Dentin Porcelain Research Articles

Evaluating the Impact of Oxidation Heat Treatment and Dual Opaquing Techniques on Enhancing Metal-Ceramic Bond Strength.

This research aims to assess the impact of oxidation heat treatment (OHT) and dual opaquing techniques on enhancing the bond strength between metal and ceramic. Eighty rectangular patterns with dimensions of 0.5x3x25 mm (according to ISO 9693-2012) were fabricated in a custom-made silicon mold by using auto-polymerized pattern resin material. These rectangular patterns were cast using base metal alloys. The samples were split into two primary groups: group A, subjected to OHT, and group B, without oxidation treatment. Each primary group was then split up into subgroups according to the application of single layers (group A1, B1)or double layers (group A2, B2) of opaque porcelain.After pre-surface treatment and Ceramco 3 paste opaque application, dentin porcelain (Ceramco 3) wasapplied to the mid-region of the samples, followed by firing to achieve a standardized thickness. Flexural strength determination was conducted via a three-point bend test performed on the universal testing machine (UTM) (Instron Corp., Model 2519-107, USA), adhering to ISO standard 9693. Post-testing failure types were analyzed by morphological assessment of debonding surfaces via a scanning electron microscope (SEM). The statistical analysis was performed with SPSS version 16, incorporating ANOVA for intergroup analysis and independent t-tests for intragroup comparisons. Group A2 exhibited the highest mean flexural bond strength (P<0.05) at 41.85 MPawhen compared to group A1 at 37.60 MPa, group B2 at 35.47 MPa, and group B1 with the least mean flexural bond strength at 30.41 MPa. SEMobservations revealed cohesive bond failure for groups A1, A2, and B2and adhesive bond failure for groupsB1. It is evident that OHT and opaquing technique are important factors in determining the bond strength of ceramo-metal restorations. When combined, these techniques greatly increase the overall success and durability of metal-ceramic restorations, underscoring their significance in contemporary dental prostheses.

Effect of different production techniques on the color of porcelain-fused-to-titanium restorations

In dentistry, the shade selection of the restoration affects the success of the restoration. For this reason, it may be decisive for clinicians to determine whether the difference in framework production influences color in metal-ceramic restorations. The study examined the effects of different framework production techniques used in porcelain-fused-to-titanium restorations on color changes. 45 square-shaped samples were manufactured using cast, milling, and laser-sintering techniques. Opaque and dentin porcelain were performed, and all samples were glazed. A spectrophotometer was used for color measurements. Before opaque application, after opaque application, and after porcelain + glaze application, it was obtained L*, a*, and b* values. Color differences (ΔE00) were calculated with the CIEDE2000 formula. ANOVA (Post Hoc: Bonferroni) and Shapiro Wilks (Normality) tests were used for statistical analysis (p < 0.05). At the different laboratory steps, the difference between cast&laser-sintered groups and between milled&laser-sintered groups was statistically significant (p < 0.05). Before and after opaque application, the differences in L*, a*, and b* values between cast, milled, and laser-sintered groups were statistically significant (p < 0.05). Different framework production methods influenced the color of porcelain-fused-to-titanium restorations.

Evaluation of the Bonding Shear Strength between Enamel and Dentin Feldspathic Porcelain and Two Different Monolithic Zirconia with Low and High Translucency.

The utilization of ceramics in the field of dentistry has seen a significant rise owing to their esthetic appeal and excellent functional properties. The use of ceramics in the field of dentistry has witnessed a notable surge, driven by their appealing esthetics and exceptional functional attributes. Zirconia, distinguished by its exceptional mechanical strength, plays a pivotal role in the fabrication of posterior crowns and bridges. Among zirconia variants, monolithic zirconia stands out, where the entire restoration is crafted from zirconia material. In parallel, feldspathic porcelain, chosen for its remarkable resemblance to natural tooth enamel, represents another significant ceramic type. This study aims to evaluate the shear bond strength (SBS) between two types of monolithic zirconia with two types of feldspathic porcelain. Forty-four monolithic zirconia veneered discs with feldspathic porcelain were subjected to SBS testing. The dimensions of the discs were 7 mm in diameter and 5 mm in height (3 mm of zirconia and 2 mm of porcelain). Subsequently, the specimens were subjected to a universal testing machine at a speed of 0.5 mm/min until failure occurred. The type of failure was examined using scanning electron microscopy. One-way analysis of variance (ANOVA), two-way ANOVA, Fisher's test, and multiple Tukey comparisons were used as statistical analyses. The highest SBS was achieved by the high-translucency monolithic zirconia with enamel porcelain group (18.81 ± 3.18 MPa) and the high-translucency monolithic zirconia with dentin porcelain group (17.89 ± 2.75 MPa), followed by the low-translucency monolithic zirconia with dentin porcelain group (15.04 ± 2.24 MPa) and the low-translucency monolithic zirconia with enamel porcelain group (14.33 ± 2.00 MPa), respectively. Additionally, the most common type of failure pattern observed was mixed, followed by adhesive failure. The translucency of the porcelain did not significantly affect SBS, while the type of monolithic zirconia used had a significant impact. Furthermore, there was no discernible relationship between the four groups in terms of the distribution of failure patterns.

