Al-3 wt% TiO 2 particle composite was solidified in the form of a vertical cylindrical ingot to segregate the particles at the top. The machined surface of the ingot showed three regions with varied particle content. Coarse particles were segregated at the top and the particle density was greater at the top zone. The next zone, at the bottom of the ingot, contained less particles, whilst the rest of the ingot appeared to be free from particles. Voids were also present in the particle-enriched zones. The top zone of the composite fractured on hot rolling due to its greater particle content (a volume fraction of 0.10). The middle zone with a 0.05 volume fraction of particles, and the bottom zone, could be rolled successfully. The particle size and the inter-particle, distance reduced on hot rolling. The hardness and tensile strength of the coarse particle-enriched zone was less than that of the bottom part of the composite, as voids were also segregated into the former. The presence of fine Al 3O 3 particles without voids in the bottom part of the composite resulted in better mechanical properties.