Cladding Modes Research Articles

Femtosecond Laser-Inscribed Cladding Mode Small-Period Long-Period Fiber Gratings for Temperature and Strain Sensing

Femtosecond Laser-Inscribed Cladding Mode Small-Period Long-Period Fiber Gratings for Temperature and Strain Sensing

An Mach-Zehnder Interferometer Refractive Index Sensor Based on Self-phase Modulation Effect in a Tapered Double-cladding Highly Nonlinear Fiber

An Mach-Zehnder interferometer (MZI) sensor based on self-phase modulation (SPM) effect in a tapered double-cladding highly nonlinear fiber (DCHNLF) was proposed and experimentally verified for refractive index (RI) measurement. The DCHNLF was tapered and the SPM spectrum generated in its untapered region acted as the broadband light source for the sensor. The integration of the SPM effect and the RI detection not only simplified the structure of the sensor, but also enhanced its long-term stability and reliability. Since the effective RI of the outer cladding mode of the tapered DCHNLF was affected by the RI variation, a spectral shift would occur in interference spectrum between the core mode and the outer cladding mode. The tapering treatment enhanced the evanescent wave on the surface of DCHNLF, making the sensor more sensitive to external RI. In the external RI range of 1.3333 ~ 1.3972, the sensor achieved an excellent sensitivity of 238.51nm/RIU. In addition, the effect of average pump power and pump wavelength on the sensor performance were experimentally discussed. The results showed that the sensitivity was not affected by the pump condition. This MZI RI sensor has advantages of excellent performance, simple structure and easy fabrication, demonstrating broad application prospects in biomedical research, marine environment monitoring, and human health detection.

Unraveling Plasmonic Tilted Fiber Bragg Gratings (TFBG): A Journey From “Anomalous Resonances” to Refined Refractometry

AbstractPlasmonic tilted fiber Bragg gratings (TFBGs) have emerged as versatile tools for refractometric analyses and biochemical sensing. Their applications have significantly blossomed these last years, from proteins and cellular bioassays to operando monitoring in batteries, to cite just a few. They are widely recognized for their cutting‐edge performance and low limits of detection, arising from their dense multimodal spectral nature featuring tens of narrowband cladding mode resonances. Their comb‐like spectrum is so rich that numerous demodulation techniques have been reported, without benchmark of their relative performance while they possess important distinctions. This review highlights developments in detangling techniques from the pioneering works based on single‐peak analysis up to the most recent approaches involving Fourier analysis, the implementation of machine learning, and cascaded spectral decomposition processes. To fairly compare the different techniques of the literature, we implemented each analysis on original experimental refractometric calibrations, revealing the assets of the most updated methods. This paper therefore reviews these demodulation techniques based on the same datasets, obtained under the same conditions. We show and discuss the results obtained from bioassays and pinpoint the importance of advanced analytical methodologies to maximize the reproducibility, reliability and performance of plasmonic‐based TFBGs biosensors.

Real-time optical fibre near-infrared chromatic dispersion analyser using collocated optical fibre gratings

We present what we believe to be a novel optical fibre device for real-time measurements of near-infrared chromatic dispersion of a liquid medium from 1100 nm to 1700 nm. This inline optical fibre chromatic dispersion analyser is based upon collocated fibre long-period gratings written adjacently in the core by femtosecond laser inscription yielding 8 attenuation bands associated with different cladding modes, yielding 8 independent measurements. This fibre device is tested on a series of chemical compounds associated with wines. The results for each compound yielded distinctive chromatic responses. A machine learning pipeline was developed that successfully clustered and classified spectral responses of the different chemicals to illustrate the distinctive responses. The limits of detection for these fibre devices ranged from 1×10−3 to 6×10−5 mol/L for the compounds associated with wines, demonstrating the potential usefulness of an optical fibre chromatic dispersion analyser is capable of monitoring in real-time effective chromatic dispersion that is not offered by any current technology.

