Stainless Steel AISI Research Articles

Mechanical Properties and Strengthening Contributions of AISI 316 LN Austenitic Stainless Steel Grade

The main goal of this contribution is to evaluate the mechanical properties, strengthening contributions and microstructure development of austenitic stainless steel AISI 316 LN with high nitrogen content in the states characterized as the initial state and the states after rolling with different thickness deformations. The initial state was represented by solution annealing (777 K/60 min). The deformation state was characterized by rolling thickness reductions carried out at ambient temperature (TA = 295 K) with deformations in the range ε ∈ (0; 50> [%]. Studies of microstructures, mechanical properties and strengthening contributions before and after rolling were carried out. The initial state after solution annealing was as follows: offset yield strength Rp0.2 = 325 MPa, elongation A5 = 49% and diameter of grain size d =214 μm. The state after ambient rolling with thickness deformation ε = 50% was as follows: Rp0.2 = 994 MPa, A5 = 4% and d =64 μm. The maximum contribution to strengthening after rolling processing with 50% thickness deformation was dislocations (∆ R P0.2_DS =560 MPa) followed by twins (∆ R P0.2_DT =140 MPa).

Metal Powder Production by Atomization of Free-Falling Melt Streams Using Pulsed Gaseous Shock and Detonation Waves

A new method of producing metal powders for additive manufacturing by the atomization of free-falling melt streams using pulsed cross-flow gaseous shock or detonation waves is proposed. The method allows the control of shock/detonation wave intensity (from Mach number 4 to about 7), as well as the composition and temperature of the detonation products by choosing proper fuels and oxidizers. The method is implemented in laboratory and industrial setups and preliminarily tested for melts of three materials, namely zinc, aluminum alloy AlMg5, and stainless steel AISI 304, possessing significantly different properties in terms of density, surface tension, and viscosity. Pulsed shock and detonation waves used for the atomization of free-falling melt streams are generated by the pulsed detonation gun (PDG) operating on the stoichiometric mixture of liquid hydrocarbon fuel and gaseous oxygen. The analysis of solidified particles and particle size distribution in the powder is studied by sifting on sieves, optical microscopy, laser diffraction wet dispersion method (WDM), and atomic force microscopy (AFM). The operation process is visualized by a video camera. The minimal size of the powders obtained by the method is shown to be as low as 0.1 to 1 μm, while the maximum size of particles exceeds 400–800 μm. The latter is explained by the deficit of energy in the shock-induced cross-flow for the complete atomization of the melt stream, in particular dense and thick (8 mm) streams of the stainless-steel melt. The mass share of particles with a fraction of 0–10 μm can be at least 20%. The shape of the particles of the finest fractions (0–30 and 30–70 μm) is close to spherical (zinc, aluminum) or perfectly spherical (stainless steel). The shape of particles of coarser fractions (70–140 μm and larger) is more irregular. Zinc and aluminum powders contain agglomerates in the form of particles with fine satellites. The content of agglomerates in stainless-steel powders is very low. In general, the preliminary experiments show that the proposed method for the production of finely dispersed metal powders demonstrates potential in terms of powder characteristics.

Analysis of microstructural, corrosion, and wear properties of austenite SS304 joints welded by underwater wet automated metal arc welding

This study explores the feasibility of using underwater wet automated metal arc welding. A specially designed welding setup was used, providing precise control over the x, y, and z axes to weld the high strength Austenite AISI304 stainless steel in present study. The welding process operated at 145 Amps of current, a voltage of 23 V, a feed rate of 2.5 mm/sec, and utilized a 3.15 mm × 350 mm flux-coated SS304 electrode, ensuring sufficient arc generation for effective welding. Microstructural analysis was conducted using optical microscopy and FESEM, while corrosion performance was evaluated through potentiodynamic tests, and wear characterization was performed using an engine tribometer. The weld zone exhibited a refined, columnar grain structure, which improved corrosion resistance, with a corrosion rate (CR) of 0.01052 mmpy, as determined by Tafel testing. Additionally, wear resistance tests revealed that the weld specimen outperformed the base metal, with a wear rate of 2.352 g/Nm × 10−10 compared to the base metal's 3.201 g/Nm × 10−10. The results emphasize the potential of underwater wet automated metal arc welding in enhancing the structural integrity of marine constructions through improved corrosion and wear performance.