Comparison of Color Accuracy between Natural Dentin Substrate and Three Dentin Porcelain Brands of Glass-Matrix Ceramic System (Digital Image Analysis)

Purpose: The purpose of this laboratory study was to differentiate the color of natural dentin (ND) and dentin porcelain (DP) by using three brands of Glass-Matrix Ceramic System (GMCS) by parametric CIE L*, a*, b* system. Materials and methods: An extracted human upper central incisor was prepared as a control group. Uniformly thick dentin specimen was taken from the middle coronal third of the labial half longitudinally. Twelve disks of GMCS dentin porcelain were fabricated according to manufactures' instructions by using conventional powder/slurry technique, 4 disks for each group; Feldspathic ceramic VITA VMK 95 (VMK), Leucite-based ceramic VITA VM9 (VM9), and Fluorapatite-based ceramic IPS e.max Ceram IVOCLAR (IEC). ND and DP specimens' thickness were (8×1 mm, shade A3) and (n=4). A digital camera was used to take samples' photos while the color readings were obtained by graphic software. The specimens' colors were measured, and the data were statistically evaluated using Levene's test, One-way ANOVA, and Post Hoc Multiple Comparisons. Results: Parametric CIE L*, a*, b*, and ΔE values of all ceramic disks compared to ND were significantly different even within ceramic brands (P&lt;.05), ΔE were ND &gt; IEC &gt; VMK &gt; VM9. Conclusions: To reproduce ND color by DP needs proper color shade guide selection due to color differences from one brand to another even in the same shade guide tab. Clinical Significance: There is a lack of information on how identical natural dentin color to dentin porcelain is at the same shade guide.

Effect of core and veneer porcelain thickness and resin cement on opalescence property of glass-ceramic veneers.

This study aimed to analyze the effect of core and veneer porcelain thickness and resin cement on the opalescence property (OP) of glass-ceramic veneers, which were used to restore discolored teeth. IPS e.max CAD LT A3 ceramic specimens were fabricated by computer aided design and computer aided manufacturing (CAD/CAM). The thickness values of core porcelain groups were 0.25 and 0.50 mm, and those of the core/veneer porcelain groups were 0.25 mm core/0.25 mm dentin, 0.50 mm core/0.25 mm dentin, 0.50 mm core/0.50 mm dentin, and 0.50 mm core/0.25 mm dentin/0.25 mm incisal. To simulate the clinical bonding procedure of porcelain veneer, resin cement Variolink N Bleach XL was coated at the bottom of CAD/CAM porcelain veneer specimens to make composite specimens of CAD/CAM porcelain veneer and resin cement. The L*a*b* values of specimens in the reflection and transmission pattern were measured by a spectrophotometer. Then, the OP was calculated. The OP values of 0.25 and 0.50 mm core porcelain groups, and 0.25 mm core/0.25 mm dentin, 0.50 mm core/0.25 mm dentin, 0.50 mm core/0.50 mm dentin, and 0.50 mm core/0.25 mm dentin/0.25 mm incisal core/veneer porcelain groups were 6.10±0.50, 7.00±0.24, 6.40±0.24, 7.08±0.28, 7.16±0.21, and 7.86±0.11 respectively. With increasing thickness of core porcelain, the OP values increased significantly (P<0.05). When 0.25 mm-thick dentin porcelain was added, no significant difference was found in the OP values of specimens with the same core porcelain thickness (P>0.05). For the 0.50 mm core porcelain group, no significant difference was found between 0.25 and 0.50 mm-thick dentin porcelain groups (P>0.05), but the OP values increased significantly after increasing the 0.25 mm incisal porcelain (P<0.05). The OP values of 0.25 mm core/0.25 mm dentin, 0.50 mm core/0.25 mm dentin, 0.50 mm core/0.50 mm dentin, and 0.50 mm core/0.25 mm dentin/0.25 mm incisal CAD/CAM porcelain veneer-resin cement composite specimens were 6.29±0.31, 7.56±0.36, 7.67±0.30, and 8.65±0.53. The OP values increased with increasing thickness of the porcelain layer (P<0.05), but no statistically signi-ficant difference was found between the groups of 0.50 mm core/0.25 mm dentin and 0.50 mm core/0.50 mm dentin (P=0.733). The influence of porcelain layer thickness and resin cement on the OP value was statistically different (P<0.05), and no interaction was found between the total thickness and the presence of resin cement (P>0.05). When using glass-ceramic veneers for discolored teeth, the following are recommended to improve the OP and obtain a natural and realistic effect: adopt the design of direct sintering incisal porcelain with core porcelain; appropriately increase the thickness of core porcelain; and select resin cement with opaque effect.

