chip. The values of brittleness and puffing ratio of the laver chip were 6.93 ± 0.33 N and 116.19 ± 0.48%, respectively, with an error within 10% of the predicted values of RSM. RFIS was prepared via RSM with the addition of precursor substances (w/v) of methionine 0.54%, threonine 3.30%, glycine 2.40%, glutamic acid 0.90%, and glucose 3% to distilled water and then heating reaction (121 °C, 90 min). The quantitatively descriptive analysis (QDA) of RFIS, baked potato-like and savory odor were 6.00 ± 0.78 and 4.00 ± 0.91, respectively, with an error within 10% of the predicted values. The laver chip exhibited high-protein (24.26 ± 0.10 g%) and low-calorie (371.56 kcal) contents.

Novel superabsorbent polymer composite embedded with sodium alginate and diatomite for excellent water absorbency, water retention capacity, and high thermal stability

The low water absorbency, poor thermal stability, and high cost of absorbent polymers remain significant challenges that need addressing to broaden their range of applications. To address these drawbacks of superabsorbents, a novel superabsorbent polymer composite (SAPc) SA-g-P(AA-co-AM)/MDE was developed using a simple aqueous polymerization method involving sodium alginate (SA), modified diatomite (MDE), acrylic acid (AA), and acrylamide (AM). The synthesized materials were systematically characterized using various techniques, including FT-IR, SEM, and XRD, to determine their chemical structure, morphology, and crystal structure. The water absorbency capacity (WAC) of SA-g-P(AA-co-AM)/MDE increased with increasing SA dosage, but it gradually declined once it exceeded 5 wt.%. The SAPc with the highest water absorbency was obtained when the SA content was 5 wt.% in both distilled water and NaCl solution. The absorption data of SA-g-P(AA-co-AM)/MDE fit well with the pseudo-first-order (PFO) kinetic model. The results of water retention capacity (WRC) demonstrated that the water-retaining time of the SAPc increased by 39.0 % compared to P(AA-co-AM). Additionally, thermal gravimetric analysis revealed that the introduction of MDE and SA enhanced the SAPc's thermal stability. Therefore, this study demonstrates that the introduction of SA and MDE can lead to SAPc with outstanding WAC, WRC, and thermal stability. These findings suggest that the SAPc prepared in this study could be a promising material for use in agriculture, industry, and sanitary goods.

Fractographic study of thermoplastic composites based on carbon fiber/PA6 conditioned in heated distilled water and saline solution and tested in tensile

Fractographic study of thermoplastic composites based on carbon fiber/PA6 conditioned in heated distilled water and saline solution and tested in tensile

Characterization of a water-based liquid scintillator for use in megavoltage radiotherapy beams

The measurement of the dose delivered in radiotherapy treatments is carried out using dosimeters that are often expensive to produce and sometimes toxic to humans and the environment, which leads to more complex and rigorous clinical manipulations. It is in this context that it is necessary to provide new types of scintillators that would no longer have these problems while having properties equivalent to those of human tissues. Thus, the following study presents the performance of a water-based liquid scintillator used at radiotherapy energies. The characteristics studied include the proportionality of the scintillation signal to the dose, the scintillation efficiency at two different energies as well as the identification of the Cherenkov portion of the signal for photon beams of 180 kVp, 6 MV as well as 18 MV. Spectral measurements of the scintillation solution and a solution of distilled water were acquired in order to isolate the contribution of the scintillation signal from the spectrum obtained, and then compared to a commercial scintillator, Ultima Gold. The signal exhibits a linear dose relationship with a correlation coefficient of 0.999 and lower scintillation efficiency than Ultima Gold.

