Solute Dispersion Research Articles

Experiments reveal effects of particle and pore-scale heterogeneity on thermal dispersion during porous media heat transport

The growing applications of heat transport in engineering and hydrogeology, including ground source heat pump systems and the assessment of water flow and sediment thermal properties, necessitate precise thermal dispersion modeling. Despite various factors like particle size, shape, and distribution impacting dispersion in porous media, a lack of experimental data and analysis has limited our grasp of the relationship between flow velocity and thermal dispersion. To address this gap, we conducted solute and heat tracer experiments using sands of different grain sizes, employing analytical models based on a universal power law relationship for dispersion. Additionally, we systematically compiled dispersion data from the scientific literature to assist in interpreting of the effects of particle size, shape, and pore-scale heterogeneity on dispersion. Our findings reveal that solute and thermal longitudinal dispersion align for high flow velocities in the dispersion-dominated flow regime (Pe > 5), where the velocity-dispersion relationship is linear. However, in the transition regime (advection approx. equal to diffusion, 0.1–0.3 < Pe < 5), the observed deviation from linearity (R2<0.9) is linked to increased pore-scale heterogeneity, particularly in smaller particle sizes. This study underscores the pivotal role of thermal dispersion and underscores the need for caution when estimating thermal dispersion based on solute dispersion, given the intricate nature of real-world conditions and the potential influence of factors such as grain size distribution and pore-scale heterogeneity in natural porous materials.

General solution for linear 2D anisotropic surface gravity water waves on uniform current

Measuring and modeling ocean waves is a routine task for oceanographers and marine engineers. Accounting for current effects on waves is less common; however, such effects can be non-trivial, particularly for strong currents. Recent research has also found that currents are increasing with global temperatures. Thus, accounting for currents is of potential importance to a growing subset of real-world environments. One significant impact of currents is their modification of dispersion. It is known that, in contrast to dispersion without current, wave–current dispersion is multivalued and anisotropic, meaning it varies with direction and can yield multiple solutions for the same frequency. Strictly speaking, a complete analysis ought to account for all dispersion solutions. This study presents a general wave field solution for linear steady-state two-dimensional surface gravity waves on current. In contrast to existing formulations, it accounts for the complete set of dispersion solutions. The multiple solutions correspond to linearly independent (same frequency) spatial modes with no analogy in models without current. To fully determine the complete temporal and spatial features of a wave field, one must determine the amplitudes of all spatial modes. This can be achieved through the solution of an inverse problem, provided one has sufficient initial conditions. The significance of accounting for all spatial modes is demonstrated through examples. It is shown that a single time-series measurement is insufficient for determining the spatial features of a monochromatic (single frequency) wave. Rather, additional spatial information must be introduced to render the problem well-posed. The theory and methodology presented can be used to improve wave models and measurements.

Electromigration effect of nano-Fe3O4 in concrete under chloride erosion environment

In order to improve the effectiveness of electro-migration repair technology, researchers have introduced new materials to address the adverse effects of electrochemical repair on concrete, such as interface softening in reinforced concrete. In this study, a dispersed solution of nano-Fe3O4 was selected as the anode electrolyte. Concrete specimens were subjected to electric treatment for repair, and the entry of nano particles into the concrete under the action of an external electric field was investigated. The microstructure and mechanical properties of the repaired concrete material were analyzed using techniques such as potentiodynamic polarization curve, chemical titration, scanning electron microscopy, energy spectrum analysis, mercury intrusion porosimetry, and pull-out test. The results showed that after 15 days of electrochemical nano-repair, the passivation film on the steel reinforcement was repaired, resulting in a 57 % reduction in corrosion rate and prevention of further chloride ingress, thus improving the corrosion resistance of the reinforcement. Furthermore, the electrochemical nano-repair did not affect the outward migration of chloride ions from the concrete, with a chloride removal efficiency as high as 72.6 %. When the treatment duration was 15 days and the current density was 3 A/m2, the bond strength exhibited the greatest improvement, with an increase of 99.15 %. Compared to electrochemical chloride removal, the electrochemical nano-repair reduced the porosity in the middle and inner layers by 17.8 % and 14.8 %, respectively. Microstructural analysis revealed that the electromigrated nano-Fe3O4 particles were uniformly dispersed within the concrete, replacing harmful byproducts and filling the pores.