Effects of dentin and enamel porcelain layer thickness on the color of various ceramic restorations.

ObjectiveTo investigate the effects of dentin and enamel porcelain layer thickness on the color of various ceramic restorations.Materials and methodsEighty specimens (shade A2 and A3, n = 10) (20 mm in length, 4 mm in width, 1.5 mm in thickness respectively) of casting ceramic (EM); alumina ceramic (AL); zirconia ceramic (ZR); and porcelain‐fused‐metal (PFM) were prepared. The color distributions of each specimen were measured at 4 places using a spectroradiometer. The dentin/enamel porcelain (D/E) layer thicknesses of the 4 places were 0.8/0.2 mm, 0.6/0.4 mm, 0.4/0.6 mm, and 0.2/0.8 mm. The color differences (ΔE00) between the specimens and the corresponding color shade tabs were calculated. Data were analyzed using three‐way repeated‐measures ANOVA and Holm–Sidak pairwise comparisons (a = 0.05). The acceptability threshold (AT) was used to analyze the results.ResultsThe minimum ΔE00 values were 1.31 (0.6/0.4 mm for EM), 1.41 (0.8/0.2 mm for AL), and 1.92 (0.2/0.8 mm for ZR) for shade A2, and 0.93 (0.6/0.4 mm for EM), 0.89 (0.8/0.2 mm for AL), and 1.34 (0.8/0.2 mm for ZR) for shade A3. Most of them were below AT value (1.8). For AL and ZR (shade A2) and ZR (shade A3), the D/E layer thicknesses of 0.8/0.2 mm and 0.6/0.4 mm had lower ΔE00 values than 0.4/0.6 mm and 0.2/0.8 mm (p ≤ 0.001).ConclusionsThe dentin/enamel porcelain layer thickness that was most color‐matched to the shade tab was different for various ceramic restorations. The color of shade A2 AL and ZR and shade A3 ZR was closer to the shade tab when dentin porcelain was thicker than enamel porcelain.Clinical significanceMatching the shade of ceramic restoration to the shade tab color is a great challenge in esthetic dentistry. The dentin/enamel porcelain layer thickness is an important factor to influence the improved color matching.

Cytotoxic effects of dental prosthesis grinding dust on RAW264.7 cells

Respiratory diseases, including pulmonary fibrosis, silicosis, and allergic pneumonia, can be caused by long-term exposure to dental prosthesis grinding dust. The extent of the toxicity and pathogenicity of exposure to PMMA dust, Vitallium dust, and dentin porcelain dust differs. The dust from grinding dental prosthesis made of these three materials was characterized in terms of morphology, particle size, and elemental composition. The adverse effects of different concentrations of grinding dust (50, 150, 300, 450, and 600 μg ml−l) on RAW264.7 macrophages were evaluated, including changes in cell morphology and the production of lactate dehydrogenase (LDH) and reactive oxygen species (ROS). The dust particles released by grinding dental prosthesis made of these materials had different morphologies, particle sizes, and elemental compositions. They also induced varying degrees of cytotoxicity in RAW264.7 macrophages. A possible cytotoxicity mechanism is the induction of lipid peroxidation and plasma membrane damage as the dust particles penetrate cells. Therefore, clinicians who regularly work with these materials should wear the appropriate personal protection equipment to minimize exposure and reduce the health risks caused by these particulates.

