Density Of Specimens Research Articles

Mechanical properties of beech wood treated with malic acid-based polyester

Abstract While chemical modification enhances wood’s resistance to deterioration and dimensional stability, it often results in alterations to the mechanical properties, limiting its engineering applications. This study focuses on the in situ esterification of beech wood using malic acid/polyol mixtures and evaluates its impact on mechanical properties. The results of the compression tests yielded limited information, characterized by a notable degree of variability as indicated by the high standard deviation. The four-point bending tests conducted here revealed an increase in the modulus of elasticity (MOE). However, this improvement in MOE was accompanied by a decrease in the modulus of rupture (MOR), indicating a trade-off between stiffness and strength. To better understand the mechanisms affecting the treated wood’s mechanical properties, we compared the experimental and theoretical glass transition (Tg) of the polymers with material stiffness. X-ray computed tomography revealed that treatment increases specimen density and creates a gradient, with higher density near the surface, potentially contributing to increased stiffness. These findings suggest a nuanced impact of the in situ esterification process using malic acid/polyol mixtures on the mechanical properties of beech wood.

A practical analysis to predict sample overheating in flash experiments using the current ramp methodology

AbstractThis work presents a straightforward strategy for achieving specific overheating during flash experiments by adjusting the initial electrical parameters. To do that, an extensive experimental analysis was performed to evaluate the temperature evolution of dense ZnO specimens during controlled‐current ramping at different furnace temperatures, which in turn modified the initial electrical resistance of the sample. A detailed electrical explanation of controlled‐current ramp flash processes is provided and, for the first time, a practical equivalence between current‐ramp and temperature‐ramp flash methodologies is established. By parameterizing the experiments in terms of an effective power density, a consistent heating pattern following the blackbody radiation trend was identified, despite the different electrical characteristics of each experiment. Finally, a “flash heating map” is introduced, which can be used to determine the starting electrical parameters necessary to achieve a specific temperature increase, whether employing current or temperature ramps.

Direct Ink Writing and Rapid Microwave Sintering of Alumina

The additive manufacturing of ceramics is gaining attention due to difficulties in fabricating complex ceramic parts because of its hard and brittle nature. Direct ink writing (DIW) is a unique process in which solid-loaded slurry is extruded to print complex-shaped ceramic parts directly. In the present work, a new composition of high-solid loaded (76 wt.%) alumina ink is prepared for printing ceramic parts with complex structures. The rheology of ink is optimized to ensure the shear thinning behavior of the ink, while thermogravimetric analysis (TGA) of the printed part was carried out to optimize the debinding temperature. The printed alumina part is sintered using the conventional furnace and rapid microwave sintering process, and a comparison has been made. Microwave, a rapid sintering method with a high heating rate, produced >97% dense specimen, while the hardness and flexural strength values of 15.18 ± 0.6 GPa and 148.87 ± 2.14 MPa were achieved, respectively. Rapid microwave sintering of additively manufactured ceramic parts can reduce the energy consumption and overall production time needed to manufacture ceramic parts.

Effects of hard anodizing on mechanical and electrochemical characteristics of aluminum alloys under tribocorrosion condition

In this research, the effects of hard anodizing on the mechanical and electrochemical characteristics of aluminum alloys under tribocorrosion conditions was investigated. Compared with dry conditions, friction coefficient of aluminum alloys under tribocorrosion conditions increased, whereas that of hard anodized specimens decreased. This was attributed to corrosive ions in the solution corroding the transfer film of the counter-body and tribofilm of the hard anodized specimen. In potentiodynamic polarization experiments under tribocorrosion conditions, the aluminum alloys exhibited high current density with applied load. However, at potentials above –0.05 V, current density decreased and was reversed. This is believed to be due to the corrosive ions preferentially reacting with the generated wear debris, thereby reducing the oxidation reaction with wear track. However, the current density of the hard anodized specimens increased with load and potential. In addition, the increasing rate in the wear width and depth was significant under tribocorrosion conditions (Width: 42.65 %, Depth: 32.63 %). This is due to the cavitation and fluid impact generated during friction/wear accelerating the cracking and damage of the hard anodizing film with the brittleness and porousity. However, the tribocorrosion resistance of the hard anodized aluminum alloy was improved by more than 97 %.