Investigation of the Effect of Mutual Diffusion on Hydrodynamic Parameters under Fluid Displacement

Formation of stagnant zones in a reservoir is mainly determined by differences in the flow velocity of fluids in heterogeneous micro and macro porous media. Additional resistance forces to fluid flow, which are of a different nature, result in a decrease in flow velocity. Forces arising from the diffusion of fluids with different physical-chemical characteristics and acting in different directions are one such class of the above-mentioned drag forces. An increase in the degree of fluid mineralization is capable of causing changes in the flow of a continuous diffusion layer. The mathematical solution of the problems considered in the study was solved using the "Matlab" program using the Finite Difference Method. The paper presents the results of displacement studies in porous media under the assumption that the flow characteristics of displacing and displaced fluids can be controlled. Theoretical and experimental substantiations showing the effect of diffusion process in fluids on flow properties have been carried out in the displacement process. The theoretical solution and modelling of concentration change in flow of mutually soluble dispersed solutions were presented. The effect of diffusion on the flow velocity in the process of displacement of mutually soluble liquid mixtures has been evaluated.

Heavy atom-induced quenching of fluorescent organosilicon nanoparticles for iodide sensing and total antioxidant capacity assessment.

We present a novel approach for iodide sensing based on the heavy-atom effect to quench the green fluorescent emission of organosilicon nanoparticles (OSiNPs). The fluorescence of OSiNPs was significantly quenched (up to 97.4% quenching efficiency) in the presence of iodide ions (I-) through oxidation by hydrogen peroxide. Therefore, OSiNPs can serve as a fluorescent probe to detect I- with high selectivity and sensitivity. The highly selective response is attributed to the hydrophilic surface enabling good dispersion in aqueous solutions and the lipophilic core allowing the generated liposoluble I2 to approach and quench the fluorescence of OSiNPs. The linear working range for I- was from 0 to 50 μM, with a detection limit of 0.1 μM. We successfully applied this nanosensor to determine iodine content in edible salt. Furthermore, the fluorescent OSiNPs can be utilized for the determination of total antioxidant capacity (TAC). Antioxidants reduce I2 to I-, and the extent of quenching by the remaining I2 on the OSiNPs indicates the TAC level. The responses to ascorbic acid, pyrogallic acid, and glutathione were investigated, and the detection limit for ascorbic acid was as low as 0.03 μM. It was applied to the determination of TAC in ascorbic acid tablets and fruit juices, indicating the potential application of the OSiNP-based I2 sensing technique in the field of food analysis.

Effect of Carbon Nanotubes on Chloride Diffusion, Strength, and Microstructure of Ultra-High Performance Concrete.

This study delved into the integration of carbon nanotubes (CNTs) in Ultra-High Performance Concrete (UHPC), exploring aspects such as mechanical properties, microstructure analysis, accelerated chloride penetration, and life service prediction. A dispersed CNT solution (0.025 to 0.075 wt%) was employed, along with a superplasticizer, to ensure high flowability in the UHPC slurry. In addition, the combination of high-strength functional artificial lightweight aggregate (ALA) and micro hollow spheres (MHS) was utilized as a replacement for fine aggregate to not only reduce the weight of the concrete but also to increase its mechanical performance. Experimental findings unveiled that an increased concentration of CNT in CNT1 (0.025%) and CNT2 (0.05%) blends led to a marginal improvement in compressive strength compared to the control mix. Conversely, the CNT3 (0.075%) mixture exhibited a reduction in compressive strength with a rising CNT content as an admixture. SEM analysis depicted that the heightened concentration of CNTs as an admixture induced the formation of nanoscale bridges within the concrete matrix. Ponding test results indicated that, for all samples, the effective chloride transport coefficient remained below the standard limitation of 1.00 × 10-12 m2/s, signifying acceptable performance in the ponding test for all samples. The life service prediction outcomes affirmed that, across various environmental scenarios, CNT1 and CNT2 mixtures consistently demonstrated superior performance compared to all other mixtures.

