Differential Scanning Calorimetry (DSC) is a thermal analysis technique which has been used for more than three decades to measure the temperatures and heat flows associated with transitions in materials as a function of time. Other techniques, are Differential Thermal Analysis DTA and Conventional Calorimetry. There is great uncertainty in the values supplied by the manufacturers (because they are referred to pure substances) and the DSC should be used to get more accurate values. It will be analyzed the thermal storage capacity depending on temperature for several compound materials formed by some aggregates, mainly gypsum and phase change materials, in various proportions. The results have been compared with other building materials such as gypsum boards and brick layer. The suitability of the new construction material for thermal energy storage will be assessed in comparison with other materials traditionally used for this purpose.