Michelson interferometer based on a fiber with a germanium-doped core and inner cladding for high-temperature sensing

We proposed and demonstrated a temperature sensor based on a fiber Michelson interferometer. The Michelson Interferometer contains a special fiber with a germanium-doped core and pure silica inner cladding, so the interference spectrum is formed as a result of interference of the mode of the core and one of the modes of the inner cladding. The existence of inner cladding reduces the number of interacting cladding modes. When annealing the sensor for 300 min at a temperature of 600 °C, no thermal hysteresis of the interference spectrum was observed. The temperature sensitivities of the proposed sensor are 48 pm/°C in the range of 20–250 °C and 78 pm/°C in the range of 250–600 °C. But when the sensor was exposed to a constant temperature of 700 °C and above for a few hours, a shift in the wavelength of the dip of the interference spectrum is observed. This wavelength shift, which occurs even at a fixed temperature, depends on the temperature of annealing. It can be explained by a number of processes occurring in glass at high temperatures: the changing fictive temperature of the glass, diffusion of germanium oxide from the core, and formation of mechanical stresses resulting from the difference in thermal expansion coefficients of the core and cladding, and relaxation of these mechanical stresses at an elevated temperature.

Highly sensitive threaded LPFG strain sensor

Long Period Fiber Grating (LPFG) strain sensors have been used to monitor the structural health of bridges and buildings, and there is a need to further improve their sensing sensitivity. This article proposed a threaded LPFG strain sensor, which used a CO2 laser to etch a long groove at the top of the cladding of a single-mode fiber. The fiber in the long groove area was heated and twisted to fabricate a long period fiber grating (TH-LPFG) strain sensor with a threaded groove on the cladding. When strain is applied, the strain is concentrated in the threaded area on the cladding, increasing and decreasing the effective refractive index changes of the cladding mode and core mode respectively, achieving enhanced strain sensing. The experimental outcomes demonstrate that the TH-LPFG strain sensor achieves a sensitivity of 44.9 pm/µε to strain, while its cross-sensitivity to temperature is minimal, at just 1.28 µε/°C. TH-LPFG provides a new solution for enhancing the sensitivity of LPFG strain sensing, with low production cost and low temperature crosstalk. It can be used in the field of highly sensitive strain monitoring of building structures.

Balloon-Shaped SMF Blood Glucose Concentration and Temperature Sensor Based on Core-Offset Structure

A blood glucose concentration and temperature sensor with a balloon-shaped single-mode fiber (SMF) based on a core-offset structure is proposed and experimentally demonstrated. The balloon-shaped SMF is created by offset-fusing a straight-line SMF between two other SMFs, thereby forming a Mach–Zehnder interferometer (MZI). The core-offset structure can effectively excite higher-order cladding modes. The experimental results showed that the maximum sensitivity of blood glucose concentration was 0.331 nm/(mmol/l) and the maximum sensitivity of temperature was 0.216 nm/°C when the offset distance was 10 μm. Dual-parameter measurement was achieved through a dual-parameter matrix. In addition, the sensor has characteristics such as simple structure, low cost, good stability, and electromagnetic interference resistance, making it potentially valuable for diagnosing high blood glucose and related conditions.

An asymmetric STNS-MZI structure and its applications in temperature and Cd2+ monitoring

In this paper, an asymmetric fiber Mach-Zehnder interferometer (MZI) is presented and investigated. The proposed asymmetric MZI structure is mainly constructed with thin core fiber (TCF) and no core fiber (NCF), sandwiched between single mode fibers (SMFs). Note that the TCF is spliced with a slight offset such that higher order cladding modes could be effectively exited. The SMF-TCF-NCF-SMF (STNS) structure is adjusted by a finite-difference beam propagation method simulation to achieve an optimal interference spectrum. Temperature monitoring performance is addressed and the calculated sensing resolution is about 0.28℃ with high precision of ± 0.3 °C. Moreover, as for the Cd2+ monitoring application, the TCF is further etched and then coated with 1-allyl-2-thiourea (ATU) forming cross-linked “-S-Cd-S-” structure. The results show that the resolution of Cd2+ could reach 2.37 × 10−11mol /L, which shows a four order of magnitude improvement compared with our previous work. Therefore, the proposed asymmetric STNS-MZI interference structure has great potential in future applications.