Isolation and Identification of Flavonoid Compounds and Antibacterial Activity Test of the Canyere Badak Plant (Bridelia glauca Blume) (Phyllanthaceae)

Flavonoid compounds from the stem bark of the Canyere Badak plant (Bridelia glauca Blume) have been isolated. 2500 g of Canyere Badak plant stem bark was macerated by methanol, and the methanol extract dissolved in distilled water. The distilled water solution was extracted by partitioning with ethyl acetate repeatedly until negative to 5% FeCl3. The ethyl acetate extract was dissolved in methanol and extracted by partitioning with n-hexane until the n-hexane layer was transparent. The methanol extract was analyzed by thin layer chromatography and separated by column chromatography with a stationary phase of silica gel and a mobile phase of chloroform: methanol (90:10; 80:20; 70:30; 60:40) v/v. Fractions 148-174 were purified by preparative thin layer chromatography using benzene: acetone (80:20) v/v eluent to produce a brownish yellow paste of 10 mg at Rf value of 0,66 using chloroform: methanol (80:20) v/v as eluent. Based on the analysis of the UV-visible spectrophotometer, it had a wavelength (λ max) of 275 nm. The FT-IR spectrum shows the presence of OH, C=C aromatic, C=O ketones, C-H, C-O-C and C-O groups. The proton Nucleus Magnetic Resonance Spectrum (1H-NMR) indicates the presence of H-2’ & H-6’ protons, H-3’ & H-5’ protons and methoxy protons. Based on the data analysis and interpretation, the isolated compound was a flavonoid of the flavanones group. The antibacterial activity of total flavonoids was determined by agar disk diffusion against Staphylococcus aureus and Escherichia coli bacteria. The results showed that total flavonoids strongly inhibited the growth of Staphylococcus aureus and Escherichia coli bacteria with MIC (Minimum Inhibitory Concentration) value at a concentration of 100 mg/mL obtained a clear zone of 9.5 mm against Staphylococcus aureus bacteria and at a concentration of 100 mg/mL obtained a clear zone of 12.15 mm against Escherichia coli bacteria.

Effects of surface treatments of bioactive tricalcium silicate-based restorative material on the bond strength to resin composite

ObjectivesThis study aimed to enhance the bond strength between Biodentine™ (BD), a bioactive tricalcium silicate (C3S) based material, and resin composite through various surface treatments. MethodologyBD samples were immersed in either double distilled water or Hank's Balanced Salt Solution and analyzed using X-ray Diffraction (XRD). Shear bond strength (SBS) evaluations of BD were performed using Prime & Bond™ NT (PNT), Single Bond Universal (SBU), Xeno V (Xeno), and glass ionomer cement (GIC) following various etching durations (0 s/ 15 s/ 30 s/ 60 s with 37.5% phosphoric acid). Two primers, RelyX™ Ceramic Primer (RCP) and Monobond ™ Plus (MBP), were chosen to prime BD for SBS enhancement. Fractography and bonding interfaces were examined with energy dispersive X-ray spectroscopy (EDS)/ scanning electron microscopy (SEM) and Fourier-transform infrared spectroscopy (FTIR). ResultsXRD confirmed BD’s main compositions as C3S, Ca(OH)2, CaCO3 and ZrO2 after 14 days crystal maturation. Etched BD did not improve SBS. GIC exhibited the lowest SBS (p < 0.05) among all adhesives, regardless of the etching mode (all < 1 MPa). The highest SBS (17.5 ± 3.6 MPa, p < 0.05) was achieved when BD primed with MBP followed by SBU application. FTIR and EDS showed γ-MPTS and10-MDP within the MBP primer interacted with C3S and ZrO2 of BD, achieving enhanced SBS. Most specimens exhibited mixed or cohesive failure modes.SignificanceBD’s subpar mechanical properties and texture may contribute to its poor adhesion to resin composite. Pretreating BD with MBP primer, followed by SBU adhesive is recommended for improving bond strength.