Preparation and application method of CNTs dispersion solution for direct electroplating on circuit board holes

Abstract The utilization of carbon black dispersion solutions for the black hole method is common in the electronics industry due to their cost-effectiveness and stable performance. However, the slow electroplating speed caused by carbon black’s poor conductivity can impact industrial processes and time. This paper introduces a water-based dispersion solution of carbon nanotubes (CNTs) for the direct copper electroplating process on circuit board holes and its application method. The dispersion solution comprises “shortened” CNTs with a small aspect ratio, a dispersant, a pH adjuster, and other optimization agents. This black hole liquid functions as a conductive fluid with “shortened” CNTs as the conductive medium, exhibiting high dispersibility, strong through-hole capability, low resistance, and excellent adhesion. Its performance surpasses that of black hole liquids using single-carbon black as the conductive medium. The key advantage lies in avoiding the entanglement associated with conventional long aspect ratio CNTs, thereby enhancing the conductivity of the water-based dispersion solution. This facilitates the formation of a uniform conductive film through the electrostatic self-adsorption method, which is suitable for preparing a conductive film on circuit board hole walls before copper electroplating.

A PEDOT: PSS/GO fiber microelectrode fabricated by microfluidic spinning for dopamine detection in human serum and PC12 cells.

Rapid and accurate in situ determinationof dopamine is of great significance in the study of neurological diseases. In this work, poly (3,4-ethylenedioxythiophene): poly (styrenesulfonic acid) (PEDOT: PSS)/graphene oxide (GO) fibers were fabricated by an effective method based on microfluidic wet spinning technology. The composite microfibers with stratified and dense arrangement were continuously prepared by injecting PEDOT: PSS and GO dispersion solutions into a microfluidic chip. PEDOT: PSS/GO fiber microelectrodes with high electrochemical activity and enhanced electrochemical oxidation activity of dopamine were constructed by controlling the structure composition of the microfibers with varying flow rate. The fabricated fiber microelectrode had a low detection limit (4.56 nM) and wide detection range (0.01-8.0 µM) for dopamine detection with excellent stability, repeatability, and reproducibility. In addition, the PEDOT: PSS/GO fiber microelectrode prepared was successfully used for the detection of dopamine in human serum and PC12 cells. The strategy for the fabrication of multi-component fiber microelectrodes isa new and effective approach for monitoring the intercellular neurotransmitter dopamine and has highpotential as an implantable neural microelectrode.

Size prediction of drug-loaded Polymeric (PLGA) microparticles prepared by microfluidics

Drug-loaded poly (lactic-co-glycolic acid) (PLGA) microparticles with ex-act control over size and homogeneity were created using a glass microfluidic cross-junction droplet generator. A numerical simulation based on the volume-of-fluid (VOF) method is used to study the behavior of two immiscible fluids that are injected into the microdevice: hydrophobic drug and (PLGA) in dichloromethane (DCM) serving as the dispersed phase and aqueous solution of poly (vinyl alcohol) (PVA) as the continuous phase. The simulation predicts the created emulsion droplet size regulation by adjusting the phase's flow rate. In a procedure known as droplet shrinking, dichloromethane extraction, and evaporation took place to further transform the monodisperse emulsion into PLGA microparticles. A numerical relationship is also given for the variations in the volume of droplets during shrinkage. The numerical results were consistent with the experiments. To further illustrate this technique's ability to manufacture designed microspheres with the least amount of repeated experiments, as well as the importance of the droplet microfluidic approach in terms of regulating diameter and monodispersity, opioid antagonist naltrexone is loaded in PLGA microspheres. According to the findings, integrating a versatile microfluidic approach with numerical methodologies enables the development of more reliable and reproducible drug delivery systems.

One-step of ionic liquid-assisted stabilization and dispersion: Exfoliated graphene and its applications in stimuli-responsive conductive hydrogels based on chitosan

Conductive hydrogels, as novel flexible biosensors, have demonstrated significant potential in areas such as soft robotics, electronic devices, and wearable technology. Graphene is a promising conductive material, but its dispersibility in aqueous solutions exists difficulties. Here, we discover that untreated graphene, after exfoliation by different ionic liquids, can disperse well in aqueous solutions. We investigate the impact of four ionic liquids with varying alkyl chain lengths ([Bmim]Cl, [Omim]Cl, [Dmim]Cl, [Hmim]Cl) on the dispersibility of grapheme, and a dual physically cross-linked network hydrogel structure is designed using acrylamide (AM), acrylic acid (AA), methyl methacrylate octadecyl ester (SMA), ionic liquid@graphene (ILs@GN), and chitosan (CS). Notably, SMA, CS, AA and AM act as dynamic cross-linking points through hydrophobic interactions and hydrogen bonding, playing a crucial role in energy dissipation. The resulting hydrogel exhibits outstanding stretchability (2250 %), remarkable toughness (1.53 MJ/m3) in tensile deformation performance, high compressive strength (1.13 MPa), rapid electrical responsiveness (response time ∼ 50 ms), high electrical conductivity (12.11 mS/cm), and excellent strain sensing capability (GF = 12.31, strain = 1000 %). These advantages make our composite hydrogel demonstrate high stability in extensive deformations, offering repeatability in pressure and strain and making it a promising candidate for multifunctional sensors and flexible electrodes.