Do repeated firings affect the color properties of porcelain‐fused‐metal restorations that are fabricated differently?

AbstractRepeated firings can affect the quality of the porcelain color. The purpose of this study is to evaluate the effect of repeated firings on the color changes of porcelain‐fused‐metal restorations that are manufactured using different methods. A total of 60 cylindrical shaped cobalt–chromium alloys (Ø = 10 mm and h = 1.5 mm) were fabricated using casting (C), milling (M), direct metal laser sintering with and without annealing (EL+, EL‐), and selective laser melting with and without annealing (CL+, CL‐). The samples were veneered with A2 (as indicated by the Vita Shade Guide) dentin porcelain of 2 mm thickness. Then the samples subjected to the repeated firings (2nd, 4th, 6th, 8th, and 10th), and the color of each sample was recorded using a spectrophotometer. The CIEDE2000 (ΔE00) formula was used to calculate color differences of the samples on repeated firings. Repeated measures analysis of variance (ANOVA) and post‐hoc Tukey's test were utilized to analyze the results (a = 05). The L*, a*, and b* values of porcelain‐fused‐metal specimens were significantly affected by the number of firings (P &lt; 0.001) and fabrication techniques (P &lt; 0.001). The ΔE00 values for C, M, CL‐, and EL‐ groups after 10th firing were above 0.8 unit, which indicates that visually perceivable color differences are clinically acceptable. On the other hand, the ΔE00 values for CL+ and EL+ groups were above the PT value after 8th repeated firings. The color properties of porcelain‐fused‐metal restorations were affected by the fabrication techniques and the number of firings.

CAN THE OPAQUE PORCELAIN AND DENTIN PORCELAIN BE SUBSTITUTED IN TITANIUM–PORCELAIN PROSTHETIC?

Due to the biocompatibility, mechanical strength and esthetics properties, titanium–porcelain prosthetic plays an important role in prosthodontics. However, weak bonding strength and considerable thickness of the porcelain restrict its application. Whether we can find a method to increase the bonding strength and reduce the thickness of the porcelain is an acute problem. In this study, ceramic coatings with similar color of nature teeth are fabricated on the surface of pure titanium by micro-arc oxidation (MAO). The colors, thickness and bonding strength of the coatings can be controlled by adding ferrous sulfate into the electrolytes. These new coatings can be used in titanium–porcelain prosthetic to substitute the opaque and dentin porcelain which can enhance the bonding strength and decrease the thickness of the porcelain compared with the conventional technique.

Preliminary evaluation on self-developed dentin porcelain color prediction system

To apply the self-developed dentin porcelain color prediction system in the fabrication of porcelain-fused-to-metal-crown(PFMC), and to evaluate its accuracy in color-matching. Twenty upper central incisors were recruited according to preset criteria, and three PFMC were made for each tooth using three shade-matching techniques. Group A: PFMC were made according to the result of visual color selection; Group B: an spectrophotometer-based color-matching technique was used; Group C: PFMC were fabricated with dentin porcelain powder calculated by the prediction system according to the L(*), a(*), b(*) value measured by a spectrophotometer. Color differences(ΔE) (measured by spectrophotometer) of three groups of crowns were calculated in the cervical, middle, and incisal regions. The results were analyzed using one-way ANOVA. Mean color differences in body regions were: Group A: 3.53±1.80, Group B: 2.86±1.63, Group C: 3.77±1.40(P>0.05), and those in incisal regions were: Group A: 2.70 ± 1.13, Group B: 2.80 ± 0.90, Group C: 3.04 ± 1.03(P>0.05). In cervical region, Group C had greater color difference than Group B(2.78±1.14)(P<0.05). Group A(3.80±2.02) and Group B, Group A and Group C had similar color difference(P>0.05). PFMC fabricated using self-developed dentin porcelain color prediction system had similar color matching compared with conventional and instrument-based methods.