A comprehensive study of LPBF parameter influence in 316L stainless steel mechanical properties, macrostructure, and printability

Additive manufacturing, particularly using Laser Powder Bed Fusion (LPBF) technologies with 316L stainless steel, has proven highly promising in biomedical engineering due to the material’s exceptional mechanical properties and biocompatibility. This study, which is a foundational step towards developing porous bone implants, focuses on assessing the influence of a broad range of parameters - spot size, scanning speed, laser power, and energy density - on the mechanical performance and structural integrity of 316L stainless steel parts across three distinct specimen geometries: fully dense parallelepipedic, fully dense cubic, and cellular (lattice) specimens. By analysing 17 different parameter sets and producing over 150 specimens, a thorough series of experimental tests were conducted, including flexural tests, compression tests, hardness tests, macroscopic evaluation of the surface of fully dense specimens, and macroscopic evaluation of the lattice structures.e in powder accumulation within the pores of cellular structures, with higher energy densities (100 J/mm3) leading to a significantly greater retention compared to lower energy densities (66 J/mm3). This underexplored phenomenon has significant implications for the selection of parameters in the fabrication of bone implants. Further research is needed to refine LPBF printing parameters and enhance the quality of porous bone implants.

Flash sintering of AlN ceramics with Y2O3 additive

This study demonstrates the fabrication of dense AlN-based ceramics through the flash sintering technique for the first time. Flash sintering was performed at a furnace temperature of 1500 °C with 10 wt% Y2O3 as a sintering aid in a nitrogen atmosphere. The effects of the current density and holding time on the microstructure evolution and mechanical properties were investigated. The results show that the relative density, grain size and Vickers hardness of specimens increase with increasing current density and holding time. The specimen showed the highest relative density of 98.6% and a Vickers hardness of 12.68 GPa when a current density of 100 mA/mm2 and a holding time of 60 min were used. Additionally, the grain sizes at the positive side of the electrodes were found to be larger than those at the negative side. These findings suggest that dense AlN-based ceramics can be fabricated in a rapid and efficient way through the flash sintering technique.

Sedimentation-affected engineering performances and microstructures of a hybrid Portland-sulfate aluminate cement grout cast in long tubes

Material sedimentation may have non-negligible impacts on engineering properties of flowable cement grouts, and this issue cannot be addressed by in-lab tests on small size specimens. Herein, sedimentation tests were conducted to a high-strength hybrid Portland-sulfate aluminate cement (P-SAC) grout cast in 6-m-long tubes. Compressive strength and density of the P-SAC specimens at different depths were measured, and microstructures were assessed by X-ray computed tomography (XCT), scanning electron microscopy (SEM), and X-ray diffraction (XRD). Results showed that the hybrid P-SAC grout possessed the superior indices of flowability, expansion and compressive strength. The increasing rates of density and compressive strength to depth were 9.3 kg/m4 and 0.5 MPa/m, respectively. The shallow sites possessed a porous structure with 14.5 % more big pores (>1 mm). The pore structure followed fractal patterns, and the fractal dimensions increased slightly with depth. Our findings not only deepen the understandings in slurry sedimentation and the consequences of engineering properties, but also narrow the knowledge gaps between in-lab tests and in-situ applications for grouting construction.

Recent Advances in High-Entropy Ceramics: Synthesis Methods, Properties, and Emerging Applications

High-entropy ceramics (HECs) represent an emerging class of materials composed of at least five different cations or anions in near-equiatomic proportions, garnering significant attention due to their extraordinary functional and structural properties. While multi-component ceramics have played a crucial role for many years, the concept of high-entropy materials was first introduced eighteen years ago with the synthesis of high-entropy alloys, and the first high-entropy nitride films were reported in 2014. These newly developed materials exhibit superior properties over traditional ceramics, such as enhanced thermal stability, hardness, and chemical resistance, making them suitable for a wide range of applications. High-entropy carbides, borides, oxides, oxi-carbides, oxi-borides, and other systems fall within the HEC category, typically occupying unique positions within phase diagrams that lead to novel properties. HECs are particularly well suited for high-temperature coatings, for tribological applications where low thermal conductivity and similar heat coefficients are critical, as well as for energy storage and dielectric uses. Computational tools like CALPHAD streamline the element selection process for designing HECs, while innovative, energy-efficient synthesis methods are being explored for producing dense specimens. This paper provides an in-depth analysis of the current state of the compositional design, the fabrication techniques, and the diverse applications of HECs, emphasizing their transformative potential in various industrial domains.