Preparation of Carbon Nanotube Dispersions in Solutions of Ethoxylated Fatty Alcohols for Modifying Gel Systems

Preparation of Carbon Nanotube Dispersions in Solutions of Ethoxylated Fatty Alcohols for Modifying Gel Systems

Dual-Site Biomacromolecule Doped Poly(3, 4-Ethylenedioxythiophene) for Bosting Both Anticoagulant and Electrochemical Performances.

Poly(3, 4-ethylenedioxythiophene) (PEDOT) as a new generation of intelligent conductive polymers, is attracting much attention in the field of tissue engineering. However, its water dispersibility, conductivity, and biocompatibility are incompatible, which limit its further development. In this work, biocompatible electrode material of PEDOT doped with sodium sulfonated alginate (SS) which contains two functional groups of sulfonic acid and carboxylic acid per repeat unit of the macromolecule. The as dual-site doping strategy simultaneously boosts anticoagulant and electrochemical performances, for example, good hydrophilicity (water contact angle of 59.40°), well dispersibility (dispersion solution unstratified in 30 days), high conductivity (4.45 S m-1), and enhanced anticoagulant property (extended activated partial thrombin time value of 59.0 s), forming an adjustable PEDOT: biomacromolecule interface; this fills the technical gap of implantable bioelectronics in terms of coagulation and thrombosis risk. At the same time, the assembled all-in-one supercapacitor with anticoagulant properties is prepared by PEDOT: sodium sulfonated alginate as electrode material and sodium alginate hydrogel as electrolyte layer. The dual-site doping strategy provides a new opinion for the design and optimization of functional conductive polymers and its applications in implantable energy storage fields.

Three-dimensional graphene with the decoration of elemental sulfur-based sulfur-nitrogen dots for CO2 capture

Using a mild hydrothermal process, elemental sulfur was directly used to develop uniformly decorated sulfur-nitrogen (NS) dots on three-dimensional (3D) graphene. UV-Visible spectroscopy confirmed that hydrophobic elemental sulfur complexed with the primary amine in polyethylenimine (PEI) solution to form a hydrophilic sulfur-amine complex, and the resulting solution served as a nitrogen (N) and sulfur (S) source while improving dispersibility in GO solution. Hydrothermal treatment of aqueous GO and PEI-sulfur solution produces NS co-doped 3D graphene foam, while x-ray diffraction (XRD) and Raman spectroscopy results reveal GO reduction to graphene, and thermal properties are determined using differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). X-ray photoelectron spectroscopy (XPS) confirms NS doping on graphene sheets in the foam structure, while scanning and transmission electron microscopy (SEM and TEM) revealed homogeneous dispersion of NS dots with an average size of 5 nm. The high dispersibility and compatibility of amine-sulfur in aqueous GO results in the formation of ultra-small, uniformly distributed NS dots on graphene layers, whereas the amount of S and N in PEI solution is easily controlled by adjusting the stoichiometric ratio. Furthermore, the textural properties of NSG-1 were determined, and the obtained BET surface area was 245 m2/g, while the pore volume and average pore size were 1.91 cm3/g and 31.1 nm, respectively. The developed NS-co-doped graphene exhibits a room-temperature adsorption capacity of 2.77 mmol/g at 1 bar, with faster kinetics and CO2/N2 capture selectivity of 16.45 and 9.19 at 0.1 and 1 bar, respectively.