Experimental and finite element study of residual thermal stresses in veneered Y-TZP structures

The main complications of zirconia-based laminated systems are chipping and delamination of veneering porcelain, which has been found to be directly associated with the development of residual thermal stresses in the porcelain layer. This study investigates the effects of cooling rate and specimen geometry on the residual stress states in porcelain-veneered zirconia structures. Bilayers of three different shapes (bars, semi-cylindrical shells, and arch-cubic structures) with 1.5mm and 0.7mm thickness of dentin porcelain and zirconia framework, respectively, were subjected to two cooling protocols: slow cooling (SC) at 32°C/min and extremely-slow cooling (XSC) at 2°C/min. The residual thermal stresses were determined using the Vickers indentation method and validated by finite element analysis. The residual stress profiles were similar among geometries in the same cooling protocol. XSC groups presented significantly higher tensile stresses (p=0.000), especially for curved interfaces. XSC is a time-consuming process that showed no beneficial effect regarding residual stresses compared to the manufacturer recommended slow cooling rate.

도재소성 시 냉각속도가 전부도재관의 색조에 미치는 영향

【Purpose: The purpose of this in vitro study was to evaluation the effect of shade on all ceramic restoration based zirconia according to cooling rate on Firing. Methods: 10 specimens applied to the dentin porcelain were made on the zirconia. After 5 specimens of the first group were burned in the furnace, these were put out rapidly. And after 5 specimens of the second group were burned in the furnace, these were put out slowly later 15 min. All specimens were measured $L^*$ , $a^*$ , $b^*$ using spectrophotometer, there were calculated 10 mean(SD) of descriptive statistics with SPSS program. These data were used for ${\Delta}E^*$ with color difference equation. Independent t tests were performed between 2 groups. Results: $L^*$ , $a^*$ , $b^*$ of 2 groups was statistically significant respectively (p ${\Delta}E^*$ was 4.55 value. Conclusion: This study showed effect of shade on all ceramic restoration based zirconia according to cooling rate on Firing.】

Effectiveness of Combination of Dentin and Enamel Layers on the Masking Ability of Porcelain.

This study evaluated the masking ability of different porcelain thicknesses and combination of enamel and/or dentin porcelain layers over simulated background dental substrates with higher (A2) and lower (C4) color values. Combination of the enamel (E) and dentin (D) monolayer porcelain disks with different thicknesses (0.5 mm, 0.8 mm, and 1 mm) resulted in the following bilayer groups (n=10): D1E1, D1E0.8; D1E0.5; D0.8E0.8; D0.8E0.5, and D0.5E0.5. CIELAB color coordinates were measured with a spectrophotometer. The translucency parameter of mono and bilayer specimens and the masking ability estimated by color variation (ΔE*ab) of bilayer specimens over simulated dental substrates were evaluated. Linear regression analysis was used to investigate the relationships translucency parameter × ΔE*, translucency parameter × porcelain thickness, and ΔE* × porcelain thickness. Data were analyzed statistically (α= 0.05). Thinner porcelain disks were associated with higher translucency. Porcelain monolayers were considerably more translucent than bilayers (enamel + dentin). Dentin porcelain was less translucent than enamel porcelain with same thickness. ΔE* was always lower when measured over A2 background. Higher ΔE* was observed for the C4 background, indicating poorer masking ability. Increased ΔE* was significantly associated with increased translucency for both backgrounds. Decreased translucency and ΔE* were associated with increased total porcelain thickness or increased dentin thickness for both backgrounds. In conclusion, increased porcelain thickness (particularly increased dentin layer) and increased porcelain opacity resulted in better masking ability of the dental backgrounds.

Influence of Different Thickness of Zirconia Core on the Flexural Strength of Bilayered Ceramics in Artificial Saliva

To study the effect of different core thickness on the flexural strength of zirconia and feldspathic ceramics. Bilayered zirconia-feldspathic samples of three commercial brands were made in three different thickness(n=10): 0.5 mm, 0.8 mm and 1.0 mm respectively. On zirconia core specimens of each thickness, feldspathic dentin porcelain was added to reach a total crown thickness of 2 mm. Samples were stored in artificial saliva with neutral pH for 10 days at 37°C. Flexural strength was conducted with 3-point bending test. Data were analyzed by one-way ANOVA, and multiple comparisons were performed using Student-Newman-Keuls test(α=0.05). The measurement of 1.0 mm group was higher than the other groups, and 0.5 mm group was the lowest(P＜0.05), regardless of any commercial brand. Commercial dental zirconia blocks had varied flexural strength, Zirkonzahn expressed highest value in any thickness group compared with the other materials. Moreover, the fracture mode of zirconia bilayered composites was different in this study, 0.5 mm and 0.8 mm groups exhibited higher number of fragments and appeared to delamination compared with 1.0 mm group. So we infer that the thickness of core can have an effect on the flexural strength of bilayered zirconia-feldspathic crown, as well as different kinds of materials.