Влияние технологических параметров на микроструктуру и свойства сплава AlSiMg, полученного методом селективного лазерного плавления

Introduction. The development of additive technologies is aimed at the synthesis of new powder compositions for selective laser melting plants, the study of the effect of mode parameters on the stable quality of products. The purpose of this work is to study the effect of the scanning strategy on the microstructure, elemental composition, porosity and density of specimens obtained by selective laser melting from non-spherical powders (Al — 91 wt. %, Si — 8 wt. %, Mg — 1 wt. %), subjected to special preparation to determine the optimal conditions for selective laser melting. The research methods are methods of X-ray diffraction and X-ray phase analysis, transmission electron microscopy. The paper examines specimens formed using four different scanning strategies. Results and discussions. A promising aluminum alloy AlSi8Mg is developed for selective laser melting. The material has good manufacturability and low powder cost. The technological parameters of melting make it possible to form a thin structure with a low level of porosity. The mechanism of influence of the scanning strategy on porosity, surface morphology, relative density and microstructure is investigated. A specimen from the AlSi8Mg powder composition with a high relative density of 99.97 % is produced by selective laser melting with an energy density of 200 J/mm3, a specimen scanning circuit when the direction of laser movement changes by an angle of 90° each odd layer. It is proved that the density of the AlSiMg alloy depends on the scanning strategy used. The calculated density of the specimen was 2.5 g/cm3, which corresponds to the density of silumin. Analysis of SEM images and maps of the distribution of elements (Al, Mg, Si) of the specimens showed that different specimen formation strategies do not affect the nature of silicon distribution. A unique grain structure is observed in the resulting AlSi8Mg alloy. The melt pool consists of small grains along the border and large grains in the center. The formation of fine grains is explained by the addition of Si and the high cooling rate during selective laser melting.

Densification, phase composition, microstructure and properties of spark plasma sintered La0.6Ce0.3Pr0.1B6 bulks

This paper studied the densification, phase composition, microstructure and properties of polycrystalline La0.6Ce0.3Pr0.1B6 bulks prepared by SPS. The dense specimen (98.9 % in relative density) with the average grain size of 15.46 μm has been determined to be a CsCl-type single-phase substitutional solid solution without any impurities or other secondary phases. The homogenous elemental distributions of La, Ce and Pr have been confirmed by both microscale and nanoscale. The room temperature (RT) Vickers hardness (Hv), indentation fracture toughness (KIC) and flexure strength of the dense specimen have been measured to be 23.0 GPa, 2.04 MPa m1/2 and 305.1 MPa, respectively. The Berkovich hardness (HB) and elastic modulus (E) of the dense specimen have been measured to be 30.0 GPa and 376.0 GPa, respectively, by nanoindentation tests at a maximum load of 40 mN. In comparison with the polycrystalline LaB6 bulk, the lower work function Φ of 2.64 eV evaluated by UPS and the larger thermionic emission current densities measured at the same operating condition suggest that the polycrystalline La0.6Ce0.3Pr0.1B6 bulk is a superior-performance thermionic cathode material.

Laser Powder Bed Fusion of Copper-Tungsten Powders Manufactured by Milling or Co-Injection Atomization Process.

The processing of pure copper (Cu) has been a challenge for laser-based additive manufacturing for many years since copper powders have a high reflectivity of up to 83% of electromagnetic radiation at a wavelength of 1070 nm. In this study, Cu particles were coated with sub-micrometer tungsten (W) particles to increase the laser beam absorptivity. The coated powders were processed by powder bed fusion-laser beam for metals (PBF-LB/M) with a conventional laser system of <300 watts laser power and a wavelength of 1070 nm. Two different powder manufacturing routes were developed. The first manufacturing route was gas atomization combined with a milling process by a planetary mill. The second manufacturing method was gas atomization with particle co-injection, where a separate W particle jet was sprayed into the atomized Cu jet. As part of the investigations, an extensive characterization of powder and additively manufactured test specimens was carried out. The specimens of Cu/W powders manufactured by the milling process have shown superior results. The laser absorptivity of the Cu/W powder was increased from 22.5% (pure Cu powder) to up to 71.6% for powders with 3 vol% W. In addition, a relative density of test specimens up to 98.2% (optically) and 95.6% (Archimedes) was reached. Furthermore, thermal conductivity was measured by laser flash analysis (LFA) and thermo-optical measurement (TOM). By using eddy current measurement, the electrical conductivity was analyzed. In comparison to the Cu reference, a thermal conductivity of 88.9% and an electrical conductivity of 85.8% were determined. Moreover, the Vickers hardness was measured. The effect of porosity on conductivity properties and hardness was investigated and showed a linear correlation. Finally, a demonstrator was built in which a wall thickness of down to 200 µm was achieved. This demonstrates that the Cu/W composite can be used for heat exchangers, heat sinks, and coils.

