Cement Film Thickness Research Articles

The Effect of the Initiator/Activator/Accelerator Ratio on the Degree of Conversion, Film Thickness, Flow, and Cytotoxicity of Dual-Cured Self-Adhesive Resin Cements.

Although self-adhesive resin cements are convenient and less technique-sensitive materials for dental clinicians, they exhibit a lower degree of conversion due to acidic components in their composition. Supplementation of the initiator, accelerator, and activator in self-adhesive resin cements has been suggested to compensate for the lower degree of conversion. This study aimed to evaluate the effects of different combinations of self-curing initiators, self-curing activators, and accelerators on the degree of conversion (DC) of self-adhesive resin cements. A dual-cured self-adhesive resin was prepared using six combinations of initiators, activators, and accelerators. The change in the DC over time was evaluated with and without light curing. The film thickness, flow properties, and cytotoxicity of each formulation were assessed. The results showed that all supplemental components had an effect on increasing the DC, but a greater increase in the DC was observed in the following order: activator, accelerator, and initiator. The cytotoxicity of the resin cements was related to the DC values, as resin cements with lower DC values exhibited higher cytotoxicity. The film thickness met the ISO standards for all groups. The results suggest that utilizing an activator is the most effective approach to enhance the DC in self-adhesive resin cement and that cytotoxicity tended to increase with lower DC values, whereas film thickness and flow properties demonstrated no correlation with DC values.

Effect of Self-Adhesive Resin Cement Film Thickness on the Shear Bond Strength of Lithium Disilicate Ceramic–Cement–Tooth Triplex

Cement film thickness may have an impact on the shear bond strength (SBS) of lithium disilicate dental ceramics luted to human enamel with resin cement. The objective of this study was to evaluate SBS of lithium disilicate ceramics adhered to enamel using resin cement at different thicknesses. In total, 50 ceramic specimens (3 × 3 × 3 mm) and 50 premolar teeth were prepared and randomly assigned to 5 groups (n = 10 each). Ceramic specimens were designed with five cement film thicknesses (50 μm; 100 μm; 150 μm; 200 μm; and 300 μm). Teeth surfaces (4 × 4 mm) were prepared with a high-speed handpiece mounted on a dental surveyor. Ceramic specimens were cemented to teeth with resin cement (3MTM RelyXTM U200, Resin-Self-Adhesive-Cement). The specimens were then thermocycled for 6000 cycles with a 30 s dwell time and a 5 s transfer time in water (5 °C and 55 °C). A Universal-Testing-Machine was used to measure SBS (MPa). Statistical analysis in SPSS included Anova and Tukey’s tests. The SBSs of ceramics adhered to teeth revealed significantly different values across all test groups (p = 0.000). The findings showed that as cement layer thickness increased, so did the SBS. The cement spaces at 50 and 300 μm had the lowest SBS (9.40 + 1.15 MPa) and maximum SBS (21.98 + 1.27 MPa), respectively. The SBS of the lithium disilicate ceramic luted to natural human enamel increased along with the cement layer thickness.

Using Functionalized Micron-Sized Glass Fibres for the Synergistic Effect of Glass Ionomer on Luting Material.

This laboratory experiment was conducted with the objective of augmenting the mechanical properties of glass ionomer cement (GIC) via altering the composition of GIC luting powder through the introduction of micron-sized silanized glass fibres (GFs). Experimental GICs were prepared through the addition of two concentrations of GFs (0.5% and 1.0% by weight) to the powder of commercially available GIC luting materials. The effect of GF in set GIC was internally evaluated using micro-CT while the mechanical attributes such as nano hardness (nH), elastic modulus (EM), compressive strength (CS), and diametral tensile strength (DTS) were gauged. Additionally, the physical properties such as water solubility and sorption, contact angle (CA), and film thickness were evaluated. Reinforced Ketac Cem Radiopaque (KCR) GIC with 0.5 wt.% GF achieved improved nH, EM, CS, and DTS without affecting the film thickness, CA or internal porosity of the set GIC cement. In contrast, both GF-GIC formulations of Medicem (MC) GIC showed the detrimental effect of the GF incorporation. Reinforcing KCR GIC with 0.5 wt.% silanized GFs could improve the physical and mechanical attributes of luting material. Silanized GF, with optimal concentration within the GIC powder, can be used as a functional additive in KCR GIC with promising results.

