Abstract The freeze resistance of vulcanized polymers has been evaluated for the past two years at this laboratory by a method which involves measurements of primary creep at successively lower temperatures. This method has been found to be particularly useful when it is desired to know, within 5° or 10° F, the temperature at which the polymer ceases to function as a rubberlike material. In a laboratory of this kind, where considerable work is done in evaluating new polymer types and where the polymerization variables studied often are of such a nature as to produce relatively large changes in the freeze resistance of the vulcanized polymer, a tolerance of 5° to 10° F has been found to be a workable value. The test is simple and can be carried out with the Shore A durometer or the A.S.T.M. hardness tester, one or both of which are generally available in a rubber laboratory. Its simplicity notwithstanding, the test is reasonably objective. Both the durometer and the A.S.T.M. tester are handled in the conventional manner, and readings are taken five and 30 seconds, respectively, after the pressure plate or presser foot contacts the specimen. The degree of creep is recorded as the difference in hardness points between these two readings. It is a matter of experience that, for most polymers, the amount of creep or flow exhibited at successively lower temperatures increases gradually, reaches a maximum, and then begins to decrease at a relatively high rate. The temperature at which this rapid drop-off occurs is considered significant because at this point the polymer begins to lose, at an accelerated rate, the fluidity which it had at higher temperatures and is being transformed into a hard, nonrubberlike material.