Feasibility of Utilizing Pulverized Ceramic Wastes as Potential Admixture for an Equimolar Clay-Brick Derivative

The heat-transmuted solid wastes of opalescent structures can be pulverised and recycled entirely for highly developed products. Hence, the objective of this paper was to investigate the feasibility of utilizing pulverised ceramic wastes (CWs) as a potential admixture for fired clay-brick derivative at 950oC with partial substitution at an equal ratio of clay (CL) and kaolin (KL) for water absorption rate and compressive strength test during loading. Several appropriate standard technics were employed. Results revealed that the sole compaction of ceramic wastes (Cs0) has the lowest strength density of 1.21MPa, compared with the progressive linear density of specimens with the addition of clay compositions as stabilizers. Sp10 has a higher resistance of 2.39MPa during compressive loading and a decrease in the quantities of ceramic wastes from Sp11-15 caused a low linear strength but an increase in the water absorption rate. Conclusively, ceramic wastes have a positive effect on clay bricks’ strength and water absorption when equally substituted with clay compositions. The study provides an avenue for solving ceramic waste disposal challenges and unveils the approach to boost the products of waste recycling industries, enhancing technological and economic growth.

Enhancing reliability in laser powder bed fusion through substrate modification: microstructure, mechanical properties and residual stress

Laser additive manufacturing (LAM) is prone to excessive tensile residual stresses, leading to cracking or even failure, seriously hindering its wide application. Therefore, controlling residual stress to avoid crack formation and improve forming quality is crucial for reliable LAM. Most of the past research controls the residual stresses by modifying the process during the forming process, which is a very complicated method. In this study, through alterations in the form of a substrate to modify its restraint effect on the resulting structure and heat dissipation channels, the impact of them on the microstructure, defects, residual stress, and fracture characteristics to mitigate the likelihood of cracking in laser powder bed fusion (LPBF) was systematically studied. The results showed that the microstructure of all the specimens consists of fine dendritic, cytosolic, and columnar. Specimens with un-grooved substrates exhibited more holes and cracks, and solidification cracks were predominant. The crack density in specimens with grooved substrates was reduced by 71 %, reaching a relative density of 98.94 %. Tensile test results showed that the mechanical properties of the grooved specimens were excellent, with the tensile strength and yield strength higher than the un-grooved samples by 29 MPa and 11.7 MPa, respectively. And the results of the residual stresses indicated significantly lower tensile residual stresses in specimens with grooves, due to reduced restraint stresses and increased heat dissipation, mitigating the extent of crack propagation. These findings provided a simpler new approach to LPBF of crack-free components with excellent mechanical properties.

The improved cyclic resistance of bio-treated sands with various gradations for liquefaction mitigation: Density increase and/or cementation?

MICP (microbial induced calcium carbonate precipitation) method shows a huge potential in solving geological and geo-environmental engineering problems, such as liquefaction mitigation, soil remediation, erosion control, slope stabilization and dust control., due to its low-carbon, sustainable and undisturbing character. For the liquefaction mitigation, previous studies showed the remarkable enhancement in cyclic behavior of bio-cemented soils. Little attention has been paid to how soil gradation affects the effectiveness of MICP method in enhancing soil properties, which is one of the key factors of soil mechanical behavior. MICP method has been mainly used in fine sands (mostly <1 mm) with narrow gradation and a certain number of particles smaller than 75 μm. As a result, few papers discussed the application of bio-cementation to soils with larger grains. In addition, the respective contributions of density increase and cementation on cyclic resistance enhancement is still not clear. In this study, a fine sand (0.1–1 mm), a coarser sand (1–5 mm), and a mixture of both, were used, featuring a larger mean size (d50 mm) and uniformity coefficient (Cu) than in most previous studies. In this study, cyclic undrained triaxial tests were performed to analyze the liquefaction potential of loose and dense untreated specimens, and initially loose treated specimens. Results show that sand gradation has a great influence on the cyclic behavior and MICP effectiveness. For all the sands, the MICP treatment gives rise to a significant increase in cyclic resistance and mitigates liquefaction. This enhancement is due to the formation of cementitious precipitates in the pores or on the surface of particles, which creates (1) bridges between particles and/or change in grain characteristics (i.e., size, roughness, angularity), and (2) an increase in density. For sands with various gradations, these two effects differ in magnitude: in the coarsest sand, the effect of density increase appears to be predominant whereas, in the finest and medium sands, the formation of bonds seems to play the major part. These results are important to evaluate the possibility of using this method to improve cyclic resistance in various sands, and to compare the treatment effect with other techniques.