Effect of degree of conversion on the surface properties of polymerized resin cements used for luting glass fiber posts

Statement of problemLack of conversion of resin cements for luting glass fiber posts in deeper levels of the root canal may compromise clinical performance. PurposeThe purpose of this in vitro study was to evaluate the effect of the degree of conversion on the surface properties of dual-polymerized resin cements used for cemented glass fiber posts according to the root level. Material and methodsFifty maxillary central incisor teeth were endodontically treated, and glass fiber posts were cemented using the following systems: self-adhesive dual-polymerized resin luting cement (RelyX U200) and dual-polymerizing flowable core and a post luting system (Rebilda DC) with a self-etching adhesive (Futurabond DC). The degree of conversion was determined via attenuated total reflectance and Fourier transform infrared spectroscopy, and surface microhardness and cement film thickness were measured. The intraradicular fit was evaluated with microscopy. All tests were performed in the coronal, middle, and apical third of the root canal. Statistical analysis was done with ANOVA and the multiple comparison Tukey test (α=.05). ResultsThe degree of conversion was higher in the coronal third using Rebilda DC (65.3 ±4.8%) than RelyX U200 (38.7 ±5.3%) (P<.05); on both resin cements, these values decreased from the coronal to the apical third (30.9 ±3.7%, 61.9 ±8.7%, respectively). The cement film thickness was higher for RelyX U200 in the 3 thirds than for Rebilda DC; significant differences (P<.05) were recorded in both cementing systems in the coronal and apical thirds. In the middle third, no significant differences were observed (P>.05). The mean surface microhardness values increased in the coronal thirds and decreased with increasing root canal depth. The marginal seal in the coronal thirds and the intraradicular fit in the middle thirds showed closer adaptation; however, some tags were observed in the interface resin cement and radicular dentin. Gap and tag formations were observed in the apical third. ConclusionsDepending on the root canal third, the surface properties of dual-polymerized resin cements are influenced by the degree of conversion.

Effect of cement film thickness on the microshear bond strength of CAD/CAM lithium disilicate bonded to cervical and mid-coronal enamel

Effect of cement film thickness on the microshear bond strength of CAD/CAM lithium disilicate bonded to cervical and mid-coronal enamel

Effect of Luting Cement Film Thickness on the Pull-Out Bond Strength of Endodontic Post Systems.

Optimal bond strength between the prefabricated post/dowel to the surrounding dentin is essential. The present study aimed to analyze and compare the effect of three different cement film thicknesses on the pull-out bond strength of three different prefabricated post systems. Extracted natural teeth (N = 90) with similar root dimensions were acquired. Teeth were mounted in resin blocks, endodontically treated, sectioned at cemento-enamel junction, divided into three groups (A: Parapost Fiber Lux plus; B: 3M ESPE Relyx fiber post; and C: Parapost XP), and stored. Uniform post spaces were prepared for the groups (A and C: Length = 8 mm, Width = 1.5 mm; B: Length = 8 mm, Width = 1.6 mm). Each group (N = 30) was further subdivided into three subgroups (n = 10) based on the size (4, 5, and 6) of the post and cemented with resin cement (MultiLink-N, Ivoclar Vivadent). After thermocycling, the specimens were subjected to a pull-out test using a universal testing machine, and tensile force was recorded (MPa). Digital microscopic evaluations were performed for modes of failure. ANOVA and Tukey-HSD tests were used for statistics. Significant differences were observed for each tested material (p = 0.000). The lowest and highest bond strength values were recorded for Group C (Titanium post) and Group A (000), respectively. Multiple comparisons showed significance (p < 0.05) among all the groups, except for space 1 and space 2 (p = 0.316) for Group A. Most of the failures occurred within the cement-dentin and post-cement interface (Adhesive failures, 73.5%). An increase in the luting cement film thickness results in the decrease in pull-out bond strength of prefabricated posts luted with resin cement, irrespective of the type/material/shape of the post. The serrated fiber posts showed the highest pull-out bond strength compared to the smooth surfaced fiber posts or serrated metal posts. Increased pull-out bond strengths were observed when appropriate post space was created with the same sized drill as the post size.