Detection of riboflavin concentration by sol-gel silica coated dual-peak long period fiber grating sensor

A dual-peak long period fiber grating (DP-LPFG)-based sensor was designed and fabricated for the sensitive detection of riboflavin concentration. LPFGs with a period of 163 μm and a cladding mode of LP0, 12 were inscribed on a standard single-mode silica fiber using a femtosecond laser direct writing technique. Coatings of silica-based materials doped with β-cyclodextrin (β-CD), prepared via the sol-gel method, were applied to the surface of the LPFGs for the detection of riboflavin. To investigate the impact of coating thickness on the sensing sensitivity, sol-gel coatings of different thicknesses were applied to the surface of the LPFG sensor. Experimental findings revealed that the sensor with a thickness of approximately 540 nm sol-gel coatings exhibited superior sensing performance. The detection limit of the prepared DP-LPFG sensor was tested to be 0.08 nM, and it exhibits a response time of less than 3 minutes, along with high sensitivity, excellent repeatability, and selectivity. Thus, this sensor holds significant promise for applications in disease treatment and diagnosis, as well as in ensuring food quality.

Cascaded dual-parameter SPR fiber sensor for RI and pH simultaneous detection based on Ag film and an Ag/self-assembled nanofilm structure

To achieve more accurate analysis and detection of changes in liquid parameters, we propose a dual-parameter surface plasmon resonance (SPR) sensor that can measure refractive index (RI) and pH simultaneously. In this paper, we compare and analyze the transmission spectrum when the SPR effect is excited by the cladding mode of a photonic crystal fiber (PCF) and the core mode of the no-core fiber. The results show that the SPR effect excited using the cladding mode is stronger and the sensor has better loss peaks, which is more conducive to realizing the detection of the external environment. Therefore, the sensor uses PCF as the substrate and utilizes a cascade composite film structure, and the area where a silver film is deposited on the surface of the PCF is selected as the RI sensing area. Another part of the PCF, after the silver film is deposited, uses a high-sensitivity polyacrylic acid/chitosan self-assembled nanofilm as the pH-sensitive film. Experimental results show that the maximum sensitivity is 4122.44 nm/RIU and -57.82 nm/pH when the RI range is between 1.333 and 1.385 and the pH range is between 3.11 and 8.63, respectively. In addition, we experimentally verified that the sensor had good stability and repeatability. The design of the sensor provides new possibilities for real-time monitoring and precise control, helping to advance scientific research and the development of industry.

Birefringence Free Spectral Tuning of Bragg Grating Based Fabry-Pérot Resonator in LiNbO₃ Waveguide Employing Counter- Propagating Cladding Modes

Birefringence Free Spectral Tuning of Bragg Grating Based Fabry-Pérot Resonator in LiNbO₃ Waveguide Employing Counter- Propagating Cladding Modes

Application of Gabor, Log-Gabor, and Adaptive Gabor Filters in Determining the Cut-Off Wavelength Shift of TFBG Sensors

Tilted fibre Bragg gratings are optical fibre structures used as sensors of various physical quantities. Their unique measurement capabilities result from the high complexity of the optical spectrum consisting of several dozen cladding mode resonances. TFBG spectra demodulation methods generate signal features that highlight changes in the spectrum due to changes in the interacting quantities. Such methods should enable the distinction between two slightly different values of the measured quantity. The paper presents an effective method of processing the TFBG spectrum for use in measuring the refractive index of liquids. The use of Gabor and log-Gabor filters and their adaptive version eliminates the problem of discontinuity in determining the SRI value related to the existence of the cladding mode comb. The Gabor filters used make visible the shifting and fading of spectral features related to the decrease in the intensity of leaking modes. Subsequent modifications of the proposed algorithm led to an increase in the quality factor of the processed spectrum.

Femtosecond laser direct writing annular small-period long-period fiber gratings for simultaneous refractive index and temperature sensing.

A new type of small-period long-period fiber grating (SP-LPFG) consisting of a series of annuli inscribed by a femtosecond laser in a single-mode fiber is proposed and demonstrated. The effects of the annuli radii and the number of annuli in each period on the transmission spectrum are studied. The transmission spectrum of the annular SP-LPFG exhibits both strong Bragg resonances and cladding mode resonances, which have similar temperature sensitivities of 9.26 and 9.75 pm/°C, respectively. The Bragg resonances are insensitive to the change of environment refractive index (RI), while the cladding mode resonances show a RI sensitivity of 141.89 nm/RIU. The proposed sensor offers a potential solution for biomolecular sensing applications by effectively eliminating the issue of temperature cross-sensitivity. Its compact design and ease of spectral acquisition enhance its practicality and convenience.

