Bond Strength Of Resin Composites Research Articles

Effect of Preheating of Resin Composite on Microtensile Bond Strength In Vitro Study

BACKGROUND: Preheating resin composite was one of the latest achievements to improve the mechanical properties of composite. AIM: This study was conducted to assess the effect of preheating of resin composite on microtensile bond strength to dentin. METHODS AND MATERIALS: A total of 32 human molars were selected and divided into two groups according to the type of resin composites either microhybrid (P60) (R1) or nanohybrid (Z250 XT) (R2). The molar teeth were embedded in acrylic resin blocks then the occlusal enamel was removed parallel to cementoenamel junction to expose the dentin. Each group was subdivided into four subgroups according to the number of preheating cycles of resin composite either no heating (C0), one preheating cycle at 68℃ (C1), two preheating cycles at 68℃ (C2), or three preheating cycles at 68℃ (C3). After bonding of resin composite, specimens were cut into beams 1 mm thick and stressed in tension using a universal testing machine (4 teeth per group/12 beams per tooth). STATISTICAL ANALYSIS USED: Two-way ANOVA and Tukey’s post hoc tests were used to test the effect of preheating resin composites for the interaction of different variables. RESULTS: In both variables of the study, the type of resin composite and the number of preheating cycles have a statistically significant effect on the microtensile bond strength to dentin. There was a significant interaction between the variables. CONCLUSION: Pre-heating of Filtek P60 as a packable composite at 68℃ can achieve significantly higher microtensile bond strength compared to Filtek Z250 as a microhybrid composite. Key Messages: Preheating of resin composite enhances the mechanical properties of resin composite. Furthermore, better adaptation is due to easily flow of the material in additional to the improvement of microtensile bond strength of resin composite due to monomer and radical mobility due to complete polymerization during preheating.

A laboratory investigation on the effect of biguanide- and pyridine-derived antiseptics on the adhesion of resin composites to dentin.

Optimal bonding of adhesive restorations to dentin is crucial to prevent microleakage and enhance the survival of root-filled teeth. The aim of this study was to investigate the effect of chlorhexidine (CHX), alexidine (ALX) and octenidine dihydrochloride (OCT) on the bond strength of resin composites to coronal dentin. Human coronal dentin specimens were treated with 2% CHX, 0.1% ALX, 0.1% OCT or saline then restored with traditional or bulk-fill resin composites. The adhesion strength between the resin and dentin was measured using the microtensile bond strength and failure mode was determined using a stereomicroscope. Treatment with ALX and OCT resulted in significantly greater μTBS compared with CHX and saline, irrespective of the resin composite used. Alexidine treatment predominantly resulted in mixed failure, while adhesive failures were frequently observed in CHX and saline-treated dentin. In conclusion, final irrigation with ALX or OCT improved the bonding of resin composites to dentin.

Use of nonhydrolyzed silane prior to the silane-containing universal adhesive application improves the repair bond strength of resin composite

ObjectiveTo compare the effect of hydrolyzed and nonhydrolyzed silanes prior to the silane-containing universal adhesive application on the repair bond strength between old and new resin composite. Material and methodsFifty-four blocks of nanohybrid resin composite (Z350 XT) were aged by water storage for six months. The aged specimen surfaces were wet-ground manually with 320-grit silicon carbide grinding paper and randomly assigned into six experimental groups according to surface treatment: silane-containing universal adhesive in the self-etch mode (Scotchbond Universal); nonhydrolyzed silane (Silane Coupling Agent) plus Scotchbond Universal; hydrolyzed silane (RelyX Ceramic Primer) plus Scotchbond Universal; self-etch adhesive system (Clearfil SE Bond); nonhydrolyzed silane plus Clearfil SE Bond; hydrolyzed silane plus Clearfil SE Bond. Blocks were repaired with the same composite. After 24 h of water storage, the blocks were sectioned and bonded sticks were submitted to microtensile bond strength test (μTBS). Two-way ANOVA and Tukey's tests were used to analyze the μTBS means. ResultsThe highest repair bond strength values were achieved when nonhydrolyzed silane was applied prior to the silane-containing universal adhesive system (p = 0.03). The previous silane application did not increase the repair bond strength when a two-step self-etch adhesive was used. Mixed/adhesive failures prevailed in all groups. ConclusionThe use of a nonhydrolyzed silane prior to the silane-containing universal adhesive in the self-etch mode application improves the repair bond strength of old and new resin composite.