INFLUENCE OF SHORT-PULSE LASER RADIATION ON THE SURFACE MICROSTRUCTURES FORMATION AND HARDNESS OF STAINLESS STEEL

The paper deals with the issues related to the technology of short-pulse laser treatment of AISI321 steel. The object of the study is the surface structures formed after short-pulse exposure to a nanosecond laser, as well as their physical and mechanical characteristics. The subject of the study in the work are the processes of formation of periodic surface structures after short-pulse laser exposure. The assumption about correlation of the character of formation of structural transformations in the surface layer of the processed material during the process of laser exposure with low intensity of laser radiation, and traditional heating cooling was formed. It is noted that when the corresponding critical irradiation conditions (irradiation power, heating and cooling rates, strain gradient, etc.) are reached, laser hardening of austenitic steel with hardness increase, i.e. quenching, occurs. It is emphasised that short-pulse laser exposure at low laser powers causes such processes in the surface layer of AISI321 stainless steel, which mainly prevent the deposition of chromium carbide and do not strengthen the material, and the absorbed laser energy is still insufficient to significantly create martensitic structures. It is also emphasised that the repeated short-term superposition of heat spots repeatedly crossing each other results in an increase in the thermal deformation of the material and, as a result, stronger crystal structures such as martensite, carbides and oxides are formed in the surface layer.

Tracing the Formation of Femtosecond Laser-Induced Periodic Surface Structures (LIPSS) by Implanted Markers.

The generation of laser-induced periodic surface structures (LIPSS) using femtosecond lasers facilitates the engineering of material surfaces with tailored functional properties. Numerous aspects of their complex formation process are still under debate, despite intensive theoretical and experimental research in recent decades. This particularly concerns the challenge of verifying approaches based on electromagnetic effects or hydrodynamic processes by experiment. In the present study, a marker experiment is designed to conclude on the formation of LIPSS. Well-defined concentration depth profiles of 55Mn+- and 14N+-ions were generated below the polished surface of a cast Mn- and Si-free stainless steel AISI 316L using ion implantation. Before and after LIPSS generation, marker concentration depth profiles and the sample microstructure were evaluated by using transmission electron microscopy techniques. It is shown that LIPSS predominantly formed by material removal through locally varying ablation. Local melting and resolidification with the redistribution of the material occurred to a lesser extent. The experimental design gives quantitative access to the modulation depth with a nanometer resolution and is a promising approach for broader studies of the interactions of laser beams and material surfaces. Tracing LIPSS formation enables to unambiguously identify governing aspects, consequently guiding the path to improved processing regarding reproducibility, periodicity, and alignment.

Investigation of cutting qualities of AISI304 stainless steel using plasma arc cutting method

Since cutting stainless steels with non-traditional manufacturing processes such as laser beam cutting or water jet cutting is quite costly, machining with the plasma arc cutting (PAC) method, which is generally more economical, has been preferred more frequently in recent years. In this context, the use of PAC method in manufacturing of machine parts, especially in the construction and manufacturing industries, as well as in other industries such as food, automotive and petrochemicals, is increasing day by day. In these sectors, where high corrosion resistance and resistance to acidic environments are required, AISI304 stainless steel is generally preferred as the raw material. In this study, comprehensive literature research on PAC was conducted and the cutting qualities of AISI304 stainless steel plates with 4 and 8 mm thickness were investigated. Nine different types of experiment conditions (E1-E9) were created by the machining parameters (gas pressure: 0.6, 0.7 and 0.8 MPa – cutting speed: 151, 215 and 217 mm/min) determined from other experimental studies in the literature. The lowest average kerf taper value (0.32̊) was obtained on the 4 mm thick plate with a gas pressure of 0.6 MPa and a cutting speed of 151 mm/min, whereas the highest average kerf taper value (2.59̊) was obtained on the 8 mm thick plate where the gas pressure was 0.8 MPa and the cutting speed was 217 mm/min. The results revealed that for both plates, as the cutting speed increases at constant pressure values, the cutting surface roughness values ​​increase. On the other hand, as the cutting speed is constant, the surface roughness decreases as the gas pressure value increases. The plates were cut into 100 mm long straight lines and the bottom surface burr formations and the top surface spatter formations in the PAC method were also examined.