The influence of the resin-based cement layer on ceramic-dentin bond strength.

The purpose of the study was to measure the cement thickness obtained when ceramic rods were luted to dentin and to analyze the relation between cement thickness and the previously published tensile bond strength of similar test specimens. In addition, the ISO standard 4049:2019 method was used to determine the film thickness of the used cements. Zirconia (n=100) and lithium disilicate (n=50) rods were cemented to bovine dentin using one of five different resin-based cements. The ceramic-dentin test specimens were cut into two slices and the cement thickness was measured using a scanning electron microscope and compared to the bond strength values of similar specimens already published. The mean cement thickness recorded for ceramic rods cemented to dentin was in the range 20-40μm, which was larger than the cement film thickness found by the ISO method. The cement film thickness determined according to ISO standard methods did not concur with the results obtained when cementing ceramic rods to dentin. For cementing ceramic restorations, a cement thickness in the range 25-35μm seems to be favorable for the bond strength.

Shear Bond Strength and Film Thickness of a Naturally Antimicrobial Modified Dental Luting Cement.

Although several natural plants and mixtures have been known and used over the centuries for their antibacterial activity, few have been thoroughly explored in the field of dentistry. Thus, the aim of this study was to enhance the antimicrobial activity of a conventional glass ionomer cement (GIC) with natural plant extracts. The effect of this alteration on the bond strength and film thickness of glass ionomer cement was evaluated and related to an 0.5% chlorohexidine modified GIC. Olive leaves (Olea europaea), Fig tree (Ficus carica), and the leaves and roots of Miswak (Salvadora persica) were used to prepare an alcoholic extract mixture. The prepared extract mixture after the evaporation of the solvent was used to modify a freeze-dried glass ionomer cement at three different extracts: water mass ratios 1:2, 1:1, and 2:1. An 0.5% chlorhexidine diacetate powder was added to a conventional GIC for the preparation of a positive control group (CHX-GIC) for comparison. The bond strength to dentine was assessed using a material-testing machine at a cross head speed of 0.5 mm/min. Failure mode was analyzed using a stereomicroscope at 12× magnification. The cement film thickness was evaluated in accordance with ISO standard 9917-1. The minimum number of samples in each group was n = 10. Statistical analysis was performed using a Kruskal–Wallis test followed by Dunn’s post hoc test for pairwise comparison. There was a statistically insignificant difference between the median shear bond strength (p = 0.046) of the control group (M = 3.4 MPa), and each of the CHX-GIC (M = 1.7 MPa), and the three plant modified groups of 1:2, 1:1, 2:1 (M = 5.1, 3.2, and 4.3 MPa, respectively). The CHX-GIC group showed statistically significant lower median values compared to the three plant-modified groups. Mixed and cohesive failure modes were predominant among all the tested groups. All the tested groups (p < 0.001) met the ISO standard of having less than 25 µm film thickness, with the 2:1 group (M = 24 µm) being statistically the highest among all the other groups. The plant extracts did not alter either the shear bond strength or the film thickness of the GIC and thus might represent a promising additive to GICs.

