An eco-rich renewable resource is a cellulose, and cellulosic fibers are a plentiful polymer of choice with a numerous industrial applications. Natural cellulosic fibers added to composites have the advantage of being biodegradable and environmentally safe materials. Desert cotton (Bui) botanically known as Aerva Tomentosa (family Amaranthaceous) is found in abundance in western Rajasthan, India. In this study, we assessed the extraction method of fibers and characterization of functional groups of ATFs(Aerva Tomentosa Fiber) by FTIR Spectroscopy of ATF (1) mercerized with 5% NaOH (alkaline treated) and un-mercerized ATF (0). In this sequence, the surface morphology of ATF (0) and ATF (1) were examined with a scanning electron microscope (SEM). Additionally, we performed the single fiber tensile strength test and the percentage elongation test in the cases of ATF (0) and ATF (1).Aerva Tomentosa (Bui) extracted cellulosic fiber bonds with Urea-Formaldehyde to form composites. Aerva Tomentosa various percentages of cellulosic fibers (7 wt%, 12 wt%, 17 wt%, 22 wt%, and 27 wt%) mixed in the composition to reinforce the synthesis of urea formaldehyde resin composites. Aerva Tomentosa Fiber Composite (ATFC)’s functional groups and bonding were analyzed using FTIR spectra. Both the mercerized fiber-loaded composite ATFC (1) and the un-mercerized fiber-loaded composite ATFC(0), ATFC's surface morphology were scanned using a scanning electron microscope (SEM).