Direct Measurement Research Articles

Avalanches and Extreme Value Statistics of a Mesoscale Moving Contact Line.

We report direct atomic force microscopy measurements of pinning-depinning dynamics of a circular moving contact line (CL) over the rough surface of a micron-sized vertical hanging glass fiber, which intersects a liquid-air interface. The measured capillary force acting on the CL exhibits sawtoothlike fluctuations, with a linear accumulation of force of slope k (stick) followed by a sharp release of force δf, which is proportional to the CL slip length. From a thorough analysis of a large volume of the stick-slip events, we find that the local maximal force F_{c} needed for CL depinning follows the extreme value statistics and the measured δf follows the avalanche dynamics with a power law distribution in good agreement with the Alessandro-Beatrice-Bertotti-Montorsi (ABBM) model. The experiment provides an accurate statistical description of the CL dynamics at mesoscale, which has important implications to a common class of problems involving stick-slip motion in a random defect or roughness landscape.

Hydrodynamic expansion and plume splitting of the ultrafast laser-induced plasma during ablation of multi-element metallic materials under atmospheric condition

In this study, the hydrodynamic expansion and splitting effect of ultrafast laser-induced plasma plume for multi-element alloys were studied. A fully coupled hydrodynamic model for femtosecond laser ablation of multi-element alloys was presented to study the ambipolar electric field during the plume expansion process. The model utilized a level-set equation to capture the interface between the condensed phase and the gaseous phase and accounted for the reaction between different species. A time-gate direct fluorescence measurement was conducted for the target material of brass, a Cu–Zn alloy, to validate the simulation results. The simulation results showed good agreement with the experimental results and were able to predict the plume-splitting effect. The ambipolar electric field induced by charged particle distribution difference was studied in detail. It was found that the ambipolar electric field was the dominant cause for the acceleration of ions, which yielded plume splitting during the expansion process. The fully coupled HD model was further used to explore the effect of the beam spot size, laser fluence, and the pulse width on plasma plume splitting.

Prospective, randomized, clinical trial on the effects of laparoscopic insufflation pressures on portal pressures in dogs.

The adverse effects of intra-abdominal pressure from capnoperitoneum on cardiovascular and pulmonary systems have been well documented, but the effects on portal pressures in dogs with various insufflation pressures is poorly defined. The aim of the present study was to measure the effect of a range of insufflation pressures on the portal pressure, using direct pressure measurements in patients undergoing laparoscopy. Clinical randomized prospective study. Nine client-owned dogs undergoing routine laparoscopy. Two rounds of direct portal pressure assessments were performed, at insufflation pressures of 0, 6, 10, and 14 mmHg in a predetermined randomized sequence. The data were analyzed for effects of insufflation pressure, hemodynamic alterations, and round. A best-fit exponential model of the relationship between portal pressure and insufflation pressure was created. Portal pressure increased by 38% at 6 mmHg, 95% at 10 mmHg, and 175% at 14 mmHg compared to baseline. Portal pressure increased at an average rate of 7.45% per mmHg of insufflation pressure. Effects of weight, weight/insufflation pressure interaction, and round of insufflation were not statistically significant. No systemic hemodynamic adverse events were observed. Portal pressure increased as insufflation pressure increased. There was no clinically significant difference in baseline portal pressure between rounds of insufflation. This exponential model of portal pressure supports the use of the minimum insufflation pressure to allow visualization during laparoscopy. The return of portal pressure to baseline following desufflation supports the comparison of portal pressure measurements before and after laparoscopic shunt attenuation.

Computational and experimental analyses of pressure drop in curved tube structural sections of Coriolis mass flow metre for laminar flow region

ABSTRACT This research presents a comprehensive investigation into the computational and experimental aspects of pressure drop phenomena within the curved tube structures. Mass flow measurement holds critical significance in process industries to mitigate inaccuracies arising from fluid property variations. The CMFM stands as a reliable instrument for direct measurement; however, its performance has exhibited discrepancies, recording lower fluid flow magnitudes than actual values in laminar flow conditions. This anomaly is suspected to be attributable to a secondary force generated within the sensor's curved tube structure. This study seeks to elucidate this phenomenon by assessing the pressure drop resulting from the secondary flow in four distinct curved tube configurations: U, Omega, Delta, and Diamond shapes under steady-state conditions. The paper underscores the pressure drop characteristics inherent in each tube structure configuration, revealing that Basic U and Omega shaped tube structures exhibit the least pressure drop.