Influence of dentin and core porcelain thickness on the color of fully sintered zirconia ceramic restorations

The influence of the thickness of dentin and core porcelain, and the glazing procedure on the color of computer-aided design and computer-aided manufacturing ceramic restorations has not been investigated. This study evaluated the influence of the thickness of dentin and core porcelain and glazing on the color of fully sintered zirconia ceramic restorations. Fully sintered zirconia core material was cut into 90 specimens of 0.3 mm (n=30, group ZC1), 0.4 mm (n=30, group ZC2), and 0.5-mm thickness (n=30, group ZC3). On a dentin disk obtained from an extracted molar, the L*, a*, b* values of the specimens were measured at different steps in the laboratory procedures (Zirconia core, Effect Bonder, Effect Liner, dentin porcelain, glazing) with a spectrophotometer. One millimeter dentin porcelain was applied on half of the specimens of each group and 1.5-mm dentin porcelain on the rest. To assess the ability of porcelain substructures to mask the underlying dark colored tooth structure, color difference (ΔE) values between the steps were calculated. Results were statistically analyzed with ANOVA. Glazing caused a decrease in the L* values and an increase in the a* and b* values (P<.05). Increasing the thickness of dentin porcelain decreased the L*, a*, and b* values (P<.05). Increasing the zirconia core thickness resulted in an increase inthe L* values and a decrease in the a* and b* values (P<.05). Increasing the dentin porcelain thickness from 1 mm to 1.5 mm resulted in a color change below the perceptibility threshold (ΔE<2.6). In the ZC1 group, glazing resulted in a color change perceptible to 50% of observers, whereas, in the ZC2 and ZC3 groups with 1-mm dentin porcelain, the ΔE value was higher than 5.5. However, the color change was perceptible to 50% of the observers in all of the groups with 1.5-mm dentin porcelain. Although the thicknesses of the dentin and core porcelain did not influence the final shade of the restoration, glazing resulted in a perceptible color difference.

Influence of different Thickness of Zirconia Core on the Flexural Strength in Article Saliva

To Study the Effect of Different Core Thickness on the Flexural Strength of Zirconia and Feldspathic Ceramics. Bilayered Zirconia-Feldspathic Samples of Three Commercial Brands were Made in Three Different Thickness(n=10): 0.5 Mm, 0.8 Mm and 1.0 Mm Respectively. on Zirconia Core Specimens of each Thickness, Feldspathic Dentin Porcelain was Added to Reach a Total Crown Thickness of 2 Mm. Samples were Stored in Artificial Saliva with Neutral Ph for 10 Days at 37°C. Flexural Strength was Conducted with 3-Point Bending Test. Data were Analyzed by One-way ANOVA, and Multiple Comparisons were Performed Using Student-Newman-Keuls Test(α=0.05). the Measurement of 1.0 Mm Group was Higher than the other Groups, and 0.5 Mm Group was the Lowest(P＜0.05), Regardless of any Commercial Brand. Commercial Dental Zirconia Blocks had Varied Flexural Strength, Zirkonzahn Expressed Highest Value in any Thickness Group Compared with the other Materials. Moreover, the Fracture Mode of Zirconia Bilayered Composites was Different in this Study, 0.5 Mm and 0.8 Mm Groups Exhibited Higher Number of Fragments and Appeared to Delamination Compared with 1.0 Mm Group. so we Infer that the Thickness of Core can have an Effect on the Flexural Strength of Bilayered Zirconia-Feldspathic Crown, as well as Different Kinds of Materials.

The effect of surface treatments on the bond strength of a nonprecious alloy-ceramic interface: an invitro study.

The purpose of this study was to compare the effect of seven different alloy surface treatments on the bond strength of the porcelain-metal interface. Three layers of opaque porcelain and a measured thickness of dentin porcelain were applied to nickel-chromium alloy, A tensile bond strength test was used. The alloy surface treatment that exhibited the highest bond strength was sandblast+surface grinding+sandblast+de-gas, whereas the alloy surface treatment that exhibited the lowest bond strength was sandblast+surface grinding+sandblast+steam cleaning+de-gas. There was a significant difference between the two methods (P<0.05). It was concluded that de-gassing the alloy prior to porcelain application increased the bond strength and excess surface grinding of the alloy reduced bond strength; steam cleaning the alloy surface prior to de-gassing and porcelain application also significantly reduced the bond strength.

