Based on previous experience, an optical particle counter has been designed which allows the direct measurement of the size and concentration of dust particles in gas flows at high temperatures. The instrument features a new optical measuring volume definition together with a signal control to avoid border-zone error effects. The instrument has a free working distance of 200 mm. Hence it is possible to make true in situ measurements in pipe flows with a cross-section of ca. 60 cm2 and additionally to protect the device against heat and dust precipitation on the optical windows. The instrument was initially used to examine the separation behaviour of cake-forming rigid ceramic barrier filters at temperatures up to 1000 °C. In particular, the fractional efficiencies and the time-related concentration changes on the clean gas side caused by a pulse jet cleaning event could be determined. The results obtained so far demonstrate that ceramic barrier filters show basically the same behaviour as conventional filters, but possess a substantially higher separation efficiency at a corresponding higher pressure drop (fractional penetration values between 10−5 and 10−9 depending on the type of filter material and the cake formation).