Quantifying free energies through local composition fluctuations in binary solid solutions: A proof-of-concept study using atomistic embedded-atom simulations

While thermodynamic fluctuation theory has been extensively utilized in liquids for decades to obtain direct thermodynamic information, such as Gibbs free energies, from local composition fluctuations, this study presents an extension of the theory for its application in solids. It is demonstrated that composition fluctuations in solids are influenced by an additional elastic work term, which is specific to solids and encompasses liquids as a special case. To verify the extended fluctuation model, atomistic simulations were conducted on an exemplary Cu–Ni embedded-atom system. Monte Carlo simulations were performed in the semi-grandcanonical ensemble at a fixed temperature, covering the entire composition range. Composition fluctuations within a subvolume were monitored over time and statistically analyzed in terms of the variance. The atomistic results exhibit perfect agreement with the predictions derived from the extended model. This methodology has primarily been developed for the analysis of experimental atom probe tomography data, which provides three-dimensional chemical information with sub-nanometer precision. This technique enables the direct measurement of local composition fluctuations, facilitating the extraction of thermodynamic information from any allowed temperature–composition pair in the phase diagram.

Nitrous oxide abuse direct measurement for diagnosis and follow-up: update on kinetics and impact on metabolic pathways.

Recreational use of nitrous oxide (N2O) has become a major health issue worldwide, with a high number of clinical events, especially in neurology and cardiology. It is essential to be able to detect and monitor N2O abuse to provide effective care and follow-up to these patients. Current recommendations for detecting N2O in cases of recreational misuse and consumption markers are lacking. We aimed to update current knowledge through a review of the literature on N2O measurement and kinetics. We reviewed the outcomes of experiments, whether in preclinical models (in vitro or in vivo), or in humans, with the aim to identify biomarkers of intoxication as well as biomarkers of clinical severity, for laboratory use. Because N2O is eliminated 5 min after inhalation, measuring it in exhaled air is of no value. Many studies have found that urine and blood matrices concentrations are connected to ambient concentrations, but there is no similar data for direct exposure. There have been no studies on N2O measurement in direct consumers. Currently, patients actively abusing N2O are monitored using effect biomarkers (biomarkers related to the effects of N2O on metabolism), such as vitamin B12, homocysteine and methylmalonic acid.

Hydrodynamically‐Driven Deposition of Mud in River Systems

AbstractThe riverine transport and deposition of mud is the primary agent of landscape construction and evolution in many fluvial and coastal environments. Previous efforts exploring this process have raised uncertainty regarding the effects of hydrodynamic and chemical controls on the transport and deposition of mud, and thus the constructions of muddy coastal and upstream environments. As such, direct measurements are necessary to constrain the deposition of mud by river systems. Here, we combine laboratory evidence and a field investigation in the Mississippi River delta to explore the controls on the riverine transport and deposition of mud. We show that the flocculation of mud, with floc diameters greater than 10 μm, in freshwater is a ubiquitous phenomenon, causing the sedimentation of mud to be driven by changes in local hydrodynamics, and thus providing an explanation for how river systems construct landscapes through the deposition of mud in both coastal and upstream environments.

Energy conservation by collective movement in schooling fish

Many animals moving through fluids exhibit highly coordinated group movement that is thought to reduce the cost of locomotion. However, direct energetic measurements demonstrating the energy-saving benefits of fluid-mediated collective movements remain elusive. By characterizing both aerobic and anaerobic metabolic energy contributions in schools of giant danio (Devario aequipinnatus), we discovered that fish schools have a concave upward shaped metabolism–speed curve, with a minimum metabolic cost at ~1 body length s-1. We demonstrate that fish schools reduce total energy expenditure (TEE) per tail beat by up to 56% compared to solitary fish. When reaching their maximum sustained swimming speed, fish swimming in schools had a 44% higher maximum aerobic performance and used 65% less non-aerobic energy compared to solitary individuals, which lowered the TEE and total cost of transport by up to 53%, near the lowest recorded for any aquatic organism. Fish in schools also recovered from exercise 43% faster than solitary fish. The non-aerobic energetic savings that occur when fish in schools actively swim at high speed can considerably improve both peak and repeated performance which is likely to be beneficial for evading predators. These energetic savings may underlie the prevalence of coordinated group locomotion in fishes.