Effects of different storage media on dentin moisture, microhardness, and bond strength of resin composite.

In in vitro studies, it is desirable that the storage solutions in which dental samples kept between extraction and experiment should prevent dehydration and have antimicrobial properties. However, it should be taken into consideration that these solutions may have some effects that directly change test results on physical and mechanical properties of laboratory samples. The aim of this in vitro study was to evaluate the effects of different storage media on dentin moisture, microhardness, and microshear bond strength of resin composite to dentin. Thirty non-carious human premolars were randomly divided into three groups: 1. 0.1% Thymol (T), 2. Distilled water (DW), 3. Dry storage (DS) (control) (n = 10). Dentin moisture was measured with a digital grain moisture meter. Dentin microhardness was measured with the Vickers test. The bond strength was measured with a microshear test. Analysis of variance (ANOVA) followed by the Bonferroni test was used for statistical evaluation (p = 0.05). Dentin moisture of the experimental groups was statistically higher than that of the control group (p < 0.05). In addition, the dentin moisture of group DW was significantly higher than that of group T (p < 0.05). The mean microshear bond strength of resin composite to dentin was higher in group DW than in group T and group DS (p < 0.05), while there was no statistical difference between group T and group DS. The microhardness values of all groups were statistically similar. Storage solutions used for disinfection and to prevent dehydration may have negative effects on dentin moisture and bond strength.

Evaluation of antioxidant application on bond strength of composite resins to bleached enamel

Abstract Aim: This study aims to assess and evaluate the application of 10% sodium ascorbate, 5% green tea extract, 5% pomegranate peel extract, and 5% grape seed extract on shear bond strength of composite to bleached enamel. Materials and Methods: Sixty extracted human maxillary central incisors were randomly divided into seven groups. The enamel surface of these specimens was bleached with hydrogen peroxide (35%), except group VII (control group). Postbleaching, the specimens of group II were placed in artificial saliva for 2 weeks before restoration and the specimens of groups III and IV and groups V and VI underwent antioxidant application; 10% sodium ascorbate, 5% green tea extract, 5% pomegranate peel extract, 5% grape seed extract, respectively, for 10 min, followed by composite resin restoration, respectively. The specimens of group I were restored with composite resin immediately after bleaching. The specimens’ shear bond strength was tested using universal testing equipment. The data obtained were statistically analyzed using a one-way analysis of variance and the Tukey post hoc test. Results: There was no statistically significant difference in the effects of various antioxidants on the shear bond strength of bleached enamel. Conclusion: Within the constraints of the study, it was concluded that the application of antioxidants efficiently recovered the bond strength of bleached enamel. The application of 5% grape seed extract treatment demonstrated better bond strength among the antioxidants tested. Clinical Significance: Antioxidants can be used immediately following bleaching to restore resin composite bond strength without the requirement of delay in the treatment to reduce the nascent oxygen species in bleached teeth.

Impact of adhesive application errors on dentin bond strength of resin composite

Objectives: To investigate the impact of adhesive application errors on dentin bond strength of resin composite. Material and Methods: 165 extracted permanent human molars were ground to mid-coronal dentin. The dentin specimens were treated with one of three adhesive systems (OptiBond FL, Clearfil SE, Scotchbond Universal) either according to manufacturer’s instructions or with systematic errors in the application procedure and before application of resin composite (Filtek Z250). After storage (37 °C, 100% humidity, 24 h) shear bond strength (SBS) was measured and data analysed with either one-way ANOVA followed by Tukey tests (OptiBond FL, Scotchbond Universal, control groups) or Kruskal-Wallis followed by Wilcoxon tests (Clearfil SE). Finally, the failure mode of all specimens was assessed. Results: With OptiBond FL and Clearfil SE omitted application (p ≤ 0.0001) as well as no evaporation (p ≤ 0.001) of the solvents in the primer significantly reduced the SBS. Omitted application of the adhesive, respectively the bond, had a negative influence on the SBS of Clearfil SE (p < 0.0001), but not of OptiBond FL (p = 0.776). With Scotchbond Universal, no evaporation of the solvents (p < 0.0001) as well as no light-cure (p = 0.0004) had a significant negative influence on the SBS. Using the adhesive systems according to manufacturer’s instructions, Clearfil SE achieved significantly lower SBS than OptiBond FL and Scotchbond Universal (p = 0.0027). Adhesive failure at the dentin surface was generally the most frequent failure mode observed. Conclusion: All three adhesive systems tested were sensitive to application errors. For optimal result and longest possible durability of resin restorations, clinicians should strictly adhere to the manufacturer’s instructions.

