Natural sand samples taken from the Rokan river, Riau Province, Indonesia, have been ball milled for 100 (one hundred) hours using a ball with a diameter of 1.5 cm and a constant rotation angular velocity of the tube of 100 revolutions / minute. Neodymium Iron Boron (NdFeB) strong magnets are used to separate magnetic minerals from their non-magnetic minerals. Magnetic induction was measured using the Pasco PS-2162 probe and its value was used to calculate the magnitude of magnetic susceptibility, it turns out that the magnetic susceptibility value of the 100-hour Ball Milling results increased significantly when compared to the magnetic susceptibility before Ball Milling, 968,245x 10−5 becomes 19.471x 10−5. The results of the X-Ray Fluorescence (XRF) test showed that the percentage of Fe milled increased from 1.669% to 35.187%, the particle size obtained from the scanning electron microscope (SEM) results was in the nanometer order of 78 nm and the X-Ray Difractometer (XRD) results.) shows that the magnetic nanoparticles produced are dominated by the hematite phase (α-Fe2O3) and the others are in the magnetite (Fe3O4) phase..