Energy conservation by collective movement in schooling fish.

Many animals moving through fluids exhibit highly coordinated group movement that is thought to reduce the cost of locomotion. However, direct energetic measurements demonstrating the energy-saving benefits of fluid-mediated collective movements remain elusive. By characterizing both aerobic and anaerobic metabolic energy contributions in schools of giant danio (Devario aequipinnatus), we discovered that fish schools have a concave upward shaped metabolism-speed curve, with a minimum metabolic cost at ~1 body length s-1. We demonstrate that fish schools reduce total energy expenditure (TEE) per tail beat by up to 56% compared to solitary fish. When reaching their maximum sustained swimming speed, fish swimming in schools had a 44% higher maximum aerobic performance and used 65% less non-aerobic energy compared to solitary individuals, which lowered the TEE and total cost of transport by up to 53%, near the lowest recorded for any aquatic organism. Fish in schools also recovered from exercise 43% faster than solitary fish. The non-aerobic energetic savings that occur when fish in schools actively swim at high speed can considerably improve both peak and repeated performance which is likely to be beneficial for evading predators. These energetic savings may underlie the prevalence of coordinated group locomotion in fishes.

Electrocaloric effect near room temperature in lead-free Aurivillius phase Sr2Bi4Ti5O18 upon La and Nb codoping

La and Nb codoping of ferroelectric five-layer Aurivillius phase Sr2Bi4Ti5O18 (TC ∼ 560 K), induces compositional disorder and diffuse relaxor transitions at much lower temperatures than the parent compound, while preserving the orthorhombic structure. For moderate La and Nb concentrations, the ferroelectric properties are enhanced in the vicinity of room temperature, and so is the electrocaloric effect as measured directly with a homemade quasi-adiabatic calorimeter. The adiabatic temperature change reaches, e.g., in Sr2Bi3.44La0.5Ti4.8Nb0.2O18, ΔT ⁓ 0.3 K at 355 K with a temperature span ⁓ 15 K, under ΔE = 37 kV/cm. Besides, a large field dispersion of the electrocaloric effect is found, ascribed to field-induced transitions from short-range-ordered relaxor to long-range-ordered ferroelectric states. Indirect estimations of the electrocaloric effect from electric polarization data are not able to quantitatively predict the direct results and emphasize the need of applying direct measurement methods, especially for relaxor ferroelectrics.

Post-process updating of model parameters to approximate thermal errors of machine tools operating in different configurations

Machine tool (MT) thermal errors induced by external and internal heat sources (e.g. changing environment, friction and power losses in MT components) are an important element in machined workpiece inaccuracies. In the past few decades, indirect software compensation techniques have been used to address thermal errors on account of their economic and ecological aspects. Many slightly different approaches are described in the literature. If thermal error models are properly identified based on experiments with sufficiently varying input parameters, they usually work within similar calibration and verification conditions. As the sensory equipment of machines increases, models can be adapted to regions with higher thermo-mechanical system nonlinearity and inhomogeneity through the introduction of deformation feedback from direct measurements into model structures. However, adaptive functionalities require discrete interruptions of the MT's work cycle, which threaten the integrity of the machined surface and complicate the model structure and thus also implementation and industrial deployment possibilities. In this research, a novel approach of automatic post-process adaptation suitable for repetitive manufacturing, which takes advantage of transfer functions (TF), is proposed for thermal error reduction. The method respects basic heat transfer mechanisms in the MT structure by combining linear parametric models, requires a minimum of additional gauges, and feedback from direct measurements is obtained only during technological pauses in the production process. Post-process adaptation is solved retrospectively by updating model parameters using the heuristic method of genetic algorithms (GA). First, the approach was tuned on a case study of a heavy-duty milling machine with a horizontal headstock for a configuration with an exchangeable spindle head and a configuration with a change in the position of the headstock in the workspace, both of which were different from the initial model's calibration range. Subsequently, the developed approach was applied to repeated production on a medium-sized milling centre. Another goal of the paper is to emphasize the need for quality input information for modelling efforts and the industrial applicability of scientific results.