Effect of half-digital workflows on the adaptation of custom CAD-CAM composite post-and-cores

Statement of problemEven without the use of an intraoral scanner, post-and-cores can be obtained by using a part-digital fabrication workflow that requires pattern modeling (direct, indirect, or impression); however, studies on the adaptation of computer-aided design and computer-aided manufacturing (CAD-CAM) composite resin post-and-cores in comparison with metal cast post-and-cores are sparse. PurposeThe purpose of this in vitro study was to analyze the adaptation of CAD-CAM composite resin post-and-cores fabricated through a part-digital fabrication workflow and to compare it with that of metal cast post-and-cores fabricated through conventional methods. Method and materialsEight extracted human premolars were endodontically treated and prepared for custom post-and-cores. Metal cast post-and-cores were fabricated with Ni-Cr alloy (Fit Cast-Sb Plus; Talmax) and conventional resin pattern modeling methods directly in the root canal (conventional direct modeling) or indirectly in a stone cast (conventional indirect modeling). Composite resin post-and-cores were milled from nanohybrid glass-ceramic composite resin CAD-CAM blocks (Brava Block; FGM) by using the part-digital workflow. A laboratory scanner was used to digitalize polyvinyl siloxane impressions (part-digital scanned impression direct CAD-CAM [PSC]) of the root canals and resin patterns fabricated directly (part-digital direct CAD-CAM [PDC]) or indirectly (part-digital indirect CAD-CAM [PIC]). All post-and-cores were placed in the respectively prepared root canals, scanned with microcomputed tomography, and measured in terms of volume of the cementation space, the luting cement film thickness in each root third, and the apical gap between the apical end of the post-and-cores and remaining gutta percha (apical gap). The groups were compared for each adaptation parameter by using 2-way (volume of the cementation space and apical gap) and 3-way (film thickness) ANOVA, and the Games-Howell multicomparison post hoc test (α=.05). ResultsThe conventional direct modeling group had lower mean volume of the cementation space than all CAD-CAM composite resin post-and-cores (P<.041). The conventional indirect modeling group had a lower volume of the cementation space mean than PDC (P<.024) but was not significantly different from PIC (P=.577) or PSC (P=.221). Regardless of the fabrication workflow, no differences were observed among the CAD-CAM composite resin post-and-cores (P>.05). At the apical root third, conventional direct modeling and conventional indirect modeling had lower film thickness means than PSC or PDC (P<.05). In the middle third, conventional direct modeling and conventional indirect modeling had lower film thickness means than PDC (P≤.001). At the cervical third, no differences in film thickness means were observed among the groups (P>.05). PDC had a lower apical gap mean than PSC (P=.013), while no significant differences were found for other pair comparisons (P>.05). ConclusionsMetal post-and-cores had slightly better adaptation than the CAD-CAM composite resin post-and-cores; however, the part-digital fabrication workflow of CAD-CAM composite resin post-and-cores provided adaptation parameters within a clinically acceptable range and is less time consuming.

Comparative Evaluation and Correlation of Marginal Fit and Retention of Metal Copings Fabricated Using Two Different Designs of Die Spacerandndash; An In Vitro Study

Introduction: The art and science of fixed prosthodontics is predicted on accomplishing precise and clinically accurate operative techniques based on sound biological and mechanical principles. Many factors have been demonstrated to influence the marginal seating and retention of crowns, such as size and shape of the prepared teeth, manipulation of the cement, retentive properties of the cement, cement film thickness, relieving space or venting for cement, cement application, and roughness of the dentinal surface. Optimum retention form is considered to be one of the most important principles of tooth preparation. The longevity of fixed prosthesis depends on the retention and marginal integrity of restoration. This study was done to evaluate, compare and correlate the marginal fit and retention for two different designs of die spacer. Materials and Method: The samples to be studied were divided into 2 groups of 15 each. Each having a different die spacer design. Results: The results showed no significant difference in marginal fit of group Ia and group IIa and retention was better in group IIb compared to group Ib. But no statistically significant differences were seen when correlating the marginal fit and retention between group Ia, group Ib and group IIa and group IIb.