Is the bond strength of zirconia-reinforced lithium silicate lower than that of lithium disilicate? - A systematic review and meta-analysis.

This study systematically reviewed the literature to compare the bond strength of resin composites with that of zirconia-reinforced lithium silicate (ZLS) and lithium disilicate (LD). This review was structured based on the Preferred Reporting Items for Systematic Reviews and Meta-Analyses (PRISMA 2020) statement. This study was registered at the International Prospective Register of Systematic Reviews (CRD42021256900). Studies were searched via PubMed, Web of Science, and Google Scholar databases without language or publication year limits. In vitro studies that evaluated the bond strength of the resin composites to ZLS and LD were included. The risk of bias in all the included articles was evaluated. Statistical analyses were performed using the Review Manager software (version 5.3, Cochrane Collaboration, Oxford, UK). Of the 90 potentially related articles, the full texts of 16 articles were evaluated after screening. Finally, seven studies were included in the qualitative synthesis and meta-analysis. All the studies presented a medium risk of bias. The results showed no significant difference in bond strength between the ZLS and LD groups (P = 0.94, mean difference=0.08, and 95% confidence interval=-1.93 to 2.10). However, a significant difference was found in the subgroup analysis considering different types of aging treatments (P = 0.0008) and different types of bond strength tests (P < 0.00001). The bond strength of resin composites was found to be similar to that of ZLS and LD, but different aging treatments and bond strength tests exhibited varying effects on the bond strength.

Effect of Remineralisation with Nano-hydroxyapatite (nHAp) and Non-collagenous Protein Analogues (PAA and STPP) on the Micro Tensile Bond Strength of the Resin Composites to Dentin – An In vitro Study

Background: Resin-dentin bonds are less durable than enamel as they rely on organic part for mineralisation. Bond denaturation mainly takes place because of hydrolysis of polymerized resin or degradation of water-rich, resin-sparse collagen by collagenolytic endogenous matrix metalloproteinase and cysteine cathepsins. Hence, this limited stability of dentin bonding tenaciously reduces the longevity of tooth-coloured restorations. One of the strategies adopted to encounter this shortcoming is to induce biomimetic remineralisation.&#x0D; Aim: To assess the microtensile bond strength of resin composites to dentin following remineralisation using an experimental paste containing nano-hydroxyapatite (nHAp) and biomimetic analogues, Poly Acrylic Acid (PAA) and Sodium Tri Polyphosphate (STPP).&#x0D; Methodology: Nine intact freshly extracted third molar were used for this study to evaluate the microtensile bond strength after treating with three different groups; Group I with paste containing nano hydroxyapatite nHAp Group II paste containing nHAp and non-collagenous protein analogues such as (Polyacrcrylic acid and Sodium tripolyphosphate) and the control groups containing adhesive and resin composite with no additional treatment. The samples were observed over a period of 24 hours and 1 week the inter group data analysis was done using ANOVA and paired sample t test and the intra-group data analysis over period of 24 hours the post HOC Bonferroni test was used for the statistical analysis.&#x0D; Results: After 24 hours the group with nHAp group showed highest value for microtensile bond strength among other groups, however after one week the group with nHAp +NCP analogues(PAA+STPP) showed highest value for microtensile bond.&#x0D; Conclusion: The treatment with the experimental paste [nHAp+NCP] analogues (PAA+STPP)] can bring about remineralisation to improve bonding to dentin.