Direct measurement of the effective properties of an additively manufactured titanium octet truss unit cell using high energy X-ray diffraction

Additively manufactured lattice structures offer a high specific strength-to-density ratio in comparison to conventional, fully dense parts. The small feature size and intricate geometry of lattice structures make it challenging to directly characterize their mechanical properties. This study presents direct measurement of the elastic mechanical properties of an additively manufactured titanium alloy octet truss unit cell. Strut stress and strain were measured using high-energy X-ray diffraction during quasi-static compressive loading. The crystallographic stress-strain relationship was converted into the stress-strain relationship of the octet truss lattice unit cell using the known symmetry of the struts. The sample studied herein was best fit by an orthorhombic linear elastic stress-strain relationship. This technique shows promise for studying additively manufactured lattice structures at length scales not previously reported.

Direct observation and measurement of circumlental space and its relation to anterior chamber angle characteristics in iridotomized phakic eyes with primary angle closure disease

Primary angle closure disease (PACD) is a major cause of blindness worldwide. It has a high prevalence in East Asia, especially in China, which leads to a higher incidence of blindness than open-angle glaucoma. The aim of this study was to directly observe the circumlental space (CLS) in laser peripheral iridotomized eyes with PACD and to determine whether this structure plays a role in the pathogenesis of PACD. Fifty eyes of 50 patients with PACD, who had received laser peripheral iridotomy performed with neodymium:yttrium–aluminum-garnet were recruited from glaucoma clinics from March 2021 to May 2022, including 17 primary angle closure suspect (PACS), 16 primary angle closure (PAC) and 17 primary angle closure glaucoma (PACG). They were classified into two groups based on whether the ciliary process and the crystalline lens equator were in contact using slit-lamp photograph: the attached group and the unattached group. The demographic, clinical characteristics and anterior segment parameters measured from ultrasound biomicroscopy were compared between the attached group and the unattached group. Thirty-three eyes were assigned to the attached group and 17 eyes belonged to the unattached group. In the unattached group, the mean CLS was 0.10 ± 0.07 mm. No significant differences were identified between the different diagnosis groups in age, sex, best-corrected visual acuity, intraocular pressure, white-to-white, axial length, central corneal thickness, anterior chamber depth, flat keratometry, steep keratometry or iridotomy diameter (p > 0.05). The unattached group had shorter trabecular-ciliary process distance (p = 0.021) and larger ciliary process area (p = 0.001) compared with the attached group. Small CLS and its potential effect (partial ciliary block) might be considered as one of the mechanisms of PACD.

Science with the ASTRI Mini-Array: From Experiment to Open Observatory

Although celestial sources emitting in the few tens of GeV up to a few TeV are being investigated by imaging atmospheric Čerenkov telescope arrays such as H.E.S.S., MAGIC, and VERITAS, at higher energies, up to PeV, more suitable instrumentation is required to detect ultra-high-energy photons, such as extensive air shower arrays, as HAWC, LHAASO, Tibet AS-γ. The Italian National Institute for Astrophysics has recently become the leader of an international project, the ASTRI Mini-Array, with the aim of installing and operating an array of nine dual-mirror Čerenkov telescopes at the Observatorio del Teide in Spain starting in 2025. The ASTRI Mini-Array is expected to span a wide range of energies (1–200 TeV), with a large field of view (about 10 degrees) and an angular and energy resolution of ∼3 arcmin and ∼10 %, respectively. The first four years of operations will be dedicated to the exploitation of Core Science, with a small and selected number of pointings with the goal of addressing some of the fundamental questions on the origin of cosmic rays, cosmology, and fundamental physics, the time-domain astrophysics and non γ-ray studies (e.g., stellar intensity interferometry and direct measurements of cosmic rays). Subsequently, four more years will be dedicated to Observatory Science, open to the scientific community through the submission of observational proposals selected on a competitive basis. In this paper, I will review the Core Science topics and provide examples of possible Observatory Science cases, taking into account the synergies with current and upcoming observational facilities.