Gradient ceramic structures via multi-material direct ink writing

Dense boron carbide-silicon carbide specimens with composition tailored at the mesoscale were produced by direct ink write additive manufacturing in three configurations: I, 2 % and II, 10 % compositional layer-to-layer steps, and III, homogeneous composition throughout. Flexural strength, indicative of tensile failure, is the highest for the Type-II design (366 MPa) due to its compressive residual stress state in the surface layers. Analysis of thermally-induced residual stresses predicts the ranking of the flexural strengths obtained for Type-II (highest), Type-I (intermediate), and Type-III (lowest) specimens. Compressive strength is load-orientation independent, highly strain-rate dependent, and reduced for specimens with thermal residual stress. Mechanical tests were performed in cube and dumbbell geometries. Dumbbell geometry compression specimens have a compressive strength that is 68 % (quasistatic) and 86 % (dynamic) higher than that of cube geometry and show a greater strain rate dependence. The rate dependency is attributed to the competition between crack propagation and loading velocities. Type-I dumbbells show the highest mean compressive strength of 3.96 GPa (quasi-static) and 5.11 GPa (dynamic). The failure mode evolves from mixed intergranular/transgranular at low strain rates to transgranular at high strain rates. High-speed video analysis indicates that dumbbell geometry specimens fail in compression due to microcrack growth and coalescence, while cubes fail due to the axial macrocracks that develop at the specimen/load platen interface and propagate into the specimen parallel to the loading direction (end splitting). This work demonstrates the impact of compositional variation, tailored by additive manufacturing, on the mechanical performance of ceramic composites.

Comparison of microstructure, mechanical properties and corrosion resistance of Ti6321 alloy by wire-arc directed energy deposition versus rolling

Ti-6Al-3Nb-2Zr-1Mo (Ti6321) alloy, as a new type of marine metal, has excellent corrosion resistance and mechanical properties, but its application is restricted by the traditional manufacturing processes. Wire-arc directed energy deposition (DED) has some incomparable advantages in the efficient and customized fabrication of large/extra-large components, which makes it become a potential manufacturing process for the fabrication of Ti6321 alloy components. However, the formability and corresponding performance evaluation of wire-arc DEDed Ti6321 alloy remains unknown. Here, for the first time, the microstructure, mechanical properties and corrosion resistance of wire-arc DEDed Ti6321 alloy was characterized and compared with rolling, and the relationship between process-microstructure-properties was established. Results show that the full lamellar α+β structure of the DEDed specimens demonstrated better corrosion resistance than the near equiaxed αp + lamellar αs/β structure of rolled specimens. This is owed to the higher grain boundary density, more content of β phase and slighter element segregation of the DEDed specimens, resulting in a more uniform and stable passivation film on its surface. Meanwhile, the grain morphology and low dislocation density of the DEDed specimens causing in lower tensile strength (decrease by ∼15.6 %) but higher elongation (increase by ∼41.5 %) than the rolled specimens. Due to the presence of coarse prior-β grains, the DEDed specimens show expected anisotropy in building direction and traveling direction, but overall exhibits sufficient mechanical properties, which exceed the execution standard. This study verified the feasibility of fabricating Ti6321 alloy with idea properties by wire-arc DED, and provides a potential strategy for the production and practical application of large-size Ti6321 alloy components.