An efficient separation for fluoride-ions from water supplies by ion precipitate flotation: Pilot scale study with generation of coagulative bubbles

Bubble surface modification is a promising technique that enables to increase the efficiency of a treatment that aims to remove a certain particle with lower consumption of chemical inputs. In this study, the so-called coagulative bubbles were generated from a mixed system consisting of amphoteric surfactant (Cocamidopropyl betaine, CAPB) and inorganic polymer coagulants (aluminum sulfate and calcium chloride) for the removal of fluoride ions present in groundwater destined for human supply. The critical micellar concentration (CMC) of CAPB was 0.26 mmol L−1. The coagulant bubbles (CB) were generated from pressurizing the coagulant solution in distilled water and applied continuously in a helical tubular reactor. The CB treatment method provided higher fluoride removal compared to conventional treatment with simple coagulant application. The CBs generated with Al made it possible to remove approximately 98 % of the initial amount of fluoride measured (3.5 mg L−1) with a dosage of 31 mg L−1 of Al; feed flow rate of 20 L min−1; pH 6 ± 0.5; and saturation pressure of 3 atm. This same operation, but without generation of CBs (regular atmospheric pressure), allowed the removal of 67 % of the initial fluoride concentration.

Agglomeration effect of nanoparticles on foam stability of nonionic surface-active liquid: experimental and density functional theory studies

Innovative applications of foam are the need of time which fundamentally depends on the stability of the foam. In the present research work, the static foam behavior of the nonionic surfactant Tween-20 in the presence and absence of Titanium dioxide nanoparticles (TiO2-NPs) was investigated. The role of TiO2-NPs on foaming power based on foam height and foamability was studied at different temperatures. At 29 ± 1 0C, maximum foam height for Tween 20 (5% surfactant solution in distilled water) without and with TiO2-NPs was increased from 45.60 to 60.30 cm exhibiting 32.25% increase. In view of studying foam stability, axial dye displacement rate (ADDR) test was performed without and with nanoparticles where TiO2-NPs resist liquid drainage. TiO2 -NPs and Tween-20 form intermolecular hydrogen bonding which helps to enhance the foam stability as revealed by the density functional theory (DFT) studies. However, TiO2 -NPs have tendency to agglomerate if zeta potential value is low that severely affect the foaming power and foamability.

FARKLI CAM İYONOMER SİMANLARIN RENK STABİLİTELERİ VE MİKROSERTLİKLERİ

Objective&#x0D; Glass ionomers are preferred in many different&#x0D; treatment procedures in dentistry due to their positive&#x0D; features. The aim of this study is to evaluate the&#x0D; color difference and microhardness values of various&#x0D; glass ionomer cement after storing them in different&#x0D; solutions.&#x0D; Material and Method&#x0D; A total of 120 samples were prepared, including 40 of&#x0D; each of the Equia Forte, AHfil Silver, and Ionofil glass&#x0D; ionomers. Each glass ionomer sample was stored in&#x0D; distilled water, cola, tea, and coffee solutions. Color&#x0D; and microhardness measurements of the specimens&#x0D; were performed before and after a week before it was&#x0D; immersed in solutions. The color measurements of the&#x0D; samples were evaluated with a spectrophotometer and&#x0D; microhardness values were evaluated with Vickers&#x0D; microhardness device. For color analysis, color&#x0D; changes (ΔE) were calculated by obtaining the values&#x0D; of L*, a*, and b* of the samples before and after a week&#x0D; after being immersed in solutions. The data obtained&#x0D; were evaluated by variance analysis (ANOVA) and&#x0D; Tukey’s test.&#x0D; Results&#x0D; Except for specimens stored in cola for AHfil Silver,&#x0D; microhardness values were increased for all materials&#x0D; immersed in test solutions. The highest color change&#x0D; was obtained in coffee for Equia Forte, in the samples&#x0D; immersed in cola for AHfil Silver and Ionophil (p

Study on the Characteristics of Pore Change in Tuff under the Frost and Salt Action Using High-Precision CT Scanning Equipment