Geomagnetic full vector fluctuation in Mexico over the last two centuries: Anomalous record between 1840 and 1940?

Study of the paleosecular variation of the Earth's Magnetic Field is an almost unique way to estimate the critical conditions at the core-mantle boundary. The continuous and quasi-periodic changes in the magnitude and directions (declination and inclination) could be detected from direct instrumental measurements or through the remanent magnetization of volcanic and sedimentary rocks. Burned archaeological artifacts are another reliable source of geomagnetic information. Besides the great efforts in Central and North America to retrieve the fine characteristics of the geomagnetic field during the last centuries, no homogeneous data distribution has still been achieved in Mexico and the surrounding areas. To improve the analysis of the geomagnetic full vector in Mexico, we compiled and updated available data for the last 200 years exclusively based on full geomagnetic vectors obtained from direct historical measurements, magnetic repeat stations, geomagnetic observatories and maritime exploratory campaigns. A relocation error procedure allowed the selection of 658 reliable data, discarding those belonging to the sites located in the most northern part of the analyzed area. The spectral analysis through the second derivatives reveals relatively fast fluctuations in both intensity and directions between 1890 and 1960. Moreover, a marked difference is observed between the Mexican record and global geomagnetic models between 1840 and 1940.

Quantifying salinity in heterogeneous coastal aquifers through ERT and IP: Insights from laboratory and field investigations

The lithological and stratigraphical heterogeneity of coastal aquifers has a great influence on saltwater intrusion (SI). This makes it difficult to predict SI pathways and their persistence in time. In this context, electrical resistivity tomography (ERT) and induced polarization (IP) methods are receiving increasing attention regarding the discrimination between saltwater-bearing and clayey sediments. To simplify the interpretation of ERT data, it is commonly assumed that the bulk conductivity mostly depends on the conductivity of pore-filling fluids, while surface conductivity is generally disregarded in the spatial and temporal variability of the aquifers, particularly, once the aquifer is affected by the presence of saltwater. Quantifying salinities based on a simplified petrophysical relationship can lead to misinterpretation in aquifers constituted by clay-rich sediments. In this study, we rely on co-located data from drilled boreholes to formulate petrophysical relationships between bulk and fluid conductivity for clay-bearing and clay-free sediments. First, the sedimentary samples from the drilled wells were classified according to their particle size distribution and analyzed in the lab using spectral IP in controlled salinity conditions to derive their formation factors, surface conductivity, and normalized chargeability. Second, the deduced thresholds are applied on the field to distinguish clay-bearing sediments from brackish sandy sediments. The results are validated with logging data and direct salinity measurements on water samples. We applied the approach along the Luy River catchment and found that the formation factors and surface conductivity of the different unconsolidated sedimentary classifications vary from 4.0 to 8.9 for coarse-grained sand and clay-bearing mixtures, while normalized chargeability above 1.0 mS.m−1 indicates the presence of clay. The clay-bearing sediments are mostly distributed in discontinuous small lenses. The assumption of homogenous geological media is therefore leading to overestimating SI in the heterogeneous clay-bearing aquifers.

Contribution of gas concentration and transfer velocity to CO2 flux variability in northern lakes

AbstractThe CO2 flux () from lakes to the atmosphere is a large component of the global carbon cycle and depends on the air–water CO2 concentration gradient (ΔCO2) and the gas transfer velocity (k). Both ΔCO2 and k can vary on multiple timescales and understanding their contributions to is important for explaining variability in fluxes and developing optimal sampling designs. We measured and ΔCO2 and derived k for one full ice‐free period in 18 lakes using floating chambers and estimated the contributions of ΔCO2 and k to variability. Generally, k contributed more than ΔCO2 to short‐term (1–9 d) variability. With increased temporal period, the contribution of k to variability decreased, and in some lakes resulted in ΔCO2 contributing more than k to variability over the full ice‐free period. Increased contribution of ΔCO2 to variability over time occurred across all lakes but was most apparent in large‐volume southern‐boreal lakes and in deeper (> 2 m) parts of lakes, whereas k was linked to variability in shallow waters. Accordingly, knowing the variability of both k and ΔCO2 over time and space is needed for accurate modeling of from these variables. We conclude that priority in assessments should be given to direct measurements of at multiple sites when possible, or otherwise from spatially distributed measurements of ΔCO2 combined with k‐models that incorporate spatial variability of lake thermal structure and meteorology.