Effects of remaining dentin thickness on the bond strength of bleached dentin

BackgroundThe bond strength of resin composites to dentin was reported to be related to either the remaining dentin thickness (RDT) or bleaching treatment. However, information is limited regarding the effects of RDT on the bond strength of bleached dentin. The present study aimed to investigate the effects of RDT on the microshear bond strength (μSBS) of resin cement to bleached dentin.MethodsA total of 120 dentin specimens were prepared and randomly divided into 2 groups: a bleaching group (group B) and a control group (group C). Hydrogen peroxide with a concentration of 35% (Ultradent, USA) was applied on the dentin surface for 2 × 1 d for group B, while no bleaching treatment was performed for group C. After the treatment, the specimens were finished and polished to obtain different RDTs (2, 1, and 0.5 mm) and divided into 3 groups of 20 specimens each. The bonding procedure was performed using Panavia V5 (Kuraray, Japan) with a bonding area of 0.785 mm2. For each group, half of the specimens were subjected to 5000 thermal cycles (subgroup T), while the other half did not receive thermocycling (subgroup N) (n = 10). The specimens were then subjected to the μSBS test using a universal testing machine. Data were analyzed by a three-way analysis of variance (α = 0.05). The fracture modes of the specimens were confirmed with a measuring microscope. Representative specimens with different fracture modes were observed with scanning electron microscopy (SEM).ResultsThe μSBS values were significantly affected by bleaching treatment (p < 0.001), whereas no significant effect was observed for thermocycling (p = 0.293). In terms of RDT, a significantly different μSBS value was found among the subgroups with different RDTs in group C (p = 0.003). However, the RDT did not significantly affect the μSBS values of bleached dentin in group B (p = 0.779). The μSBS values were significantly lower in group B than in group C (p < 0.001). A higher percentage of adhesive failure was observed in group B than in group C.ConclusionBased on the present findings, it can be concluded that the RDT did not affect the bond strength of resin cement to bleached dentin.Clinical significanceSince RDT did not affect the bond strength of resin cement to bleached dentin, bonding procedures should not be performed immediately after intracoronal bleaching, even if the dentin is planned to be removed due to a tooth preparation process.

Influence of various antioxidants on micro-shear bond strength of resin composite to bleached enamel.

Teeth bleaching causes an immediate decrease in resin composite bonding ability. This study aimed to investigate the influence of various antioxidants on resin composite bond strength to bleached enamel. One hundred and ten human maxillary incisors were used. A negative control (group A) (n = 10) was assigned (no bleaching-no antioxidant). The remaining teeth were divided into two groups (n = 50) according to the bleaching agent used: group B (40% hydrogen peroxide) and group C (35% carbamide peroxide). Both groups were subdivided into five subgroups (n = 10). A positive control subgroup (no antioxidant) and other four subgroups according to the antioxidant solution used (10% sodium ascorbate, 10% grape seed extract, 10% green tea extract, and 5% alpha-lipoic acid). After resin composite building, the micro-shear bond strength test was performed. Fracture analysis was examined using a stereomicroscope. Statistical analysis was performed using a two-way analysis of variance and Tukey's HSD post hoc test. Bond strength significantly decreased after bleaching and there was no significant difference between bleaching agents (P < .0848). Except for alpha-lipoic acid subgroups, the other antioxidants subgroups revealed significantly higher bond strengths than bleached control subgroups (P < .0001). All antioxidants used except alpha-lipoic acid were effective in the reversal of compromised bonding after bleaching. Immediate bonding procedures after bleaching are requisite when bleaching fails to treat teeth discoloration and the direct composite veneer is considered, also when shades of old composite restorations become mismatched after bleaching and should be replaced. Immediate reestablishment of resin bond strengths after bleaching can be achieved by using several antioxidants without the need for delay.

Effect of different surface treatments on the repair bond strength of resin composites with titanium

The purpose of this study was to evaluate the effect of different surface treatment combinations on the bonding of composite resins to NiCr and titanium alloys after thermal cycling. Square-shaped specimens (10 mm x 10 mm x 2 mm) were made from NiCr and titanium alloys. The specimens were divided into 6 pretreatment groups (n = 11): (1) machined titanium (control, no treatment); (2) CoJet sand application; (3) grinding with a diamond bur; (4) metal primer application; (5) CoJet sand + metal primer application; and (6) grinding with a diamond bur + metal primer application. The surface roughness of the mechanically treated specimens (control, grinding, CoJet sand) was evaluated. The surface morphology of both metals and elemental composition were examined with SEM and EDS. The composite resin was applied to the specimens. Shear bond strength (SBS) was tested after thermal cycling (5000 cycles, 5 °C to 55 °C). Failure modes were determined. The data were analyzed using the Shapiro-Wilk test, two-way ANOVA and post hoc Fisher’s LSD test (p = .05). For titanium specimens, the grinding + metal primer exhibited higher values than the other groups, and all groups showed higher SBS values than the control group. Combined use of CoJet sand, grinding with a diamond bur, and metal primer application would be useful for enhancing the bond strength of composite resin to titanium. The grinding of the NiCr surface with a diamond bur is the only method that could improve the bond strength of a composite resin compared to the other methods.

