Mapping the intensity distribution across a radiation beam by means of photographic film is convenient and inexpensive, but the question of accuracy of this method requires investigation. An experiment was carried out at the National Bureau of Standards to examine, with film, the uniformity of some of the x- and γ-ray beams used in calibration work. By exercising certain precautions in film selection, positioning, processing, and photometric measurement, it was possible to determine the relative intensity of radiation across the beams with an accuracy of 1 per cent. A commercial x-ray film type was chosen, which, when exposed to Co60 γ-radiation and, for maximum contrast, processed for twice the prescribed time in a commercial x-ray developer, showed a fog density level of only 0.11 and a linear response up to a density level of 3.5, within the accuracy of the photometric readings. This film was available in 14 × 17-inch size, in individual envelopes with center position and orientation marked on the outside for easy and accurate positioning. During the exposure, the film was held rigidly between layers of plastic, thick enough for electronic equilibrium, in a plane perpendicular to the central ray of the beam. All other supporting materials were kept outside the beam, to avoid errors due to radiation scattering. Commercial x-ray developer was used for processing for ten minutes at 20° C. and, with vigorous, random, manual agitation, produced highly uniform densities on the large sheets of film. Certain photographic artefacts were avoided by using fresh developer, stop bath, and fixer, and by thorough washing and uniform drying. For the photometric measurement, a photoelectric densitometer was used, whose inherent accuracy over a density range from 0 to 5.00 was within 0.02 density units. Readings over a relatively narrow spread of densities were found to be reproducible within the reading accuracy that was limited by the resolution of the densitometer scale. With this procedure, relative intensity readings at any one point on several film sheets, exposed identically at a 1-meter distance in a Co60 γ-ray beam and processed in various orientations in the developer, showed agreement within 0.5 per cent. A plot of the intensity distribution for one direction across the beam is shown in Figure 1, A. The points represent average readings at the various positions on three different film sheets. More than 400 densitometric readings over a central area of 8 × 8 cm. of the exposed films showed a root mean square deviation of 0.7 per cent. This is within the 1 per cent accuracy limit of the photographic method. For this particular beam, only beyond a distance of 10 cm. from the center did the intensity decrease by a statistically significant value.