Using high-precision CT scanning equipment, two series of tests on frost and salt weathering were conducted to investigate the characteristics of pore change in tuff. Experiments on frost and salt aging were performed with pieces of tuff from the same area of southeast China. One set of tuff samples was soaked in saturated sodium sulfate or magnesium sulfate solutions for 60 days. Another set of tuff samples were subjected to 60 freeze–thaw cycles after being submerged in saturated sodium sulfate or magnesium sulfate solutions for 48 h. Our study demonstrates that processes such as salt erosion and freeze–thaw affect the pore evolution of tuffs significantly. Tuff lost 1.56% of its mass after being submerged in magnesium sulfate solutions for 60 days, while tuff submerged in sodium sulfate solutions gained a negative 0.33% of its mass. After 60 freeze–thaw cycles, the mass loss of tuff samples immersed in sodium sulfate, magnesium sulfate, and distilled water solutions was 3.52%, 3.58%, and 3.82%, respectively. The average porosity of the magnesium sulfate and sodium sulfate test groups increased by 6.59% and 4.14%, respectively, when the number of days of salt erosion was extended from 10 to 60 days. The average porosity of tuff samples immersed in magnesium persulfate and sodium sulfate solutions increased by 2.25% and 2.18%, respectively, as the number of freeze–thaw cycles went from 10 to 60.

Closed loop liquid cooling of high-powered CPUs: A case study on cooling performance and energy optimization

This case study presents an experimental investigation of closed loop liquid cooling of CPUs. The cooling system implements a pumped liquid supplying a cold plate fixed to the emulated CPU heat source and a remote Air-Cooled Heat Exchanger (ACHE). The Hybrid Liquid-Air (HLA) system employs 25% v/v Arteco-Freecor with distilled water solution as the primary coolant, and air as the secondary coolant. The thermal-hydraulic performance of the system is characterized over a range of operating conditions, including CPU heat loads (12–72 W/cm2), water volumetric flow rates (0.5–8 L/min), and air velocities (1–3 m/s). In order to provide a performance frame of reference, evaluations were also conducted with a conventional air-based fan-fin CPU cooling system. The results indicate that the HLA system significantly outperforms the traditional air-cooled fan-fin system, with much lower CPU temperatures and feasible power levels exceeding 300 W. Additionally, the study highlights the importance of the liquid flow rate and fan speed on the overall cooling performance. Finally, an optimal combination of liquid and air flow rates is identified for minimum energy consumption. Overall, these findings support the conclusion that conventional air-cooling is reaching its theoretical limit and closed loop liquid cooling has the potential keep pace with the escalating power levels of modern CPUs. However, the additional energy cost of the cooling system should be carefully managed in order to maximize overall system Coefficient of Performance.

The experimental investigating in water-rock interaction to reduce the thermal cracking threshold temperature of organic-rich shale

Thermal stimulation has excellent potential for enhancing the productivity of organic-rich shale. However, this shale's high thermal cracking threshold temperature (Ttct) results in excessive energy consumption and stringent casing safety requirements. Thus, optimizing thermal stimulation technology and reducing the Ttct is critical for efficient oil and gas production. This study proposes a novel method for quantifying the Ttct by fitting the S-shaped characteristics of the curve using the Sweibull2 model and defining the temperature corresponding to the maximum first-order derivative as the threshold value. Furthermore, we investigate the feasibility of reducing the high Ttct via water-rock interactions. Our findings show that the average Ttct of the anhydrous shale rock samples was 574 ℃, which decreased significantly to 344 ℃ and 336 ℃ for those samples saturated with distilled water and KCl solution, respectively. Persulfate oxidation resulted in noticeable reductions in the shale's Ttct and led to sample deformation and the initiation of large-scale fractures at temperatures below 200 ℃. However, the Ttct did not decrease significantly after acidizing and averaged 545 ℃. In summary, by adjusting the salinity of the fracturing fluid and incorporating suitable additives to match the reservoir’s properties, the effectiveness of heat treatment can be significantly enhanced. These findings present potential opportunities for improving oil and gas recovery while simultaneously reducing the energy consumption associated with thermal stimulation.