SRF material research using muon spin rotation and beta-detected nuclear magnetic resonance

Muon spins precess in transverse magnetic fields and emit a positron preferentially in the spin direction at the instant of decay, enabling muon spin rotation (μSR) as a precise probe of local magnetic fields in matter. μSR has been used to characterize superconducting radio-frequency (SRF) materials since 2010. At TRIUMF, a beam of 4.2 MeV μ+ is implanted at a material-dependent depth of approximately 150 μm. A dedicated spectrometer was developed to measure the field of first vortex penetration and pinning strength in SRF materials in parallel magnetic fields of up to 300 mT. A low-energy beam available at PSI implants μ+ at variable depth in the London layer allowing for direct measurements of the London penetration depth from which other material parameters relevant for SRF applications, such as the lower critical field and the superheating field, can be calculated. Beta-detected nuclear magnetic resonance (β-NMR) is a technique similar to low-energy μSR using beams of low-energy β radioactive ions. With a recent upgrade, it is capable of detecting the penetration of parallel magnetic vortices, depth resolved with nanometer resolution at applied fields of up to 200 mT. In this paper, we review the impact and capabilities of these techniques for SRF research.

Thermal relaxation parameters estimation of non-Fourier heat transfer in laser-irradiated living tissue using the Levenberg-Marquardt algorithm

The present work is concerned with solving the inverse heat transfer problem (IHTP) to estimate the thermal relaxation parameters corresponding to the dual phase lag (DPL) model-based bio-heat transfer in laser-irradiated living tissue. This problem is divided into two parts: direct and inverse problems. The solution of the inverse problem has been obtained using the Levenberg–Marquardt algorithm. On the other hand, the solution to the direct problem is obtained by solving the DPL model-based bio-heat transfer equation (BHTE) with the transient radiative transfer equation (TRTE). So, the TRTE has been numerically solved by the modified discrete ordinate method (DOM) to find the intensity field in the living tissue subjected to short-pulsed laser radiation, and it acts as a heat source in the DPL model-based BHTE. So, the DPL model-based BHTE has been analytically solved by employing the finite integral transform technique to get the temperature variation inside the laser-irradiated living tissue. First, the computer code developed for estimating unknown thermal relaxation parameters using the Levenberg–Marquardt algorithm has been verified against the data given in the literature, and found good agreement between them. Then, the thermal response of laser-irradiated living tissue has been investigated. After that, the influence of sensor position on the sensitivity of the IHTP solution has been discussed. The impact of the total transient readings and the measurement error on estimating the unknown parameters have been investigated. The present study’s findings can significantly contribute to various parameter estimation problems where the conventional methods for direct measurements of parameters are impossible or very difficult. Furthermore, the current results may considerably impact the study of the thermic response of living tissue during laser-based photothermal therapy.

Longshore sediment transport rate in Formosa Bay, Rio de Janeiro State - Southeast Brazil

An approach involving data on wave-induced sediment transport estimates is essential for managing coastal environments. Numerical models are powerful tools to understand and investigate many processes responsible for longshore sediment transport (LST) in a systematic way, since direct measurement of LST is a difficult task. This paper presents estimates of longshore sediment transport through numerical modeling of wave-induced sediment dispersion patterns in the Formosa Bay, State of Rio de Janeiro - Southeast Brazil. The analysis was conducted using the computational package Coastal Modeling System/SMC-Brazil and mathematical formulations proposed by Cerc (1984). The results suggest average residual solid discharge (Qsravg) in the order of 131,442.745 m3/yr in northern sector, −151,908.32 m3/yr in central sector, and 71,987.69 m3/yr in southern sector of investigated area. In addition, it is important to highlight that minor variations in the wave incidence angle may cause changes in the longshore sediment drift, promoting the convergence and divergence zones throughout the investigated area. The results presented contribute to the advancement of knowledge on the topic addressed here and will be useful in future engineering projects related to beach nourishment and the management of coastal areas subject to erosion processes.