Gradient microstructures and mechanical properties of WAAMed and aged Al–Cu alloy after laser shock peening

The integration of wire-arc additive manufacture (WAAM) and laser shock peening (LSP) facilitated the study of the gradient microstructure in T6-treated WAAM Al–Cu alloy and the synergistic strengthening mechanisms involving the precipitation phase and LSP parameters. The results indicate that pore closures, increases in kernel average misorientation (KAM), and low angle grain boundary (LAGB) are positively associated with LSP energy density. Residual stress positively correlates with LSP energy density and inversely with spot diameter, where larger spots exacerbate non-uniformity. The values of dislocation density, microhardness and residual stress of the post-LSP specimen gradually increase with the increase of depth, and reach the maximum value at ~100 μm. As the depth continues to increase, the value begins to decrease gradually. Dislocation accumulation near grain boundaries, interacting with θ’-Al2Cu, contributes to strength enhancement. The main strengthening mechanisms enhanced by LSP involve creating a gradient microstructure through significant plastic deformation, pore closure, and the presence of high-density dislocations. Post-T6 treatment, θ’-Al2Cu significantly restricts dislocation slip, pins dislocations, and encourages the emergence of new dislocation sources, thereby enhancing the strengthening effect and stability induced by LSP.

Evolution of structure and anisotropic shear stiffness of compacted loess during compression

Different compaction conditions (water content and density) may induce various soil structures. The influence of these structures on small strain shear stiffness G seems contradictory and is not understood (e.g., denser specimens may have larger or smaller G than looser specimens after compression). Furthermore, the influence of compaction condition on stiffness anisotropy remains unclear. This study investigated the evolution of structure and anisotropic stiffness of saturated and compacted loess during isotropic compression. Specimens compacted at different water contents and densities were explored. The measured G was normalised by a void ratio function (f(e)) to eliminate density effects. Before yielding, G/f(e) increases with decreasing compaction water content and increasing density. These two trends are reversed at large stresses (2 to 3 times yield stress), implying that an initially softer structure becomes stiffer. Based on MIP, SM and SEM results, the trend reversal is likely because interparticle contacts are more strengthened and pores are more compressed in the initially softer specimens. Furthermore, the stiffness anisotropy becomes more significant with decreasing compaction water content and increasing density because of more orientated fabrics, as evidenced by the particle/aggregate directional distribution results.

Field-assisted sintering of barium titanate and 45S5 bioactive glass for biomedical applications

The development of electrically active biomaterials, which create electrical cues on demand to foster cellular stimulation, remains a challenge. Here, we utilized a Field-assisted sintering approach to densify barium titanate and 45S5 bioactive glass to create a piezoelectric and potentially bioactive composite. By using Field-assisted sintering, we aimed to fabricate dense piezoelectric specimens, preserving a low degree of crystallization of the bioactive glass to keep bioactivity as high as possible. Therefore, we have varied the compositions of the materials and processed them at different sintering temperatures. This enabled us to produce dense test specimens in the 94 %–98 % relative density range. The samples were successfully polarized, and piezoelectric charge constants d33 were determined for the composites. The content of bioactive glass and the sintering temperature influence the charge constant d33. It is in the range of 0.8–3.4 pC/N for the composites, approximately in the order of magnitude assigned to natural tissues such as bone. X-ray diffraction was used to analyze the composition of the processed samples and to investigate the influence of an additional thermal post-treatment. Altogether, we established a process window for field-assisted sintering, allowing the fabrication of a piezoelectric and potentially bioactive biomaterial for tissue engineering.

Mechanical behaviors and progressive fracture processes of dry basalt after Martian cryogenic freeze-thaw cycles

The steep Martian terrain features numerous notches and alcoves that could potentially be adapted as temporary shelters. By sealing their entrances and modifying the interior space, these alcoves can be transformed into habitable structures. Given their prolonged exposure to Martian temperature fluctuations, it is crucial to understand the mechanical properties of alcove rocks to design appropriate shelter parameters. This study investigates the mechanical behavior of basalt specimens subjected to Martian cryogenic freeze-thaw (F-T) cycles (−143∼35 °C) and subsequent uniaxial cyclic loading tests. The test results indicate that the longitudinal wave velocity, peak stress, and elastic modulus of basalt specimens degrade to varying degrees with an increasing number of F-T cycles. At higher stress levels, the ratio of dissipated energy density to elastic energy density in basalt specimens subjected to different F-T treatments converges to approximately 0.25. During the uniaxial cyclic loading tests, both cumulative acoustic emission (AE) counts and average maximum principal strains of the specimens increase stepwise. For specimens after F-T treatment, the spectral-domain characteristics can be classified into three frequency bands, with the middle and high frequencies predominating. The application of the Gaussian Mixture Model (GMM) clustering algorithm enhances the analysis of AE results, facilitating the identification of tensile and shear cracks. As the number of F-T cycles increases, the percentage of shear cracks in basalt specimens decreases from 76.5% (0 cycle) to 53.5% (7 cycles).