Comparative Study of Cementum and Dentin Shear Bond Strength using Resin Composite with Universal Adhesive System and Resin Modified Glass Ionomer

Objective: to compare the shear bond strength of resin composite using universal adhesive system containing MDP and resin modified glass ionomer cement to cementum and compare the results with those of cervical dentin. Materials and methods: A total of 12 lower premolars were used in this study, they were sectioned just above the cemento-enamel junction, the roots were then sectioned into two halves and divided into two main groups according to the tooth substrate in which group 1) Cervical dentin and group 2) Cementum. They were further subdivided into two subgroups according to the material used where n= 6 subgroup 1) Resin composite (Brilliant Ever-Glow) using universal adhesive (One coat 7 universal), subgroup 2) Resin modified glass ionomer (Fuji II LC). Shear bond strength was then evaluated for all specimens and statistically analyzed. Results: There was statistically significant difference between resin composite using universal adhesive system and resin modified glass ionomer when applied on cementum. While on comparing the resin composite using universal adhesive system and resin modified glass ionomer on cervical dentin it showed no statistically significant difference. Meanwhile no statistically significant difference was found between cervical dentin and cementum when using resin composite with universal adhesive system. Comparing resin modified glass ionomer on dentin and cementum there was also no statistical difference. Conclusion: using universal adhesive containing MDP with resin composite it showed the same bond strength to cervical dentin and cementum. While the resin modified glass ionomer showed higher bond strength to cementum than that of the universal adhesive system.

Effect of Remineralizing Agents on Bond Strength of Resin-Composites to Primary Enamel.

Aim: The purpose of this in vitro investigation was to assess the effect of three remineralizing agents (Voco Remin Pro®, Uncle Harry's remineralization kit, Sunshine remineralization gel) on the shear bond strengths of two resin-composites (Tetric® N-Ceram and Filtek™ Z250 Universal Restorative) to enamel of primary molars. Study design: Ninety-six enamel specimens were prepared and randomly distributed to eight groups according to the control, remineralizing agents, and resin composite used. Shear bond strength was measured at a crosshead speed of 0.5 mm/min and the type of bond failure was recorded. Results: The highest shear bond strength (Mean+SD) in MPa was for Tetric® N-Ceram/control [21.06+1.68] while the lowest was for Filtek™ Z250/Sunshine remineralization gel [11.98+1.46]. Tukey HSD Post Hoc Tests showed significant difference between Tetric® N-Ceram/control and all other groups (p=0.0001) except Filtek™ Z250/control. In addition, there was significant difference between Filtek™ Z250/control and all other groups (p=0.0001) except Tetric® N-Ceram/control and Tetric® N-Ceram/Uncle Harry's remineralization kit. Mode of failure was cohesive (9.38%), adhesive (55.21%), and mixed (35.42%). Conclusions: The three tested remineralizing agents affect shear bond strength of the tested resin-composites to enamel of primary teeth. In general, shear bond strength values were acceptable. Mode of failure was mostly adhesive.

Efficacy of multi-mode adhesive systems on dentin wettability and microtensile bond strength of resin composite

Purpose: To evaluate the wetting ability and the microtensile bond strength of adhesive systems in various depths of dentin. Materials and Method: 48 extracted human molars cut in half in buccolingual direction. Buccal and lingual surfaces were used to obtain deep (n = 48) and superficial (n = 48) dentin. Groups were divided into 4 subgroups: Self-etch (CSE), etch&rinse (SB), multi-mode self-etch (SAU) and multimode etch&rinse (EAU) adhesive systems. 3 consecutive contact-angle measurements were obtained: T0- 3 μl drop of distilled water on dentin; T1-Droplet of the adhesive; T2- Distilled water after polymerization of the adhesive. After composite build-ups, microtensile measurements were performed. Contact angle data were analysed with analysis of variance for repeated measures. Bond strength data were analyzed by repeated measures analysis of variance, comparisons were made according to the logarithmic values (p < 0.05). Results: The difference between groups was not significant regardless of dentin depth for all measurements (p < 0.05). All groups except CSE enhanced the wetting ability of the adhesive but reduced the wetting ability of distilled water after application of the adhesive (p < 0.05). Regarding adhesive systems, the groups showed no significant difference between bond strengths to various depths of dentin except SAU (p > 0.05); in SAU, bond strength to deep dentine were significantly higher than superficial dentin (p < 0.05). Regarding adhesives’ bond strength, CSE showed significantly greater values than the other groups (p < 0.05). Conclusion: The cavity depth does not affect the bonding ability for all adhesive systems; self-etch adhesive systems might be a better choice since different adhesives may influence the wetting ability and microtensile bond strength of the dentin substrates.

Repair bond strength of resin composite to bilayer dental ceramics.