A large-dynamic range conductivity-modulated PANI online analysis and sensing platform for ammonia gas detection using coupled optical probing mode

Due to the large-dynamic range and reversible conductivity modulation capability, polyaniline (PANI) shows promising prospects for diverse applications, such as supercapacitors, rechargeable batteries, and electrochromic materials. However, online characterization of the optical properties of the conductive polymer in the infrared band throughout the synthesis and redox state changing processes poses a challenge. Here, we propose and demonstrate an analysis and sensing platform for real-time evaluation of both thickness and the complex refractive index of PANI nanofilm, and employed for ammonia gas concentration sensing. The coupled optical probing mode of tilted fiber Bragg grating (TFBG) as a robust and portable permittivity perception tool is utilized for online perceiving the large-dynamic-range conductivity change of PANI nanofilm. By reproducing the spectral evolution of the probing cladding mode resonance, we introduce a simulation method for analyzing the optical properties of polymer nanofilms within the infrared band. For ammonia gas detection, the sensing platform exhibited continuous and reliable detection within a concentration range of 25–500 ppm, with an optimal film thickness of 156 nm. A good linear response was observed with a sensitivity of up to 5.2 × 10−3 dB/ppm, and a linearity (R2 = 0.9876) with a detection limit of 10 ppm. Our proposed low-cost and large dynamic range conductivity-modulated PANI-TFBG platform for optical properties online analysis and sensing shows potential in environmental monitoring, healthcare, and the biochemical field.

High-sensitive glucose sensor based on tilted fiber Bragg gratings

In this paper, we proposed a high-sensitive glucose sensor using the tilted fiber Bragg gratings (TFBGs). The TFBGs with different tilt angle has been fabricated by phase mask scanning method with an argon ion double-frequency 244 nm laser. As tilt angle increases, the bandwidth of the cladding mode excited by TFBGs gradually expands and cladding mode region shifts towards shorter wavelengths. The higher-order cladding modes appeared at the shorter wavelength side demonstrate a larger separation in the spectrum. TFBGs with different tilt angles for glucose concentration measurement have been investigated experimentally. When the concentration of glucose solution increases, the surrounding refractive index changing make the cut-off mode resonance shift to a longer wavelength. In addition, the tilt angle of TFBGs does affect the glucose sensitivity, that the larger tilt angle is, the higher sensitivity could achieve. In this work, a maximum glucose sensitivity of 80.91 pm/(mg/ml) could be obtained for TFBGs with tilt angle of 10°. The proposed TFBGs with superiorities of high glucose sensitivity and wider detection range, makes it potential for glucose detection in the field of chemical and biomedical sensing.

Highly Sensitive Optical Fiber MZI Sensor for Specific Detection of Trace Pb2+ Ion Concentration

A novel chitosan (CS) functionalized optical fiber sensor with a bullet-shaped hollow cavity was proposed in this work for the trace concentration of Pb2+ ion detection in the water environment. The sensor is an optical fiber Mach–Zehnder interferometer (MZI), which consists of a sequentially spliced bullet-shaped hollow-core fiber (HCF), thin-core fiber, and another piece of spliced bullet-shaped HCF. The hollow-core fiber is caused to collapse by adjusting the amount of discharge to form a tapered hollow cavity with asymmetric end faces. The bullet-like hollow cavities act as beam expanders and couplers for optical fiber sensors, which were symmetrically spliced at both ends of a section of thin core fiber. The simulation and experiments show that the bullet-like hollow-core tapered cavity excites more cladding modes and is more sensitive to variation in the external environment than the planar and spherical cavities. The ion-imprinted chitosan (IIP-CS) film was fabricated with Pb2+ ion as a template and uniformly coated on the surface for specific recognition of Pb2+. Experimental verification confirms that the developed sensor can achieve high-sensitivity Pb2+ ion detection, with a sensitivity of up to −12.68 pm/ppm and a minimum Pb2+ ion detection concentration of 5.44 ppb Meanwhile, the sensor shows excellent selectivity, repeatability, and stability in the ion detection process, which has huge potential in the direction of heavy metal ion detection in the future.