Microcomputed tomography evaluation of cement film thickness of veneers and crowns made with conventional and 3D printed provisional materials.

To evaluate, through microcomputed tomography (μCT), the cement film thickness of veneers and crowns made with different provisional materials. A veneer and a crown preparation were performed on a central incisor and a second molar of a dental model, respectively, scanned with an intraoral scanner, and the .stl files were exported to an LCD-based SLA three-dimensional (3D)-Printer. Twenty-four preparations were 3D-printed for each veneer and crown and divided into four groups (n = 6/group): (a) Acrylic resin (Acrílico Marche); (b) Bisacrylic resin (Protemp 4); (c) PMMA computer-aided design and computer-aided manufacturing (CAD-CAM) (Vipiblock); and (d) 3D-printed resin for provisional restorations (Raydent C&B for temporary crown and bridge). Veneers and crowns restorations were performed and cemented with a flowable composite. Each specimen was scanned with a μCT apparatus, files were imported for data analysis, and cement film thickness was quantitatively measured. Data were analyzed by 2-way ANOVA and Tukey post-hoc tests (α = .05). Crowns presented a thicker cementation film than veneers (P < .05).The bisacrylic resin showed the smallest veneer film thickness, similar to the acrylic resin (P = .151), which was not significantly different than the PMMA CAD/CAM material (P = .153). The 3D printed provisional material showed the thicker film, different than all other materials (P < .05). The bisacrylic resin showed a cement film thickness with a high number of voids in its surface. For crowns cementation, the 3D printed provisional material showed the thicker cementation film, different than all other materials (P < .05). Different provisional materials present different film thicknesses. The 3D printed provisional material showed the highest veneer and crown film thicknesses. Veneers film thicknesses were smaller than crowns for all provisional materials. The 3D printed provisional material studied can be satisfactorily used, presenting appropriate adaptation with the tooth preparation, however, it shows the highest cement film thickness for both veneers and crowns cementations when compared with other provisional materials. A better internal fit, or smaller cement film thickness is obtained by CAD/CAM materials, acrylic and bisacrylic resins. Veneer cementation showed a smaller cement film thickness compared with crown cementation for all provisional materials.

Evaluation of Film Thickness of Crown Disclosing Agents and Their Comparison with Cement Film Thickness after Final Cementation.

Objective Verification of the accuracy of crown fit before final cementation is imperative. The aim of this in vitro study was to evaluate the film thickness of commonly used dental crown disclosing materials and their comparison with final cement thickness. Materials and Methods One hundred fifty provisional crowns (Protemp) were fabricated on standardized resin dies and divided into five groups ( N = 150; n = 30) based on five disclosing agents: A = Fit-Checker auto-mix; B = Okklu-top; C = Express; D = Fit-Checker hand-mix; E = Coltene PSI, and Final cement = Relyx U200. Crowns were loaded with test materials, tried over dies under load (50N), and later cemented under same load. Film thickness (µm) was recorded between crown margin and the finish line of die after loading with test material and final cementation using a digital microscope. Statistical Analysis Descriptive statistics, analysis of variance, Tukey’s and paired t -test were used for statistical analysis ( p < 0.05). Results Significant variations were found between the film thicknesses of the five disclosing agents ( p = 0.019). Group-A showed the lowest (131.67 ± 101.10 μm), while group-B (295.00 ± 263.88 μm) showed the highest film thickness ( p = 0.011). Film thicknesses after cementation were similar for groups ( p = 0.957). Significant difference was observed for group-B disclosing agent versus final cement ( p = 0.010). The lowest mean difference between the film thicknesses of the disclosing agent and final cementation of 13.1 μm was revealed for group-A. Conclusions Variations in the film thicknesses of the tested disclosing agents were found. Fit-Checker auto-mix was found with minimal film thickness and satisfied the requirements as the disclosing agent, while Okklu-top aerosol spray did not.