Fabrication of Functional Coating Layer for Emerging Transparent Electrodes using Antimony Tin Oxide Nano-colloid

This study fabricated a functional coating layer for transparent electrodes using antimony tin oxide nanopowder. The wet grinding method was employed to create a stable dispersion solution of antimony tin oxide nanopowder with aminopropyl tri-methoxysilane and acetyl acetone as primary dispersing agents. Various concentrations of these dispersing agents were used to determine optimal conditions, followed by a gel reaction to form a stable solution. The primary objective was to provide a viable alternative to indium-based transparent electrodes, specifically indium tin oxide, by incorporating antimony oxide. This approach not only addresses limitations associated with indium, but also enhances mechanical properties. The methodology involves the utilization of antimony tin oxide nanopowder and various solvents including ethanol and aforementioned dispersing agents to create a stable antimony tin oxide sol through wet grinding. Effects of dispersant concentration and milling time on the secondary particle size of the antimony tin oxide sol were thoroughly evaluated. Furthermore, this study examined sheet resistance of resulting coating layers by conducting a comparative analysis between antimony tin oxide and indium tin oxide under similar conditions. Findings of this study meticulously detailed in subsequent sections of the manuscript provide valuable insights into optimizing the entire process, encompassing synthesis, coating, heat treatment, and the production of high-quality transparent conductive coatings. These techniques and outcomes can significantly contribute to the development of more sustainable and cost-effective alternatives to traditional indium-based transparent electrodes.

Wastewater irrigation beneath the water table: analytical model of crop contamination risks

Wastewater irrigation alleviates freshwater scarcity. However, conventional (near)surface irrigation techniques directly expose crops to contaminants. Irrigating wastewater into shallow phreatic zones to raise the water table enhances groundwater evapotranspiration, while using the vadose zone as a bioreactor that attenuates contaminants through dilution, adsorption, and biodegradation. Nevertheless, contaminants may spread across the groundwater, soil, and vegetation. In this study, we focus on the crop contamination risks, and derive a simple analytical model to estimate crop solute uptake. Although crops are not directly exposed to the irrigated wastewater, contaminants (and nutrients) may spread to the root zone. Results show that crop contamination is primarily determined by the root zone water balance, and by solute dispersion and biogeochemical reaction parameters. The model contributes towards identifying hydrogeologically and climatically suitable locations for phreatic zone wastewater irrigation, determining acceptable levels of irrigation water quality, and evaluating crop contamination hazards against the fertigative value of wastewater.

Study on the Characteristics and Mechanism of Shield Tunnel Mud Cake Disintegration in Complex Red-Bed Geology

The complex red-bed geology is primarily composed of iron-rich sedimentary rock layers with clay minerals as a major component. The soil water content exceeds 30%, and its high viscosity and water content lead to the easy formation of mud cake on the cutterhead, endangering the safety and progress of construction, which poses a significant challenge for tunnel boring machines (TBMs). The use of dispersants to eliminate mud cake is a common method in engineering projects. This paper presents an improved disintegration experiment instrument to study the disintegration characteristics of mud cake from the red-bed geology under different dispersant solutions, proposing a dispersant formulation suitable for the red-bed geology of the Haizhu Bay Tunnel project. The results indicate that mud cake samples exhibit a moderate disintegration effect in pure water. Furthermore, it has been observed that the disintegration effect decreases as the thickness of mud cake increases. Sodium silicate solution was not suitable for treating the red-bed geological mud cake, while sodium hexametaphosphate and oxalic acid solutions had a good promoting effect on the disintegration of red-bed geological mud cake. However, there was a threshold for the dispersant concentration; exceeding this threshold actually worsened the disintegration effect. Ultimately, the engineering application of a 10% oxalic acid solution, which proved effective in disintegrating the mud cake, significantly enhanced the excavation efficiency in the Haizhu Bay Tunnel project.

A General Synthesis Method for Covalent Organic Framework and Inorganic 2D Materials Hybrids.

Two-dimensional (2D) inorganic/organic hybrids provide a versatile platform for diverse applications, including electronic, catalysis, and energy storage devices. The recent surge in 2D covalent organic frameworks (COFs) has introduced an organic counterpart for the development of advanced 2D organic/inorganic hybrids with improved electronic coupling, charge separation, and carrier mobility. However, existing synthesis methods have primarily focused on few-layered film structures, which limits scalability for practical applications. Herein, we present a general synthesis approach for a range of COF/inorganic 2D material hybrids, utilizing 2D inorganic materials as both catalysts and inorganic building blocks. By leveraging the intrinsic Lewis acid sites on the inorganic 2D materials such as hexagonal boron nitride (hBN) and transition metal dichalcogenides, COFs with diverse functional groups and topologies can grow on the surface of inorganic 2D materials. The controlled 2D morphology and excellent solution dispersibility of the resulting hybrids allow for easy processing into films through vacuum filtration. As proof of concept, hBN/COF films were employed as filters for Rhodamine 6G removal under flow-through conditions, achieving a removal rate exceeding 93%. The present work provides a simple and versatile synthesis method for the scalable fabrication of COF/inorganic 2D hybrids, offering exciting opportunities for practical applications such as water treatment and energy storage.