Study of the coefficient of friction and forward slip in cold rolling of stainless steel AISI 430 in Sendzimir mills

Study of the coefficient of friction and forward slip in cold rolling of stainless steel AISI 430 in Sendzimir mills

FEM Analysis of Crane Hooks with Different Cross Section

In this paper the 3D model of the crane hook was realized using Autodesk Inventor Professional 2025 and finite element analysis, was performed using Ansys Workbench, in order to determine the state of stress, deformation and safety factor, by applying restrictions and loads conditions. Two materials were chosen, for crane hook, in accordance with the specialized literature. The materials taken for static analysis was Stainless Steel AISI 1020 and 34CrMo4. The FEM analysis of a crane hook provides critical information for evaluating the design's structural integrity, identifying potential problem areas, and ensuring that the hook can safely carry the loads it is intended to handle.

ZrN-Based Multilayers Prepared by Reactive Sputtering as Coatings for Electrode Plates of Proton Exchange Membrane Water Electrolyzers.

ZrN and TiN thin coatings have been investigated for use on stainless steel for bipolar plates of proton exchange membrane water electrolyzers. Films were deposited by reactive magnetron sputtering using Ar and N2 from metallic Zr and Ti targets on different substrates to perform a deep characterization of their relevant properties. The effect of the deposition parameters, such as N2/Ar ratio, working pressure, or supplied power, has been explored. The structural, electrical, compositional, and optical properties of the films have been investigated by different techniques such as X-ray diffraction, 4-probe van der Pauw resistance, Rutherford backscattering, and optical reflectance and Raman spectroscopies, providing significant information about the films. Finally, after optimization of the preparation parameters to obtain suitable films, the electrochemical behavior of stainless steel coated by different films has been tested. The obtained corrosion current density for a ZrN/TiN/ZrN trilayer on mirror-polished AISI-304 stainless steel evidence their potential as electrodes in bipolar plates of proton exchange membrane electrolyzers.

Intercomparison of Indexable Cutting Inserts' Wear Progress and Chip Formation During Machining Hardened Steel AISI 4337 and Austenitic Stainless Steel AISI 316 L.

This article deals with a mutual comparison of indexable cutting inserts of the CNMG 120408 type from two different manufacturers during the machining of hardened steel AISI 4337 and austenitic stainless steel AISI 316 L. The main goal is to analyse the different wear processes depending on the difference in the manufacturer's design and also depending on the properties of the different machined materials. The progress of the wear of the main spine of the tool, the types of wear and the service life of the cutting edge were monitored, with the achievement of the critical value VBmax = 300 µm being the standard. In addition to the wear of the inserts, the production of chips was monitored in terms of their shape, average size and number of chips per 100 g of chips produced. In order to understand the relationships arising from the obtained data, an SEM equipped with an elemental analyser was used to analyse the coating layers and the substrate of the unworn inserts and the types of wear and the intensity of the surface damage of the worn inserts. A several-fold difference in the lifetime of the cutting edge was found, both in terms of design and in terms of the selected machined material, while in both cases the cutting edge with Al2O3 and TiCN layers of half thickness achieved a better result in liveness. From the point of view of chip formation, very similar results in shape and average length were observed despite the different designs of chip breakers. Cutting inserts with half the thickness of the coating layers achieved longer cutting edge life in the non-primary material application compared to the target workpiece material. At the same time, it was observed that a thinner coating layer has a positive effect on chip formation in terms of its length and shape.