Factors Affecting on the Bond Strength of Dental Zirconia to Veneering Porcelains

The bond strengths between two kinds of zirconia and three kinds of feldspathic veneering porcelains were measured. The specimens were prepared at four firing temperatures for three holding periods, respective opaque porcelain was painted and vacuum-fired. Then, each dentin porcelain was condensed in an acrylic resin mold and vacuum-fired under the conditions mentioned above. Cross sections of the interface between zirconia and porcelain were observed with a scanning electron microscope. The specimens were fixed to specimen holder on a universal testing machine. Data of the bonding test were statistically analyzed. The results showed that all the four factors statistically affected the bonding strength (p&lt;0.01). The contribution of the firing temperature was highest and that of the porcelain type was lowest (p&lt;0.01).

WITHDRAWN: Light transmission of zirconia ceramics with different colors and thicknesses

Abstract Background/purpose It is clear that any reduction in the degree of conversion due to inadequate power output from a polymerization lamp will have an adverse effect on resin performance. The aim of this study was to evaluate the light transmission of zirconia ceramics with different zirconia core thicknesses and colors when irradiated with different types of light polymerization units. Materials and methods Zirconia core specimens, 11 mm in diameter, were made in three different thicknesses (0.5 mm, 0.8 mm, and 1.0 mm) for each of 16 color shades of the Vita Lumen Classical scale ( n = 240). On zirconia core specimens of each color and thickness group, feldspathic dentin porcelain of the same color was added to reach a total veneer thickness of 1.5 mm. In total, 48 groups ( n = 5) consisting of different zirconia core thicknesses and colors were glazed. Light transmission of all groups was measured by a radiometer and recorded as mW/cm 2 for a conventional halogen light (Hilux 200), LED 1 (Hilux LED-max 550), LED 2 (Hilux LED-max 1055), Bluephase LED ‘curing light' (Ivoclar), and plasma arc light (Monitex SP-200). Data were statistically analyzed with three- and two-way ANOVAs. For multiple comparisons of mean values, Tukey's HSD test was used ( α = 0.05). Results According to the three-way ANOVA results, when comparing different light units, thickness, and color groups, there were statistically significant differences among groups ( P Conclusion For any thickness, color, and polymerization unit tested, there did not appear to be adequate transmission of light through the zirconium ceramic samples to achieve effective resin polymerization.

The influence of resin flexural modulus on the magnitude of ceramic strengthening

IntroductionThe aim was to determine the magnitude of ceramic resin-strengthening with resin-based materials with varying flexural moduli using a regression technique to assess the theoretical strengthening at a ‘zero’ resin-coating thickness. The hypothesis tested was that experimentally, increasing resin flexural modulus results in increased resin-strengthening observed at a theoretical ‘zero’ resin-coating thickness. MethodVitadur Alpha dentin porcelain disk (n=250) were condensed, fired, alumina particle air abraded and randomly assigned into ten groups. Groups were resin-coated at 50, 100 and 150μm with Venus Flow, Rely-X Veneer and Clearfil AP-X before biaxial flexure testing at 24h and the stress at failure calculated using a multilayer analysis. An analytical methodological approach was undertaken to predict the biaxial flexure stresses under boundary conditions that reflected the experimental test and a finite element model was used to verify the analytical prediction. ResultsThe magnitude of resin-reinforcement was significantly influenced by resin-coating type (P<0.001) and resin-coating thickness (P=0.013), however, a significant interaction was observed between resin-coating type and thickness (P=0.048). Linear regression identified a 17, 38 and 47% biaxial flexure strength contribution when Venus Flow, Rely-X Veneer and Clearfil AP-X were used, respectively. The finite element model determined the maximum principal stress was within 3.3% of the predicted analytical solution. SignificanceExperimentally, the flexural modulus and thickness of resin-based material used to cement DBC or PLV restorations have a significant impact on the magnitude of resin-strengthening observed. However, for resin-based materials with different flexural moduli the variability in the relationships between thickness and observed increases in biaxial flexure strength of the ceramic requires careful characterization to optimize clinical performance.