Carbon nanotubes are fascinating electronic material with unique physical properties and many important potential applications. Due to various applications of CNTs it is necessary to develop new methods for the synthesis of CNTS. In this chemical method, complexes of transition metal Co (II) with amino acid present in egg albumin have been synthesized. The complex so formed, is analyzed on the basis of spectroscopic method using, IR and NMR spectra confirms the lysine cobalt metal ion complex. The lysine cobalt metal ion complex is decomposed at higher temperature using muffle furnace to get metal carbon nanotubes. These metal carbon nanotubes are characterized using scanning probe instruments like AFM and DLS and X- RD.