Investigating the effect of dynamic laser beam oscillations in remote fusion cutting process

The latest research on laser beam fusion cutting has revealed significant improvements in process productivity and cut quality through the use of dynamic beam shaping techniques. While many studies have investigated dynamic beam shaping for proximity cutting, the influence of laser beam oscillations on the remote fusion cutting process remains unexplored. The present work aims to study the effect of dynamic beam shaping on the remote fusion cutting process through analytical modeling, experimental investigations, and in situ high-speed monitoring. Initially, an analytical model based on thermodynamic analysis was developed to assess the influence of circular oscillations on the process zone. This model facilitates the evaluation of process performance from an energetic perspective, providing an estimate of the maximum achievable cutting speed for the remote fusion cutting process across various operating conditions. A significant increment in process productivity could be achieved through beam oscillations. Furthermore, based on theoretical findings, the effect of circular laser beam oscillations superimposed on the processing feed direction was experimentally investigated using a 1 mm thick AISI304 stainless steel material. A 6 kW fiber laser was utilized, alongside a high-speed camera-based system for in situ process monitoring. The experimental results demonstrate a significant increase in the process productivity under dynamic beam shaping conditions, consistent with theoretical findings. Specifically, the maximum achievable cutting speed could be increased from 0.13 to 0.20 m/s. Furthermore, the cut quality of produced samples was evaluated in terms of kerf morphology and profile.

Static and Thermal Analysis of Internal Combustion Engine Valves

Abstract: In this paper the 3D model of the internal combustion engine valves was realized using Autodesk Inventor Professional 2024 and finite element analysis, static and thermal was performed, in order to determine the state of stress, deformation and temperature evolution, by applying restrictions and loads conditions. Two materials were chosen, for internal combustion engine valves, in accordance with the specialized literature. The materials taken for static and thermal analysis was Stainless Steel AISI 446 and NiCr0TiAl. Following the comparative study for the two models, it can be specified the importance of the material for the construction of the internal combustion engine valves who depends on the material properties and their design.

Experimental and numerical study of dissimilar fiber laser welding of martensitic AISI 1060 carbon steel with different configuration with austenitic 304 and ferritic 420 stainless steel

Welding with fiber laser for two distinct stainless steel types was performed to join with the martensitic carbon steel (AISI 1060) in order to assess the effect of laser welding operating parameters for two dissimilar materials on the weld characterization thorough experimental design method and numerical investigation. A full central composite design (CCD) matrix in accordance with the response surface methodology (RSM) was developed to represent the responses variations by equations including quadratic and nonlinear interaction terms. Different laser welding parameters were taken into account, such as laser power, linear speed of welding, focal distance of the beam, and beam deviation. The responses considered were the temperature field next to the melt pool border line, the maximum penetration depth of the fusion zone and the ultimate tensile strength of the dissimilar weld joint. Additionally, the variation of the microstructure fusion zone and adjacent areas and failure mechanism of the weld joint were evaluated. The experimental results indicate that the temperature field measured at the vicinity of the melt pool fusion line with both 304 and 420 stainless steel which primarily influenced by the incident power of the laser and linear velocity of beam, respectively. Additionally, the numerical simulation results are in good agreement with temperature experimental results at vicinity of fusion line where the temperature measured, experimentally. Apart from this, at the center of the fusion zone, the temperature clearly predicts via numerical simulation results which is not possible to assess experimentally. A clear comparison between the temperature distribution with different joint configuration illustrates that distinct relation between the temperature variation rate and different thermal conductivity coefficient of AISI 1060 with different AISI 304 and 420 joint configuration resulted different temperature distribution. The weld joint microstructure for 420 stainless steel–AISI 1060 steel joint at fusion boundary zone consists of columnar dendrites and skeletal columnar ferrite. At the center of fusion zone, a cellular-type structure is seen. For 304 stainless steel joint, the fusion zone has composed of a remarkable part of skeletal delta-ferrite and dendritic microstructure at austenite matrix microstructure. The fracture section of 304 steel has a ductile fracture and the depth of fracture dimples and cavities toward 304 stainless steel are higher than AISI 1060 steel.