PURPOSEThe purpose of this study was to investigate the effect of various surface treatments (ST) on the shear bond strength of resin composite to three bilayer dental ceramics made by CAD/CAM and two veneering ceramics.MATERIALS AND METHODSThree different bilayer dental ceramics and two different veneering ceramics were used (Group A: IPS e.max CAD+IPS e.max Ceram; Group B: IPS e.max ZirCAD+IPS e.max Ceram, Group C: Vita Suprinity+Vita VM11; Group D: IPS e.max Ceram; Group E: Vita VM11). All groups were divided into eight subgroups according to the ST. Then, all test specimens were repaired with a nano hybrid resin composite. Half of the test specimens were subjected to thermocycling procedure and the other half was stored in distilled water at 37℃. Shear bond strength tests for all test specimens were carried out with a universal testing machine.RESULTSThere were statistically significant differences among the tested surface treatments within the all tested fracture types (P<.005). HF etching showed higher bond strength values in Groups A, C, D, and E than the other tested ST. However, bonding durability of all the surface-treated groups were similar after thermocycling (P>.00125).CONCLUSIONThis study revealed that HF etching for glass ceramics and sandblasting for zirconia ceramics were adequate for repair of all ceramic restorations. The effect of ceramic type exposed on the fracture area was not significant on the repair bond strength of resin composites to different ceramic types.

Effects of surface treatments on repair bond strength of a new CAD/CAM ZLS glass ceramic and two different types of CAD/CAM ceramics.

We evaluated the effects of three different surface treatments and two different bonding procedures on shear bond strength of resin composites to different computer-aided design/manufacturing (CAD/CAM) ceramics with or without thermocycling. The test specimens were prepared from three different CAD/CAM ceramics (Group A, IPS e.max CAD; Group B, IPS e.max ZirCAD; Group C, Vita Suprinity). They were divided into eight subgroups according to the surface treatment and bonding procedures. After resin composite was applied to the surfaces of all test specimens, they were stored in distilled water for 24 h at 37°C. Next, half of the test specimens were subjected to a thermocycling procedure, and the other half were stored in distilled water at 37°C throughout thermocycling. The shear bond strength was performed using a universal testing machine. Statistical analysis revealed that the ceramic types (P > 0.0031) and thermocycling (P > 0.0021) did not, but the surface treatment technique did significantly affect the shear bond strength values (P < 0.05; except group C). Higher bond strength values were observed with HF etching in Groups A and C compared with the other tested surface treatments.

Effect of Ultraviolet Irradiation on Tensile Bond Strength of Resin Composites and Multi-Purpose Bonding System Treated Adherends

Effect of Ultraviolet Irradiation on Tensile Bond Strength of Resin Composites and Multi-Purpose Bonding System Treated Adherends

Effect of acid etching on the micro-shear bond strength of resin composite-calcium silicate interface evaluated over different time intervals of bond aging.

Introduction:With the introduction of calcium silicate materials, pulp capping procedure has been simplified due to their therapeutic pulp capping capabilities and ability to be used as a provisional bulk restorative material simultaneously. The quality of the adhesive bond between these cements and composite is of clinical significance with regard to the longevity of the final laminate restoration. Thus, this study aims to compare the in vitro microtensile bond strengths of resin composite to different calcium silicate cements versus glass ionomer cement (GIC).Materials and Methodology:Resin composite was bonded to standardized disks of Biodentine, mineral trioxide aggregate (MTA), and GIC. The samples were divided into the following three groups, and each group was further divided into two subgroups based on the aging time (1 and 2 weeks) of the samples: (1) Group 1 – phosphoric acid etching on Biodentine. (2) Group 2 – phosphoric acid etching on MTA. (3) Group 3 – phosphoric acid etching on GIC. After bond aging, the microtensile bond strength was analyzed using the Instron universal testing machine.Results:There was no significant difference in micro-SBS between 1- and 4-week bond aging of MTA and Biodentine group, while a significant decrease is seen in the GIC group.Conclusion:Calcium silicate cements are weak in the early setting phase. Thus, placing the overlying composite is best delayed for at least 2 weeks to allow adequate maturation of the material.

Effect of aging in artificial saliva on the shear bond strength of resin composite

Effect of aging in artificial saliva on the shear bond strength of resin composite

The effect of green tea extract as a matrix metalloproteinase inhibitor on the bond strength of resin composite

The effect of green tea extract as a matrix metalloproteinase inhibitor on the bond strength of resin composite