Effect of an inclined magnetic field on dispersion of solute in a pulsatile flow through a channel of absorptive porous walls

The present investigation gives an insight to comprehend the complex mechanism of species transport through porous walls, which has applications for crude oil refining, oil reservoir engineering, and separation of metal from fluids. The paper analyzes the impact of an inclined magnetic field on mass transport phenomena of solute through an unsteady, viscous, incompressible, and electrically conducting fluid flowing between two parallel plates. Both plates are permeable, and the flow is driven by a periodic pressure gradient. At both channel walls, the first order boundary reaction is applied. The governing time depending advection and diffusion equation is solved numerically based on Aris's method of moments. To determine the axial mean concentration distribution of solute, the first four central moments are used in a Hermite polynomial representation. It is significant to note that the dispersion of tracer is more significant for the low frequencies rather than the high frequencies. The behavior of the dispersion process of the tracer is studied for various flow parameters such as the angle of inclination of the magnetic field (α), Hartmann number (M), absorption parameter (β), suction Reynolds number (R), injection Reynolds number (R′), Womersley number (ω), and dispersion time (t) for both purely oscillatory and combined flows. It is significant to note that with the increment of R, α, and M, the amplitude of the dispersion coefficient of the solute reduces. On the other hand, an opposite phenomenon is observed for R′. It is seen that the transport coefficient moves cyclically with a double frequency period for all values of R and R′. Also, it is found that the peak of the mean concentration distribution enhances with the increment of α and M because the flow velocity decreases.

Transient dispersion of reactive solute transport in electrokinetic microchannel flow

Motivated by emerging applications in bio-microfluidic devices, the present study rigorously examines the generalized Taylor–Gill hydrodynamic dispersion of a point source solute injected into a microchannel, influenced by a constant axial static electric field along the channel and charged surface with different wall potentials. The solute engages in a first-order irreversible chemical reaction at both the microchannel walls. By incorporating different wall potentials and absorptive coefficients at the lower and upper walls, the current transport model for electro-osmotic flows is extended to encompass a wider range of applications. The solute transport phenomenon is intricately modeled using the unsteady convective diffusion equation. Employing Gill's generalized dispersion model, a concentration decomposition technique, up to the third-order accuracy, we meticulously analyze the transport process. Furthermore, a comprehensive comparison between analytical outcomes and numerical simulations using the Brownian Dynamics method is undertaken, enhancing the robustness of the analytical approach. The scattering process is mainly analyzed with the help of exchange, convection, dispersion, and asymmetry coefficients, along with the mean concentration profile. The effect of initial solute release at various vertical locations in the microchannel is shown to exert a considerable impact on all the transport coefficients at initial times.

Study on Mudcake disintegration in clayey strata during shield tunneling: Effects of dispersants and bentonite slurry

While tunnel boring machines (TBMs) tunneling in clayey strata, the adhered excavated soil on the cutterhead and cutting tools tends to form mudcake after compaction and consolidation. Mudcake can obstruct the cutterhead openings and rendering the cutting tools ineffective, leads to a substantial reduction in advance rate. Dispersants are recognized as an effective method for the disintegration of mudcakes. A novel set of equipment, comprising a mudcake compression device and a mudcake disintegration apparatus, is developed for assessing mudcake disintegration properties. The results showed that mudcakes underwent a tripartite disintegration process in water, including an initial stage, a rapid disintegration stage, and a stable stage. In the initial stage, the mudcakes absorbed water before disintegration, resulting in marginal changes in the weight of the disintegrated mudcakes. In the rapid disintegration stage, the weight of the disintegrated mudcakes increased quickly. During the stable stage, the weight of the disintegrated mudcakes remained relatively constant. The submersion of mudcakes in a dispersant solution substantially increased the rate of disintegration. Greater dispersant concentration corresponded to an increase in the disintegration rate. No weight gain was observed in mudcakes during the initial disintegration stage. When mudcakes disintegrated in a bentonite slurry, the weight of the disintegrated mudcakes initially decreased and then stabilized. The weight of the disintegrated mudcakes turned negative, indicating an increase in the weight of mudcakes. This suggested that bentonite significantly hindered mudcake disintegration.