Application of impact-based and laser-based surface severe plastic deformation methods on additively manufactured 316L: Microstructure, tensile and fatigue behaviors

Applying post-processing methods can play a crucial role in addressing defects inherent in the as-built state of additively manufactured materials. This study comprehensively examined the effects of various post-processing techniques, including surface severe plastic deformation (SSPD) methods such as severe shot peening (SSP), ultrasonic shot peening (USP), ultrasonic nanocrystal surface modification (UNSM), and laser shock peening (LSP), combined with stress relieving (SR) on the tensile properties and fatigue behavior of laser powder bed fusion (LB-PBF) stainless steel AISI 316L specimens. Experimental characterization was carried out, focusing on microstructure, porosity, surface texture, hardness, residual stresses, monotonic tensile properties, and rotating bending fatigue behavior. The results demonstrated an excellent combination of enhanced strength and ductility after applying SR and SSPD treatments. Additionally, the post-processing methods significantly improved fatigue behavior by increasing strength, closing subsurface pores, surface layer nanocrystallization and hardening, inducing compressive residual stresses, and modifying the surface texture. Notably, in the high-cycle fatigue regime at the lowest stress amplitude, the SR + UNSM treated specimens exhibited the greatest improvement in fatigue life, followed by SR + USP, SR + SSP, SR + LSP, and SR, when compared to the as-built state.

Effect of TaC content on microstructure and wear behavior of PRMMC Fe-TaC coating manufactured by electrospark deposition on AISI304 stainless steel

The Fe-TaC coatings on stainless steel by electrospark granule deposition in an anode mixture of iron granules and tantalum carbide powder were first obtained. The material deposition rate on the substrate increased with the TaC powder concentration growth in the anode mixture, facilitating the initiation of electrical discharges. X-ray analysis of deposited coatings shows the presence of the TaC, γFe, and αFe phases. The tantalum carbide concentration grows with an increase in the content of TaC powder in the anode mixture, from 2.4 to 14.8 vol%. The dependence of the wear rate of coatings on the concentration of tantalum carbide in the anode mixture had a parabola form, with a minimum of 5 vol%. However, with a further increase in the TaC concentration in the anode mixture, the wear rate of the coatings monotonically increased due to spalling of TaC grains due to a deficiency of the metal binder.

Bending fatigue behavior of metastable and stable austenitic stainless steels with different surface morphologies

AbstractThe surface morphology has a significant influence on the fatigue behavior of components. For austenitic stainless steels (ASSs), this issue is even more pronounced due to their metastability. Based on the complex deformation mechanisms of metastable ASSs, which include dislocation slip, deformation twinning, and deformation‐induced martensitic phase transformation, the metastable stainless steel AISI 347 was investigated in this study together with the stable AISI 904L as a reference material. Four‐point bending fatigue tests with load ratio R = 0.1 and testing frequency f = 10 Hz at ambient temperature were carried out on specimens with five technically relevant surface morphologies: mechanical polished, milled, microshot peened, laser shock‐peened, and ultrasonic modified. Systematic material characterizations were carried out to elucidate the crucial role of surface roughness and deformation‐induced α′‐martensite in the fatigue behavior of both metastable and stable materials. While surface roughness is a well‐known key factor in conventional fatigue cases, deformation‐induced martensite layers implemented by various surface modification methods were proven to improve the fatigue life in metastable austenitic steels, opening new perspectives to extend the lifetime of ASS components.

Effect of Residual Stresses on the Fatigue Stress Range of a Pre-Deformed Stainless Steel AISI 316L Exposed to Combined Loading

AISI 316L austenitic stainless steel is utilized in various processing industries, due to its abrasion resistance, corrosion resistance, and excellent properties over a wide temperature range. The physical and mechanical properties of a material change during the manufacturing process and plastic deformation, e.g., bending. During the combined tensile and bending loading of a structural component, the stress state changes due to the residual stresses and the loading range. To characterize the component’s stress state, the billet was bent to induce residual stress, but a phase transformation to martensite also occurred. The bent billet was subjected to combined tensile–bending and fatigue loading. The experimentally measured the load vs. displacement of the bent billet was compared with the numerical simulations. The results showed that during fatigue loading of the bent billet, both the initial stress state at the critical point and the stress state during the dynamic loading itself must be considered. Analysis was demonstrated only for one single critical point on the surface of the bent billet. The residual stresses due to the phase transformation of austenite to martensite affected the range and ratio of stress. The model for the stress–strain behaviour of the material was established by comparing the experimentally and numerically obtained load vs. displacement curves. Based on the description of the stress–strain behaviour of the pre-deformed material, guidelines have been provided for reducing residual tensile stresses in pre-deformed structural components.