Comparison of the film thickness of composites of different degrees of viscosity

The measurement of the film thickness of the composite cement Variolink Esthetic («Ivoclar-Vivadent», Liechtenstein) and the microhybrid composite Enamel («Micerium», Italy) was carried out according to ISO 4049: 2009 standards with a load force of 5 kg. While reducing the load force to 5 kg, all materials showed an increase in the film thickness; the film thickness of the Variolink Esthetic composite cement was changed from 23 microns (at 15 kg) to 32 microns (at 5 kg), and the film thickness of the microhybrid composite film Enamel was changed from 39 microns (at 15 kg) to 102 microns (at 5 kg). After preheating, the film thickness was changed from 23 microns (at 15 kg) to 44 microns (at 5 kg).

Impact of speed sintering on marginal discrepancy, internal fit and microleakage of monolithic zirconia crowns with different chamfer width

Purpose: The current in-vitro investigation analyzed the impact of speed sintering and different finish line width on marginal adaptation, internal fit and microleakage of translucent monolithic zirconia crowns.Materials and Methods: Sixty maxillary premolars were reduced based on basic guidelines of tooth preparation for a zirconia crown with either 0.5, 0.8 and 1.2 mm chamfer width (n=20each finish line width). After digital scanning and milling of zirconia crowns, the sintering procedure was performed in special furnace for two different sintering programs (n =10 per group) following either standard or speed sintering procedure. Each crown was cemented to its corresponding prepared tooth utilizing self-adhesive-resin cement. After 15000 thermal cycles between 5°C and 55°C, specimens were submersed in methylene blue for 12 hours. After sectioning bucco-lingually, marginal gap and cement film thickness values were recorded at nine sites using a digital microscope followed by microleakage scores examination.Results: Tested groups with 0.5 mm chamfer widths had the greatest mean marginal gap values of 47.9±5.4 and 50.1±5.6 µm for both conventional and speed sintering respectively, while groups with 1.2 chamfer widths had the lowest mean gap values of 42.3±5.6 and 44.5±5 µm for both standard and speed sintering, respectively. Two-way ANOVA revealed statically insignificant impact of sintering procedure on crown adaptation (p=.08). The greatest mean microleakage score (3±088 µm) was obtained from the 0.5 mm chamfer width group, while the smallest (2±0.78 µm) score was obtained from the 1.2 mm chamfer width group. Conclusions: Marginal adaptation and internal fit of translucent monolithic zirconia crowns are affected by width of the preparation margin while sintering protocol has little impact on adaptation.

In vitro marginal and internal adaptation of metal-ceramic crowns with cobalt-chrome and titanium framework fabricated with CAD/CAM and casting technique.

The purpose of this study was to compare the marginal and internal fit of Co-Cr and titanium ceramic crowns fabricated with 2 different techniques: CAD/CAM milling and traditional casting (TC). Ten traditional casting of Co-Cr (TCC), 10 CAD/CAM milling of Co-Cr (MC), 10 traditional casting of titanium (TCT), 10 CAD/CAM milling of titanium ceramic crowns (MT) were fabricated. Silicone replicas were obtained to measure internal gap volume, marginal gap and internal adaptation that was evaluated at 3 regions: axial wall, axio-occlusal angle, and occlusal surface. Measurements were made with a X-ray micro computerized tomography (micro-CT) and analyzed with Bonferroni and Dunnet T3 post-hoc tests (α = 0.05). One-way ANOVA revealed no statistically significant differences among the groups for measurements at the marginal gap (P > 0.05). At axial wall region the mean values of TCT group were higher than those of groups but only statistically not significant for TCC group (P < 0.05). TCC group statistically gives better results than MC group in axio-occlusal and occlusal regions (P < 0.05). The mean measurement of internal gap volume were 20.59 ± 0.83 mm3 for TCC, 22.73 ± 0.82 mm3 for MC, 22.83 ± 1.11 mm3 for TCT and 20.51 ± 1.16 mm3 for MT. Mean internal gap volume values MT group were smaller than those of groups but only statistically not significant for TCC group (P > 0.05). All groups performed similar marginal adaptation. The cement film thickness at axio-occlusal angle point and occlusal region were higher for MC crowns.

