ABSTRACT The high-pressure flash pipeline of coal coke gasification leaked within one week after the operation. Further macroscopic observation showed that cracks appeared in the base material area near the weld. The medium transported by the pipe was low-concentration acid gas. Visual inspection, tensile testing, impact testing, chemical composition analysis, metallographic analysis, energy dispersive spectroscopy, X-ray diffraction analysis, and electron backscattering diffraction analysis were used to reveal the sources of cracks in the pipeline. It was found that the cracks were intergranular and filled with corrosion products. The chemical composition of the corrosion products is rich in Cr, S, and O. After the crack was opened, fracture features of ‘rock candy’ were observed, exhibiting brittle fracture characteristics. The cracks were caused by hydrogen-induced cracking along the grain boundary. On this basis, suggestions and countermeasures were put forward for the failure of the high-pressure flash gas pipeline.
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