Performance of Regenerated Activated Carbons on Pesticides Removal from the Aqueous Phase

Adsorbents presenting high adsorption capacity, fast adsorption rate, easy regeneration, and a good possibility for reusability are ideal for removing 4-chloro-2-methyl-phenoxyacetic acid (MCPA) or other pesticides from wastewater. Here, the effects of regeneration treatments on adsorption–desorption cycles are examined using two commercial activated carbons (ACs) (Merck and Norit 1240 X). MCPA adsorption was fast on Merck and Norit ACs in powder form (6 h) but on Norit AC, in granular form, adsorption was too slow, and the equilibrium time was reached only after 288 h. MCPA adsorption kinetic data were analyzed by applying pseudo-first-order, pseudo-second-order, and Weber–Morris models. The pseudo-second-order model fit better to all data, and the Weber–Morris representation allows confirming that on Norit 1240 X, in granular form, the pore diffusion was the limiting factor concerning the MCPA adsorption. Merck and Norit 1240 X (in powder and granular form) ACs loaded with MCPA were submitted to different regeneration process by washing with distilled water, ethanol, HNO3, and NaOH solutions and washed with NaOH solutions or ethanol followed by a thermal treatment. The ACs regenerated with ethanol performed well in the subsequent adsorption–desorption cycles. All ACs had more than 99% desorbed MCPA after the first cycle of washing with ethanol. The washing with NaOH solution was less efficient. The regeneration process, consisting of washing the sample with a solution of NaOH and subsequent heating at 573 K, was very effective. After this regeneration procedure, the amount of MCPA adsorbed on Norit 1240 X AC was even higher than the amount adsorbed in the first adsorption cycle. At present, washing methods for adsorbent regeneration are not used at an industrial level. However, research for environmentally friendly regeneration methods is necessary to achieve the objectives of the circular economy.

The Influence of Wet Granulation Parameters on the Compaction Behavior and Tablet Strength of a Hydralazine Powder Mixture.

The aim of this paper was to describe the influence of high-shear wet granulation process parameters on tablet tensile strength and compaction behavior of a powder mixture and granules containing hydralazine. The hydralazine powder mixture and eight types of granules were compacted into tablets and evaluated using the Heckel, Kawakita and Adams analyses. The granules were created using two types of granulation liquid (distilled water and aqueous solution of polyvinylpyrrolidone), at different impeller speeds (500 and 700 rpm) and with different wet massing times (without wet massing and for 2 min). Granulation resulted in improved compressibility, reduced dustiness and narrower particle-size distribution. A significant influence of wet massing time on parameters from the Kawakita and Adams analysis was found. Wet massing time had an equally significant effect on tablet tensile strength, regardless of the granulation liquid used. Granules formed with the same wet massing time showed the same trends in tabletability graphs. Tablets created using a single-tablet press (batch compaction) and an eccentric tablet press showed opposite values of tensile strength. Tablets from granules with a higher bulk density showed lower strength during batch compaction and, conversely, higher strength during eccentric tableting.

Лабораторная диагностика засухоустойчивости образцов суданской травы методом набухания семян в растворах осмотиков

The results of studies of the nature and intensity of swelling of seeds of Sudanese grass samples in hypertonic solutions of osmotics and distilled water in 2021-2023 made it possible to establish a significant effect of the genotype, conditions of the year and the duration of the experiment. The seeds of the studied samples were distinguished by different water absorption intensities during the experiment period. On average, over the years of research, a high intensity of the seed swelling process was established in the initial (in the 1-st and 2-nd hours – 47,9-55,6%) and the final period of the experiment (24 and 48 hours – 86,4-105,1%, respectively), with a significant slowdown in the increase in the mass of grains during the lag phase – 4-6 hours from the beginning of the experiment (62,6-67,9%). The most intense swelling was found in Sudanese grass seeds in a 2022 laboratory experiment: the average value for samples in the studied variants was 78,0%; in 2021 – 74,2%, in 2023 – 60,5%. Relatively drought-resistant under conditions of artificially simulated stress include varieties of Sudanese grass Allegoriya, Ambiciya, promising breeding lines – Faina, L-30/17, which are used in the selection of new varieties and hybrids with high adaptive potential, adapted to cultivation in arid regions of the Russian Federation. Keywords: DROUGHT RESISTANCE, SUDANESE GRASS, ARTIFICIALLY SIMULATED STRESS, SEED SWELLING