Comparative Evaluation of Film Thickness and Temperature of Different Luting Cements: An In Vitro Study

Comparative Evaluation of Film Thickness and Temperature of Different Luting Cements: An In Vitro Study

Evaluation of marginal and internal fit of acrylic bridges using optical coherence tomography.

The potential of non-invasive optical coherence tomography (OCT) as a tool for assessment of fit of indirect reconstructions is not fully explored. The objectives were to investigate the feasibility and validity of OCT, and to measure the internal and marginal fit of acrylic bridges fabricated using direct and indirect digitalisation. The accuracy of the employed swept source OCT (wavelength: 1310nm) was assessed by comparing with an object with known dimensions. Validity was assessed by measuring an OCT measurements on replica, mimicking the cement film thickness, with stereomicroscopic measurements. The reconstructions were placed on the abutments without cementation. The internal and marginal fit of acrylic bridges from direct and indirect digitalisation techniques were then assessed by obtaining 5 OCT B-scans per abutment tooth at pre-defined positions located 250μm apart. The marginal and internal cement gaps were measured using image-processing software (ImageJ). Mean and standard deviation were calculated for both groups and t test assuming unequal variances was carried out. The level of significance was defined at 0.05. A strong linear correlation (r=0.865) between OCT and stereomicroscopy was found. T test showed significantly (P<0.01) better internal fit of bridges made from indirect digitalisation, but no difference in marginal fit. OCT is a feasible and valid tool for investigating internal and marginal fit of acrylic dental reconstructions. Better internal fit was observed in bridges fabricated using the direct digitalisation technique. No difference in marginal fit was found between the two fabrication methods.

Physical Properties, Film Thickness, and Bond Strengths of Resin-Modified Glass Ionomer Cements According to Their Delivery Method.

To determine the effect of changing the dispensing or mixing method of resin-modified glass ionomer (RMGI) cements on their water sorption, solubility, film thickness, and shear bond strength. Disc-shaped specimens of RMGI cements (RelyX: Luting [handmix], Luting Plus [clicker-handmix], Luting Plus [automix], GC: Fuji PLUS [capsule-automix], FujiCEM 2 [automix], [n=10]) were prepared according to ISO standard 4049 for water sorption and solubility tests. Furthermore, the percentage of mass change, percentage of solubility, and percentage of water absorbed was also determined. Film thickness was measured according to ISO standard 9917-2; the mean of 5 measurements for each cement was calculated. Shear bond strength for each cement was determined according to ISO standard 29022 before and after thermocycling at 20,000 cycles, temperatures 5 to 55°C with a 15-second dwell time (n=10/subgroup). Two- and one-way ANOVA were used to analyze data for statistical significance (p < 0.05). Water sorptions of the RMGI cements were in close range (214-250 μg/mm3 ) with no statistical differences between counterparts (p > 0.05). RelyX Luting Plus (clicker-handmix) displayed lower solubility than its handmix and automix counterparts (p < 0.05). Film thickness of RelyX cements was significantly different (p < 0.05). RelyX Luting Plus (automix) had the lowest film thickness (19 μm) compared to its handmix (48 μm) and clicker-handmix (117 μm) counterparts (p < 0.05). GC Fuji PLUS (capsule-automix, 22 μm) was significantly lower than the automix version (GC FujiCEM 2, 127 μm) (p < 0.05). Shear bond strength of RelyX Luting Plus (automix) was significantly lower than its handmix and clicker-handmix versions (p < 0.05). GC Fuji PLUS (capsule-automix) was significantly higher than GC FujiCEM 2 (automix) (p < 0.05). The binary interaction of the two independent variables (dispensing/mixing method and thermocycling) was significant for the shear bond strengths of the GC cements only (p < 0.05). Change in the dispensing/mixing method of RMGI cement from the same brand may have an effect on its physical properties, in addition to its film thickness and shear bond strength. Newer, easier, and faster cement delivery systems are not necessarily better. Clinical outcomes of these differences are yet to be confirmed.