Effect of welding parameters on microstructure and mechanical properties of dissimilar AISI 304/ductile cast iron fusion welded joints

Problems associated with dissimilar fusion welding are mainly originated from the differences in melting points, coefficients of thermal conductivity and thermal expansion, …etc., and carbon content when welding dissimilar ferrous materials. In this study, the problems associated with dissimilar fusion welding of stainless steel AISI304 with ductile cast iron DCI grade A536 were investigated. Using shielded metal arc welding (SMAW) process, various welding parameters were studied to investigate the successful/accepted dissimilar welded joint(s). Welding electrodes and welding techniques were the main studied parameters. Microstructural and mechanical investigations were carried out for welded joints under different welding parameters. Tensile, impact and hardness tests coupled with optical and scanning electron microscopic examinations with EDX analysis were made for metallurgical and mechanical evaluations of welded joints. This extensive study could solve the problem of dissimilar welding between ductile cast iron and 304 stainless steel. The main results showed that joints welded by ENiCrFe-3 electrode in root pass and ENiFe-CI in filling passes were the successful dissimilar welded joints with 422 MPa tensile strength which represents 104% of annealed DCI base metal and without any changes in toughness properties, where toughness at HAZ of DCI was 18 J. High Ni content in weld metal increased the strength, ductility and reduced the weld metal dilution.

Tribocorrosion of couplings in seawater environment: An investigation on the positive-negative role of synergy

Tribocorrosion is a recent paradigm of tribology defined as the combination of simultaneous mechanical and chemical wear of couplings. To date, this phenomenon is common in several engineering fields, such as the naval sector where marine equipment, offshore platforms and so on are clear examples. In this regard, the synergy between the mechanical and the chemical effects has a notable effect on the behavior of couplings in seawater environment. Nevertheless, the latter can act also as antagonistic factor. Hence, in this manuscript, an investigation was conducted on a tribosystem composed of an alumina sphere and a stainless-steel AISI 316 L flat, immersed in an artificial seawater solution of 3.8 % NaCl and a pH of 8.2. The analysis, carried out by a reciprocating tribometer equipped with a two/three-electrode potentiostat, was performed for different loads and frequency values, and their correlation with synergistic effects was investigated. The open-circuit potential, friction coefficient, tribocorrosive current and total wear were evaluated for different tribological conditions. It was found that the force and sliding velocity had a significant position in the synergistic response, passing from positive to negative mainly due to the protective action of oxide layer and lubrication behavior of corrosion products formed during the motion. Moreover, the current was modeled via two analytical laws discussed in literature, providing a good agreement with experimental data. Lastly, was provided the oxide thickness evolution formed on the samples surface and its relationship with total wear.

Determining of the effect of reinforcing microrelief guides on the efficiency of folding integrated covers

The object of research is the processes of strengthening the working surfaces of profile folding strips made of stainless steel AISI 347 and carbon steel AISI 1005 using laser formation of microrelief guides. The analytical and experimental studies are based on the technique of laser microrelief formation by pulsed laser effects. The main assumption of the study is that the use of laser microrelief formation could increase the hardness and wear resistance of the folding strips, improving the process of folding integrated covers. Analyzing the effect of different hardening methods on the mechanical properties and wear resistance of the working surfaces of folding strips is necessary to achieve this goal. A methodology for assessing microstructural changes and their impact on the mechanical properties of folding strips during laser hardening has been proposed. It has been shown that the formation of microrelief guides by laser pulse exposure reduces the thermal load on the material, increases the uniformity of hardening and wear resistance. The revealed wear rates calculated for carbon steel AISI 1005 are 0.875, and for stainless steel AISI 347 – 0.345. To improve the accuracy and efficiency of the folding process, a methodology has been devised for calculating the quantitative formation of microrelief guides on the working surface of profile folding strips. This will not only improve the wear resistance and mechanical properties of the strips but also optimize production processes. Differences in the results of hardening for stainless steel AISI 347 and carbon steel AISI 1005 were found: the hardness values for AISI 347 are 3,088–4,904 MPa at a load of 50–350 g with a deviation of 37.1 %, and for AISI 1005 – 2141–1665 MPa with a deviation of 22.3 %