A high Q-factor evanescent field fiber sensor coated with C-MWCNT for label-free HPV determination

A high Q-factor evanescent field fiber sensor is designed based on a fiber Bragg grating (FBG) coated with carboxylic multi-walled carbon nanotubes (C-MWCNT). In a high-reflectivity FBG, multiple cladding modes are stimulated as the forward-moving guided mode within the core of the multimode fiber is coupled to the FBG’s reverse-moving guided mode within the cladding. Our evanescent field fiber sensor is highly sensitive to the refractive index without altering the architecture of fiber or deviating from the conventional process of fabricating fiber gratings. The proposed sensor exhibits a full-width at half maximum (FWHM) of 78 pm and a Q-factor of 1.9 × 104 for its standard cladding-mode resonance, outperforming the majority of reported evanescent field fiber sensors in these parameters. Furthermore, by coating C-MWCNT on the fiber sensing surface, our sensor has been demonstrated to combine multiple functions into one, such as label-free determination of human papilloma virus (HPV) DNA sequences, the measurement of different concentrations, and mispairing discrimination. The sensor design put forward offers a compelling technique within the realm of optical fiber sensing for refractive index and label-free biomolecule detection.

High sensitivity strain and refractive index MZI-SPR sensing based on dual fiber winding structure.

Fiber strain and refractive index dual parameter sensor have enormous potential in the field of underwater structural health monitoring. This article proposes a strain and refractive index highly sensitive MZI-SPR composite sensor based on a dual fiber winding structure. By twisting single-mode fiber and multi-mode fiber, the two fibers are wound together to produce regular multiple bends. Among them, single-mode fiber achieves beam splitting and coupling of light during the first bending and the end of bending, forming a double beam interference MZI. The multi bending structure excites high-order cladding mode to achieve highly sensitive strain sensing. Meanwhile, multi-mode fiber excites cladding mode at the bending point and generate surface plasmon resonance effect, forming a cladding type SPR sensor. By controlling the winding parameters, the bending curvature is controlled, further controlling the SPR incidence angle and achieving highly sensitive refractive index sensing. The experiment indicates that the sensor can achieve simultaneous detection of strain and refractive index, and its sensitivity can reach 33pm/ µε and 4386.262 nm/RIU, respectively. The proposed MZI-SPR composite dual parameter sensor has a stable structure and high sensitivity, providing a reliable solution for simultaneously measuring strain and refractive index in the field.

Restoration of high-pressure turbine blade combs using a concentrated energy flow

A useful model of temperature distribution in the deposited layer of ВЖ159 powder and in the zone of its connection with the base material — ЖС6У alloy, during laser cladding is developed. The optimal modes of laser cladding of powder onto alloy blades are determined. The properties of the deposited layer and the quality of its bonding with the base material are studied. It is shown that there are no defects such as pores, cracks and discontinuities in the deposited layer and the interface zone. Keywords:restoration, laser cladding, blades, high-pressure turbine, temperature distribution, microstructure, microhardness, X-ray spectral microanalysis

Tilted Bragg grating in a glycerol-infiltrated specialty optical fiber for temperature and strain measurements.

In this Letter, we propose an in-line tilted fiber Bragg grating sensor for temperature and strain measurements. The grating is inscribed in a specialty optical fiber using tightly focused femtosecond laser pulses and the line-by-line direct writing method. Beside the central core in which the grating is produced, a hollow channel filled with glycerol aqueous solution significantly improves the sensitivity of the fiber cladding modes due to its high thermo-optic coefficient. We show that the temperature sensitivity of the core mode is 9.8 pm/°C, while the one of the cladding modes is strongly altered and can reach -24.3 pm/°C, in the investigated range of 20-40°C. For the strain measurement, sensitivities of the core mode and the cladding modes are similar (∼0.60 pm/με) between 0 and 2400 με. The significative difference of temperature sensitivity between the two modes facilitates the discrimination of the dual parameters in simultaneous measurements.