Comparative study on the tensile bond strength and marginal fit of complete veneer cast metal crowns using various luting agents: An in vitro study.

Introduction:Several commercially available luting agents are used to cement the dental restorations such as intra-coronal, extra-coronal, and fixed partial dentures. Tensile bond strength (TBS) and accurate marginal fit are the essential factors to determine the good clinical results in fixed prosthesis. The retentivity of the luting cements is assessed by their adhesive capacity over the tooth surface and metal surface. Generally, the adhesive ability has been evaluated with in vitro testing, with tensile bond tests. The failure of fixed prosthesis may be happened as a result of incomplete seating during cementation. Most research on cementation of crowns relates seating failure to the thickness of the cement film.Materials and Methods:The study is divided into four groups with 10 samples for each of the luting cement taken up for testing TBS and four groups with 5 samples for each luting agent chosen for assessing marginal fit. The results were tabulated and statistically analyzed.Results:In this in vitro study, the TBS of luting cements, and marginal fit in relation to luting cements were tested by using appropriate testing devices. The TBS of cement is measured using universal testing machine, and the results are tabulated. The marginal gap that exists between the margin of the cast metal crown, and the finish line is measured using travelling microscope before and after cementation. The difference between these two values gives the discrepancy that is due to the film thickness of cement used for luting the restoration.Summary and Conclusion:The TBS value of zinc phosphate cement and glass ionomer cement were found to be almost same. The chemical adhesiveness of the glass ionomer with calcium ions of enamel and dentin may be the attributed reason (ionic bonding). In this study, the polycarboxylate is the one that showed low TBS, and it may be attributed to the weakness of the cement due to reduced film thickness, though this cement has a chemical bonding nature. The observation of results of marginal fit in this study is the increased gap found in zinc phosphate cement followed by resin cement, zinc polycarboxylate, and glass ionomer cement. It is agreeable to estimate the marginal fit of the restoration, which could be affected by the film thickness of the luting cement along with other factors.

Evaluation of marginal/internal fit of chrome-cobalt crowns: Direct laser metal sintering versus computer-aided design and computer-aided manufacturing.

The purpose of this study was to evaluate the internal and marginal fit of chrome cobalt (Co-Cr) crowns were fabricated with laser sintering, computer-aided design (CAD) and computer-aided manufacturing, and conventional methods. Polyamide master and working models were designed and fabricated. The models were initially designed with a software application for three-dimensional (3D) CAD (Maya, Autodesk Inc.). All models were fabricated models were produced by a 3D printer (EOSINT P380 SLS, EOS). 128 1-unit Co-Cr fixed dental prostheses were fabricated with four different techniques: Conventional lost wax method, milled wax with lost-wax method (MWLW), direct laser metal sintering (DLMS), and milled Co-Cr (MCo-Cr). The cement film thickness of the marginal and internal gaps was measured by an observer using a stereomicroscope after taking digital photos in ×24. Best fit rates according to mean and standard deviations of all measurements was in DLMS both in premolar (65.84) and molar (58.38) models in μm. A significant difference was found DLMS and the rest of fabrication techniques (P < 0.05). No significant difference was found between MCo-CR and MWLW in all fabrication techniques both in premolar and molar models (P > 0.05). DMLS was best fitting fabrication techniques for single crown based on the results.The best fit was found in marginal; the larger gap was found in occlusal.All groups were within the clinically acceptable misfit range.